{"id":6201,"date":"2026-01-06T08:03:28","date_gmt":"2026-01-06T08:03:28","guid":{"rendered":"https:\/\/www.hcftir.com\/?p=6201"},"modified":"2026-01-12T05:51:34","modified_gmt":"2026-01-12T05:51:34","slug":"standard-operating-procedure-preparation-of-high-quality-kbr-pellets-for-ftir-analysis","status":"publish","type":"post","link":"https:\/\/www.hcftir.com\/ja\/standard-operating-procedure-preparation-of-high-quality-kbr-pellets-for-ftir-analysis-article\/","title":{"rendered":"\u6a19\u6e96\u64cd\u4f5c\u624b\u9806\uff1aFTIR\u5206\u6790\u7528\u9ad8\u54c1\u8ceaKBr\u30da\u30ec\u30c3\u30c8\u306e\u8abf\u88fd"},"content":{"rendered":"

\u76ee\u7684<\/h2>\n\n\n\n

\u9ad8\u900f\u904e\u7387\u3067\u4e0d\u7d14\u7269\u306e\u306a\u3044KBr\u30b5\u30f3\u30d7\u30eb\u30c7\u30a3\u30b9\u30af\u3092\u4f5c\u6210\u3059\u308b\u305f\u3081\u306e\u6a19\u6e96\u5316\u3055\u308c\u305f\u30d7\u30ed\u30bb\u30b9\u3092\u5b9a\u7fa9\u3057\u3001\u660e\u78ba\u306a\u7279\u6027\u30d4\u30fc\u30af\u3092\u78ba\u4fdd\u3057\u3001\u30d9\u30fc\u30b9\u30e9\u30a4\u30f3\u5e72\u6e09\u3092\u6700\u5c0f\u9650\u306b\u6291\u3048\u308b\u3002 FTIR\u5206\u5149\u6cd5<\/a>.<\/p>\n\n\n

\n
\"\"<\/figure><\/div>\n\n\n

\u7d20\u6750\u3068\u74b0\u5883\u4ed5\u69d8<\/h2>\n\n\n\n
    \n
  • KBr\u306e\u7d14\u5ea6\uff1a<\/strong> FTIR\u30b0\u30ec\u30fc\u30c9\uff08\u30b9\u30da\u30af\u30c8\u30eb\u30b0\u30ec\u30fc\u30c9\uff09\u306eKBr\uff08\u7d14\u5ea6$ge$ 99.99%\uff09\u306e\u307f\u3092\u4f7f\u7528\u3057\u3066\u304f\u3060\u3055\u3044\u3002\u5206\u6790\u30b0\u30ec\u30fc\u30c9\u3084\u5316\u5b66\u30b0\u30ec\u30fc\u30c9\u306f\u3001\u30b4\u30fc\u30b9\u30c8\u30d4\u30fc\u30af\u306e\u539f\u56e0\u3068\u306a\u308b\u5fae\u91cf\u306e\u70ad\u9178\u5869\u3084\u785d\u9178\u5869\u3092\u542b\u3080\u305f\u3081\u907f\u3051\u3066\u304f\u3060\u3055\u3044\u3002<\/li>\n\n\n\n
  • \u4e7e\u71e5\u3055\u305b\u308b\uff1a<\/strong> KBr\u7c89\u672b\u306f\u3001120\u2103\uff5e150\u2103\u306e\u30aa\u30fc\u30d6\u30f3\u3067\u5c11\u306a\u304f\u3068\u30822\u6642\u9593\u713c\u304f\u5fc5\u8981\u304c\u3042\u308b\u3002\u30c7\u30b7\u30b1\u30fc\u30bf\u30fc\u307e\u305f\u306f60\u2103\u306e\u4fdd\u6e29\u5eab\u3067\u4fdd\u7ba1\u3059\u308b\u3002<\/li>\n\n\n\n
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    \u6a5f\u6750\u306e\u6e96\u5099<\/h2>\n\n\n\n
      \n
    • \u4e73\u9262\u3068\u4e73\u68d2\uff1a<\/strong> \u30a2\u30b2\u30fc\u30c8\u30bb\u30c3\u30c8\u306e\u307f\u3092\u4f7f\u7528\u3057\u3066\u304f\u3060\u3055\u3044\u3002\u30ac\u30e9\u30b9\u3084\u78c1\u5668\u306e\u9053\u5177\u306f\u3001\u30b7\u30ea\u30ab\u306e\u4e0d\u7d14\u7269\uff081000 $cm^{-1}$\u306b\u5438\u53ce\u30d4\u30fc\u30af\u3092\u5f15\u304d\u8d77\u3053\u3059\uff09\u3092\u6301\u3061\u8fbc\u3080\u53ef\u80fd\u6027\u304c\u3042\u308a\u307e\u3059\u3002<\/li>\n\n\n\n
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        \n
      1. \u30b5\u30f3\u30d7\u30eb\u6bd4\u7387\uff1a<\/strong>\n
          \n
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        • \u7814\u78e8\u6280\u8853\uff1a<\/strong> * \u8a66\u6599\u3092\u307e\u305a\u4e73\u9262\u306b\u5165\u308c\u3001\u7d30\u304b\u304f\u7c89\u7815\u3059\u308b\u3002\n
            \n
          • KBr\u30922\uff5e3\u56de\u306b\u5206\u3051\u3066\u52a0\u3048\u308b\u3002\u6df7\u5408\u7269\u304c\u5747\u8cea\u306b\u306a\u308a\u3001\u30c6\u30af\u30b9\u30c1\u30e3\u30fc\u304c\u5fae\u7c89\uff08\u7c92\u5b50\u30b5\u30a4\u30ba$le$ 2 $u$m\uff09\u306b\u306a\u308b\u307e\u3067\u3001\u7a4f\u3084\u304b\u306b\u5186\u3092\u63cf\u304f\u3088\u3046\u306b\u52d5\u304b\u3059\u3002<\/li>\n\n\n\n
          • \u6ce8\u610f\uff1a\u7814\u78e8\u3057\u3059\u304e\u308b\u3068\u8868\u9762\u7a4d\u304c\u5927\u304d\u304f\u306a\u308a\u3001\u904e\u5ea6\u306e\u5438\u6e7f\u306b\u3064\u306a\u304c\u308b\u3053\u3068\u304c\u3042\u308b\u3002<\/em><\/li>\n<\/ul>\n<\/li>\n<\/ol>\n\n\n\n
            \"FTIR\u7528KBr\u30da\u30ec\u30c3\u30c8\u306e\u8abf\u88fd\u6cd5\"<\/figure>\n\n\n\n
            \"FTIR\u7528KBr\u30da\u30ec\u30c3\u30c8\u306e\u8abf\u88fd\u6cd5\"<\/figure>\n\n\n\n

            \u30d5\u30a7\u30fc\u30baB\uff1a\u91d1\u578b\u306e\u7d44\u307f\u7acb\u3066\u3068\u30d7\u30ec\u30b9<\/h4>\n\n\n\n
              \n
            1. \u30ed\u30fc\u30c7\u30a3\u30f3\u30b0\uff1a<\/strong> \u30c0\u30a4\u30d9\u30fc\u30b9\u3092\u6c34\u5e73\u306a\u5834\u6240\u306b\u7f6e\u304f\u3002\u5c0f\u3055\u306a\u30d8\u30e9\u3092\u4f7f\u3063\u3066\u3001\u6df7\u5408\u7269\u3092\u30c0\u30a4\u30b9\u30ea\u30fc\u30d6\u306b\u79fb\u3059\u3002\u30d7\u30e9\u30f3\u30b8\u30e3\u30fc\u3092\u8efd\u304f\u53e9\u304f\u304b\u56de\u8ee2\u3055\u305b\u3001\u30d1\u30a6\u30c0\u30fc\u304c\u5747\u4e00\u306b\u306a\u308b\u3088\u3046\u306b\u3059\u308b\u3002<\/li>\n\n\n\n
            2. \u6383\u9664\u6a5f\u3092\u304b\u3051\u308b\uff08\u91cd\u8981\uff09\uff1a<\/strong> \u771f\u7a7a\u30dd\u30f3\u30d7\u3092\u30c0\u30a4\u306b\u63a5\u7d9a\u3059\u308b\u3002\u771f\u7a7a\u30dd\u30f3\u30d7\u3092\u30c0\u30a4\u306b\u63a5\u7d9a\u3059\u308b\u3002 1\uff5e2\u5206<\/strong>.\u3053\u308c\u306b\u3088\u308a\u3001\u9589\u3058\u8fbc\u3081\u3089\u308c\u305f\u7a7a\u6c17\u304c\u53d6\u308a\u9664\u304b\u308c\u3001\u5727\u529b\u4e0b\u3067\u306e\u5fae\u7d30\u306a\u6c17\u6ce1\u3084\u4e80\u88c2\u306e\u767a\u751f\u304c\u9632\u6b62\u3055\u308c\u308b\u3002<\/li>\n\n\n\n
            3. \u5727\u529b\u3092\u304b\u3051\u308b\uff1a<\/strong> \u6cb9\u5727\u30d7\u30ec\u30b9\u306b\u91d1\u578b\u3092\u5165\u308c\u308b\u3002\u3086\u3063\u304f\u308a\u3068\u5727\u529b\u3092\u4e0a\u3052\u3066 8\uff5e10\u30c8\u30f3<\/strong> (\u6a19\u6e9613mm\u30c0\u30a4\u7528\uff09\u3002<\/li>\n\n\n\n
            4. \u5727\u529b\u30e1\u30f3\u30c6\u30ca\u30f3\u30b9\uff1a<\/strong> \u306e\u9593\u3001\u5727\u529b\u3092\u7dad\u6301\u3059\u308b\u3002 60\uff5e90\u79d2<\/strong> KBr\u306e\u7d50\u6676\u304c\u878d\u5408\u3057\u3066\u4e00\u4f53\u5316\u3057\u305f\u900f\u660e\u306a\u683c\u5b50\u306b\u306a\u308b\u3088\u3046\u306b\u3002<\/li>\n\n\n\n
            5. \u30b3\u30f3\u30c8\u30ed\u30fc\u30eb\u30ea\u30ea\u30fc\u30b9\uff1a<\/strong> \u3086\u3063\u304f\u308a\u3068<\/strong> \u5727\u529b\u5f01\u3092\u958b\u653e\u3059\u308b\u3002\u6025\u6fc0\u306a\u6e1b\u5727\u306f\u5185\u90e8\u5fdc\u529b\u3092\u5f15\u304d\u8d77\u3053\u3057\u3001\"\u30af\u30e2\u306e\u5de3\u72b6 \"\u9aa8\u6298\u3084 \"\u767d\u6fc1\u3057\u305f \"\u690e\u9593\u677f\u306e\u539f\u56e0\u3068\u306a\u308b\u3002<\/li>\n<\/ol>\n\n\n\n
              \"\"<\/figure>\n\n\n\n
              \"\"<\/figure>\n\n\n\n

              \u54c1\u8cea\u691c\u67fb\uff08QC\uff09<\/h2>\n\n\n\n

              \u9069\u683c\u306aKBr\u30da\u30ec\u30c3\u30c8\u306f\u3001\u534a\u900f\u660e\u304b\u3089\u900f\u660e\uff08\u8584\u3044\u6c37\u306e\u3088\u3046\uff09\u3067\u3001\u8868\u9762\u304c\u6ed1\u3089\u304b\u3067\u3001\u7c92\u72b6\u3067\u306a\u3044\u3082\u306e\u3067\u306a\u3051\u308c\u3070\u306a\u3089\u306a\u3044\u3002<\/p>\n\n\n\n

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              \u66c7\u308a\u30d1\u30c3\u30c1<\/strong><\/td>\u3053\u3082\u3063\u305f\u7a7a\u6c17\u3084\u6e7f\u6c17<\/td>\u771f\u7a7a\u304c\u6a5f\u80fd\u3057\u3066\u3044\u308b\u3053\u3068\u3092\u78ba\u8a8d\u3059\u308b\u3002<\/td><\/tr>
              \u4e80\u88c2\uff0f\u9aa8\u6298<\/strong><\/td>\u6025\u6fc0\u306a\u6e1b\u5727\u307e\u305f\u306f\u4e0d\u5747\u7b49\u306a\u8ca0\u8377<\/td>\u5727\u529b\u3092\u3086\u3063\u304f\u308a\u89e3\u653e\u3059\u308b\u3002<\/td><\/tr>
              \u30e9\u30fc\u30b8\u30a6\u30a9\u30fc\u30bf\u30fc\u30d4\u30fc\u30af (3400 $cm^{-1}$)<\/strong><\/td>\u9ad8\u6e7f\u5ea6\u307e\u305f\u306f\u6e7f\u3063\u305f\u30b5\u30f3\u30d7\u30eb<\/td>IR\u30e9\u30f3\u30d7\u306e\u4e0b\u3067\u64cd\u4f5c\u3057\u3001\u8a66\u6599\u3092\u4e00\u5b9a\u91cd\u91cf\u307e\u3067\u4e7e\u71e5\u3055\u305b\u308b\u3002<\/td><\/tr><\/tbody><\/table><\/figure>\n\n\n\n

              \u5206\u6790\u5f8c\u306e\u30e1\u30f3\u30c6\u30ca\u30f3\u30b9<\/h2>\n\n\n\n
                \n
              • \u30d6\u30e9\u30f3\u30af\u30b3\u30f3\u30c8\u30ed\u30fc\u30eb\uff1a<\/strong> \u5927\u6c17\u4e2d\u306e$CO_2$\u3068\u6b8b\u7559$H_2O$\u306e\u5e72\u6e09\u3092\u5dee\u3057\u5f15\u304f\u305f\u3081\u306b\u3001\u30d0\u30c3\u30af\u30b0\u30e9\u30a6\u30f3\u30c9\u3068\u3057\u3066\u5e38\u306b \"Blank KBr Pellet\"\uff08\u30b5\u30f3\u30d7\u30eb\u306a\u3057\uff09\u3092\u5b9f\u884c\u3057\u307e\u3059\u3002<\/li>\n\n\n\n
              • \u91d1\u578b\u306e\u4fdd\u7ba1\uff1a<\/strong> KBr\u306f\u92fc\u9244\u306b\u5bfe\u3057\u3066\u8150\u98df\u6027\u304c\u9ad8\u3044\u3002\u4f7f\u7528\u5f8c\u3059\u3050\u306b\u3001\u3059\u3079\u3066\u306e\u91d1\u578b\u90e8\u54c1\u3092\u30a8\u30bf\u30ce\u30fc\u30eb\u3067\u6d17\u6d44\u3057\u3001\u4e7e\u71e5\u3055\u305b\u3066\u30c7\u30b7\u30b1\u30fc\u30bf\u30fc\u306b\u4fdd\u7ba1\u3059\u308b\u3002<\/li>\n<\/ul>\n\n\n\n

                \u4e3b\u306a\u6539\u5584\u70b9\u306e\u6982\u8981<\/h2>\n\n\n\n
                  \n
                • \u6a19\u6e96\u5316\u3055\u308c\u305f\u7528\u8a9e\uff1a<\/strong> \u696d\u754c\u6a19\u6e96\u7528\u8a9e\u306b\u5909\u66f4\uff08\u4f8b\uff1a\u300c\u30b9\u30da\u30af\u30c8\u30eb\u30b0\u30ec\u30fc\u30c9\u300d\u3001\u300c\u6cb9\u5727\u30d7\u30ec\u30b9\u300d\uff09\u3002<\/li>\n\n\n\n
                • \u30d0\u30ad\u30e5\u30fc\u30e0\u30fb\u30b9\u30c6\u30c3\u30d7<\/strong> \u30d0\u30ad\u30e5\u30fc\u30e0\u6bb5\u968e\u3092\u660e\u793a\u7684\u306b\u8ffd\u52a0\u3057\u305f\u3002\u3053\u308c\u306f\u3001\u5143\u306e\u30ef\u30fc\u30af\u30d5\u30ed\u30fc\u3067\u30da\u30ec\u30c3\u30c8\u304c\u5931\u6557\uff08\u767d\u6fc1\uff09\u3059\u308b\u6700\u3082\u4e00\u822c\u7684\u306a\u7406\u7531\u3067\u3042\u308b\u3002<\/li>\n\n\n\n
                • \u30c8\u30e9\u30d6\u30eb\u30b7\u30e5\u30fc\u30c6\u30a3\u30f3\u30b0\u8868\uff1a<\/strong> \u4e00\u822c\u7684\u306a\u30d7\u30ec\u30d1\u30ec\u30fc\u30b7\u30e7\u30f3\u30a8\u30e9\u30fc\u3092\u7279\u5b9a\u3057\u3001\u4fee\u6b63\u3059\u308b\u305f\u3081\u306e\u30af\u30a4\u30c3\u30af\u30ea\u30d5\u30a1\u30ec\u30f3\u30b9\u30ac\u30a4\u30c9\u3092\u63d0\u4f9b\u3002<\/li>\n\n\n\n
                • \u5727\u529b\u30d1\u30e9\u30e1\u30fc\u30bf\u30fc\uff1a<\/strong> \u4e00\u8cab\u3057\u305f\u7d50\u679c\u3092\u5f97\u308b\u305f\u3081\u306b\u3001\u30c8\u30f3\u6570\u3068\u4fdd\u6301\u6642\u9593\u3092\u660e\u78ba\u306b\u3057\u305f\u3002<\/li>\n<\/ul>\n\n\n\n
                  \"FTIR\u5206\u6790\"<\/figure>","protected":false},"excerpt":{"rendered":"

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