{"id":5991,"date":"2025-10-24T00:12:15","date_gmt":"2025-10-24T00:12:15","guid":{"rendered":"https:\/\/www.hcftir.com\/expert-guide-3-proven-methods-for-how-to-prepare-a-solid-sample-for-ir-analysis-article\/"},"modified":"2025-10-24T00:12:17","modified_gmt":"2025-10-24T00:12:17","slug":"expert-guide-3-proven-methods-for-how-to-prepare-a-solid-sample-for-ir-analysis","status":"publish","type":"post","link":"https:\/\/www.hcftir.com\/ja\/expert-guide-3-proven-methods-for-how-to-prepare-a-solid-sample-for-ir-analysis-article\/","title":{"rendered":"\u30a8\u30ad\u30b9\u30d1\u30fc\u30c8\u30ac\u30a4\u30c9IR\u5206\u6790\u7528\u56fa\u4f53\u8a66\u6599\u306e\u8abf\u88fd\u65b9\u6cd5\u306b\u95a2\u3059\u308b3\u3064\u306e\u5b9f\u8a3c\u6e08\u307f\u65b9\u6cd5"},"content":{"rendered":"<p><img loading=\"lazy\" decoding=\"async\" style=\"display: block; margin-left: auto; margin-right: auto;\" data-src=\"https:\/\/www.hcftir.com\/wp-content\/uploads\/2025\/09\/cuvette-1.webp\" alt=\"\" width=\"600\" height=\"600\" src=\"https:\/\/www.hcftir.com\/wp-content\/uploads\/2025\/09\/cuvette-1.webp\" data-ll-status=\"loaded\" class=\"entered loaded\"><\/p>\n<h2 id=\"abstract\">\u8981\u65e8<\/h2>\n<p>\u56fa\u4f53\u8a66\u6599\u304b\u3089\u9ad8\u54c1\u8cea\u306e\u30d5\u30fc\u30ea\u30a8\u5909\u63db\u8d64\u5916\u5206\u5149\uff08FTIR\uff09\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5f97\u308b\u306b\u306f\u3001\u305d\u306e\u8a66\u6599\u8abf\u88fd\u306b\u3069\u306e\u3088\u3046\u306a\u65b9\u6cd5\u3092\u9078\u629e\u3059\u308b\u304b\u304c\u57fa\u672c\u7684\u306b\u91cd\u8981\u3067\u3059\u3002\u56fa\u4f53\u8a66\u6599\u306e\u7269\u7406\u7684\u72b6\u614b\u306b\u306f\u3001\u5149\u306e\u6563\u4e71\u3084\u4e0d\u5747\u4e00\u6027\u3068\u3044\u3063\u305f\u56fa\u6709\u306e\u8ab2\u984c\u304c\u3042\u308a\u3001\u3053\u308c\u304c\u6c42\u3081\u308b\u632f\u52d5\u60c5\u5831\u3092\u4e0d\u660e\u77ad\u306b\u3057\u305f\u308a\u3001\u6b6a\u307e\u305b\u305f\u308a\u3057\u307e\u3059\u3002\u3053\u306e\u8a18\u4e8b\u3067\u306f\u3001IR\u5206\u6790\u306e\u305f\u3081\u306b\u56fa\u4f53\u8a66\u6599\u3092\u8abf\u88fd\u3059\u308b\u65b9\u6cd5\u306b\u3064\u3044\u3066\u3001\u81ed\u5316\u30ab\u30ea\u30a6\u30e0\uff08KBr\uff09\u30da\u30ec\u30c3\u30c8\u6cd5\u3001Nujol mull\u6cd5\u3001\u304a\u3088\u3073\u6e1b\u8870\u5168\u53cd\u5c04\uff08ATR\uff09\u5206\u5149\u6cd5\u306e3\u3064\u306e\u4e3b\u8981\u306a\u624b\u6cd5\u3092\u5305\u62ec\u7684\u306b\u691c\u8a0e\u3057\u307e\u3059\u3002\u5404\u624b\u6cd5\u306f\u3001\u305d\u306e\u57fa\u672c\u7684\u306a\u7269\u7406\u539f\u7406\u3001\u624b\u9806\u306e\u8907\u96d1\u3055\u3001\u3055\u307e\u3056\u307e\u306a\u30b5\u30f3\u30d7\u30eb\u30bf\u30a4\u30d7\u3078\u306e\u9069\u5408\u6027\u306b\u57fa\u3065\u3044\u3066\u8a55\u4fa1\u3055\u308c\u308b\u3002\u4e00\u822c\u7684\u306a\u624b\u9806\u306e\u8aa4\u308a\u3001\u30c8\u30e9\u30d6\u30eb\u30b7\u30e5\u30fc\u30c6\u30a3\u30f3\u30b0\u306e\u6226\u7565\u3001\u6f5c\u5728\u7684\u306a\u30b9\u30da\u30af\u30c8\u30eb\u306e\u30a2\u30fc\u30c1\u30d5\u30a1\u30af\u30c8\u306e\u89e3\u91c8\u306b\u3064\u3044\u3066\u3082\u89e6\u308c\u3066\u3044\u307e\u3059\u3002\u3053\u308c\u3089\u306e\u30e1\u30bd\u30c3\u30c9\u3092\u610f\u601d\u6c7a\u5b9a\u306e\u67a0\u7d44\u307f\u306e\u4e2d\u3067\u6587\u8108\u5316\u3059\u308b\u3053\u3068\u3067\u3001\u5206\u6790\u8005\u304c\u6700\u3082\u9069\u5207\u306a\u524d\u51e6\u7406\u30c6\u30af\u30cb\u30c3\u30af\u3092\u9078\u629e\u30fb\u5b9f\u884c\u3059\u308b\u305f\u3081\u306b\u5fc5\u8981\u306a\u5fae\u5999\u306a\u7406\u89e3\u3092\u8eab\u306b\u3064\u3051\u3001\u591a\u69d8\u306a\u56fa\u4f53\u7269\u8cea\u304b\u3089\u4fe1\u983c\u6027\u3001\u518d\u73fe\u6027\u3001\u5206\u6790\u7684\u4fa1\u5024\u306e\u3042\u308b\u30b9\u30da\u30af\u30c8\u30eb\u30c7\u30fc\u30bf\u3092\u78ba\u5b9f\u306b\u751f\u6210\u3067\u304d\u308b\u3088\u3046\u306b\u3059\u308b\u3053\u3068\u3092\u76ee\u7684\u3068\u3057\u3066\u3044\u308b\u3002<\/p>\n<h2 id=\"key-takeaways\">\u8981\u70b9<\/h2>\n<ul>\n<li>KBr\u30da\u30ec\u30c3\u30c8\u306e\u5834\u5408\u3001\u5149\u306e\u6563\u4e71\u3092\u6700\u5c0f\u9650\u306b\u6291\u3048\u308b\u305f\u3081\u3001\u8a66\u6599\u3092\u7d30\u304b\u304f\u5747\u4e00\u306a\u7c89\u672b\u306b\u3059\u308b\u3002<\/li>\n<li>\u5727\u529b\u3084\u6e7f\u6c17\u306b\u654f\u611f\u306a\u7d20\u6750\u306b\u306f\u3001\u30cc\u30b8\u30e7\u30fc\u30eb\u30fb\u30de\u30eb\u30fb\u30c6\u30af\u30cb\u30c3\u30af\u3092\u9078\u629e\u3059\u308b\u3002<\/li>\n<li>\u6e1b\u8870\u5168\u53cd\u5c04\uff08ATR\uff09\u3092\u4f7f\u7528\u3059\u308b\u3068\u3001\u6700\u5c0f\u9650\u306e\u6e96\u5099\u3067\u8fc5\u901f\u304b\u3064\u975e\u7834\u58ca\u7684\u306a\u8868\u9762\u5206\u6790\u304c\u53ef\u80fd\u3067\u3059\u3002<\/li>\n<li>IR\u5206\u6790\u7528\u306e\u56fa\u5f62\u30b5\u30f3\u30d7\u30eb\u306e\u6e96\u5099\u65b9\u6cd5\u3092\u30de\u30b9\u30bf\u30fc\u3059\u308b\u3053\u3068\u306f\u3001\u6b63\u78ba\u306a\u7d50\u679c\u3092\u5f97\u308b\u305f\u3081\u306e\u57fa\u790e\u3068\u306a\u308b\u3002<\/li>\n<li>\u6c5a\u67d3\u30d4\u30fc\u30af\u3092\u7279\u5b9a\u3059\u308b\u305f\u3081\u306b\u3001\u5869\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u307e\u305f\u306f\u30de\u30ea\u30f3\u30b0\u5264\u306e\u30d0\u30c3\u30af\u30b0\u30e9\u30a6\u30f3\u30c9\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5e38\u306b\u5b9f\u884c\u3059\u308b\u3002<\/li>\n<li>\u5f37\u529b\u306aATR\u30b7\u30b0\u30ca\u30eb\u3092\u5f97\u308b\u305f\u3081\u306b\u306f\u3001\u8a66\u6599\u3068\u7d50\u6676\u3092\u78ba\u5b9f\u306b\u5bc6\u7740\u3055\u305b\u308b\u3053\u3068\u3002<\/li>\n<li>\u524d\u51e6\u7406\u6cd5\u3092\u9078\u629e\u3059\u308b\u524d\u306b\u3001\u30b5\u30f3\u30d7\u30eb\u306e\u7279\u6027\u3068\u5206\u6790\u76ee\u6a19\u3092\u8003\u616e\u3057\u3066\u304f\u3060\u3055\u3044\u3002<\/li>\n<\/ul>\n<h2 id=\"table-of-contents\">\u76ee\u6b21<\/h2>\n<ul>\n<li><a href=\"#the-unseen-foundation-why-solid-sample-preparation-dictates-spectroscopic-success\">\u898b\u3048\u306a\u3044\u57fa\u76e4\uff1a\u78ba\u5b9f\u306a\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u304c\u5206\u5149\u5b66\u306e\u6210\u529f\u3092\u5de6\u53f3\u3059\u308b\u7406\u7531<\/a><\/li>\n<li><a href=\"#method-1-the-kbr-pellet-technique-a-classic-for-a-reason\">\u65b9\u6cd51\uff1aKBr\u30da\u30ec\u30c3\u30c8\u6cd5-\u53e4\u5178\u306b\u306f\u7406\u7531\u304c\u3042\u308b<\/a><\/li>\n<li><a href=\"#method-2-the-nujol-mull-an-alternative-for-delicate-samples\">\u65b9\u6cd52\uff1a\u30cc\u30b8\u30e7\u30eb\u30fb\u30de\u30eb-\u30c7\u30ea\u30b1\u30fc\u30c8\u306a\u30b5\u30f3\u30d7\u30eb\u306e\u305f\u3081\u306e\u4ee3\u66ff\u6cd5<\/a><\/li>\n<li><a href=\"#method-3-attenuated-total-reflectance-atr-the-modern-powerhouse\">\u65b9\u6cd53\uff1a\u6e1b\u8870\u5168\u53cd\u5c04\u7387\uff08ATR\uff09 - \u73fe\u4ee3\u306e\u30d1\u30ef\u30fc\u30cf\u30a6\u30b9<\/a><\/li>\n<li><a href=\"#choosing-the-right-path-a-decision-making-framework\">\u6b63\u3057\u3044\u9053\u3092\u9078\u3076\u610f\u601d\u6c7a\u5b9a\u306e\u30d5\u30ec\u30fc\u30e0\u30ef\u30fc\u30af<\/a><\/li>\n<li><a href=\"#frequently-asked-questions-faq\">\u3088\u304f\u3042\u308b\u8cea\u554f\uff08FAQ\uff09<\/a><\/li>\n<li><a href=\"#conclusion\">\u7d50\u8ad6<\/a><\/li>\n<li><a href=\"#references\">\u53c2\u8003\u6587\u732e<\/a><\/li>\n<\/ul>\n<h2 id=\"the-unseen-foundation-why-solid-sample-preparation-dictates-spectroscopic-success\">\u898b\u3048\u306a\u3044\u57fa\u76e4\uff1a\u78ba\u5b9f\u306a\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u304c\u5206\u5149\u5b66\u306e\u6210\u529f\u3092\u5de6\u53f3\u3059\u308b\u7406\u7531<\/h2>\n<p>\u30d5\u30fc\u30ea\u30a8\u5909\u63db\u8d64\u5916\u5206\u5149\u8a08\u3092\u4f7f\u3063\u3066\u7269\u8cea\u306e\u5206\u6790\u306b\u53d6\u308a\u304b\u304b\u308b\u3068\u3001\u307e\u308b\u3067\u73fe\u4ee3\u7684\u306a\u5360\u3044\u306e\u3088\u3046\u306a\u6c17\u5206\u306b\u306a\u308b\u3002\u7269\u8cea\u306b\u5149\u7dda\u3092\u7167\u5c04\u3057\u3001\u3069\u306e\u5468\u6ce2\u6570\u304c\u5438\u53ce\u3055\u308c\u308b\u304b\u3092\u89b3\u5bdf\u3059\u308b\u3053\u3068\u3067\u3001\u305d\u306e\u7269\u8cea\u306e\u539f\u5b50\u306e\u79d8\u5bc6\u306e\u914d\u7f6e\u3084\u7d50\u5408\u306e\u6027\u8cea\u3092\u5360\u3046\u306e\u3060\u3002\u3057\u304b\u3057\u3001\u3053\u306e\u5f37\u529b\u306a\u6280\u8853\u306f\u975e\u5e38\u306b\u7e4a\u7d30\u3067\u3042\u308b\u3002\u30b9\u30da\u30af\u30c8\u30eb\u304c\u8a9e\u308b\u30b9\u30c8\u30fc\u30ea\u30fc\u306e\u8cea\u306f\u3001\u88c5\u7f6e\u306e\u7cbe\u5de7\u3055\u3060\u3051\u3067\u6c7a\u307e\u308b\u308f\u3051\u3067\u306f\u306a\u304f\u3001\u8d64\u5916\u7dda\u30d3\u30fc\u30e0\u3092\u6d74\u3073\u308b\u524d\u306e\u30b5\u30f3\u30d7\u30eb\u306e\u6e96\u5099\u306b\u8cbb\u3084\u3055\u308c\u305f\u6ce8\u610f\u3068\u77e5\u6075\u306b\u652f\u914d\u3055\u308c\u308b\u3053\u3068\u304c\u591a\u3044\u3002\u6c17\u4f53\u3084\u6db2\u4f53\u306e\u5834\u5408\u3001\u3053\u308c\u306f\u3057\u3070\u3057\u3070\u7c21\u5358\u3067\u3042\u308b\u3002\u3057\u304b\u3057\u3001\u56fa\u4f53\u306e\u5834\u5408\u306f\u3088\u308a\u8907\u96d1\u3067\u3042\u308b\u3002\u56fa\u4f53\u306e\u72b6\u614b\u305d\u306e\u3082\u306e\u304c\u969c\u5bb3\u3068\u306a\u308a\u3001\u9bae\u660e\u306a\u306f\u305a\u306e\u30b9\u30da\u30af\u30c8\u30eb\u304c\u3001\u30ce\u30a4\u30ba\u306e\u591a\u3044\u3001\u89e3\u91c8\u4e0d\u80fd\u306a\u6df7\u4e71\u3057\u305f\u30b9\u30da\u30af\u30c8\u30eb\u306b\u306a\u308a\u304b\u306d\u306a\u3044\u306e\u3067\u3059\u3002\u3053\u308c\u3089\u306e\u8ab2\u984c\u3092\u7406\u89e3\u3059\u308b\u3053\u3068\u304c\u3001\u8ab2\u984c\u3092\u514b\u670d\u3059\u308b\u7b2c\u4e00\u6b69\u3068\u306a\u308b\u3002<\/p>\n<h3 id=\"what-is-infrared-spectroscopy-a-quick-refresher\">\u8d64\u5916\u5206\u5149\u6cd5\u3068\u306f\uff1f\u7c21\u5358\u306a\u5fa9\u7fd2<\/h3>\n<p>\u3069\u306e\u3088\u3046\u306b \"\u3092\u6398\u308a\u4e0b\u3052\u308b\u524d\u306b\u3001\"\u306a\u305c \"\u3092\u7c21\u5358\u306b\u518d\u78ba\u8a8d\u3057\u3066\u304a\u3053\u3046\u3002\u5206\u5b50\u7d50\u5408\u306f\u9759\u7684\u306a\u68d2\u3067\u306f\u306a\u3044\u3002\u5206\u5b50\u7d50\u5408\u306f\u9759\u7684\u306a\u68d2\u3067\u306f\u306a\u304f\u3001\u4f38\u3073\u305f\u308a\u3001\u66f2\u304c\u3063\u305f\u308a\u3001\u306d\u3058\u308c\u305f\u308a\u3057\u3066\u632f\u52d5\u3059\u308b\u30d0\u30cd\u306e\u3088\u3046\u306a\u3082\u306e\u3067\u3042\u308b\u3002\u7d50\u5408\u306e\u7a2e\u985e\uff08C-H\u5358\u7d50\u5408\u3001C=O\u4e8c\u91cd\u7d50\u5408\u3001O-H\u7d50\u5408\u306a\u3069\uff09\u3054\u3068\u306b\u3001\u7279\u5fb4\u7684\u306a\u5468\u6ce2\u6570\u3067\u632f\u52d5\u3059\u308b\u3002\u5206\u5b50\u306b\u8d64\u5916\u7dda\u3092\u7167\u5c04\u3059\u308b\u3068\u3001\u5206\u5b50\u306f\u30a8\u30cd\u30eb\u30ae\u30fc\u3092\u5438\u53ce\u3057\u3001\u305d\u306e\u7d50\u679c\u3001\u5206\u5b50\u304c\u6301\u3064\u56fa\u6709\u306e\u632f\u52d5\u5468\u6ce2\u6570\u3068\u4e00\u81f4\u3059\u308b\u5468\u6ce2\u6570\u306e\u5149\u3092\u5438\u53ce\u3059\u308b\u3002FTIR\u30b9\u30da\u30af\u30c8\u30ed\u30e1\u30fc\u30bf\u30fc\u306f\u3001\u3053\u306e\u5438\u53ce\u3092\u3055\u307e\u3056\u307e\u306a\u5468\u6ce2\u6570\u3067\u6e2c\u5b9a\u3057\u3001\u30b9\u30da\u30af\u30c8\u30eb\u3092\u751f\u6210\u3059\u308b\u3002\u3053\u306e\u30d5\u30a3\u30f3\u30ac\u30fc\u30d7\u30ea\u30f3\u30c8\u306b\u3088\u3063\u3066\u3001\u30b5\u30f3\u30d7\u30eb\u306b\u5b58\u5728\u3059\u308b\u5b98\u80fd\u57fa\u3092\u7279\u5b9a\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u3001\u5316\u5b66\u7269\u8cea\u306e\u540c\u5b9a\u3001\u54c1\u8cea\u7ba1\u7406\u3001\u7814\u7a76\u306b\u4e0d\u53ef\u6b20\u306a\u30c4\u30fc\u30eb\u3068\u306a\u308b\u3002<\/p>\n<h3 id=\"the-challenge-of-solids-scattering-thickness-and-concentration\">\u56fa\u4f53\u3078\u306e\u6311\u6226\uff1a\u6563\u4e71\u3001\u539a\u307f\u3001\u6fc3\u5ea6<\/h3>\n<p>\u66c7\u308a\u30ac\u30e9\u30b9\u8d8a\u3057\u306b\u672c\u3092\u8aad\u3082\u3046\u3068\u3057\u3066\u3044\u308b\u3068\u3053\u308d\u3092\u60f3\u50cf\u3057\u3066\u307f\u3066\u307b\u3057\u3044\u3002\u305d\u3053\u306b\u6587\u5b57\u304c\u3042\u308b\u3053\u3068\u306f\u308f\u304b\u308b\u304c\u3001\u5149\u304c\u591a\u65b9\u5411\u306b\u6563\u4e71\u3057\u3001\u6587\u5b57\u304c\u5224\u8aad\u3067\u304d\u306a\u3044\u307c\u3084\u3051\u65b9\u3092\u3057\u3066\u3044\u308b\u3002\u3053\u308c\u304c\u3001\u56fa\u4f53\u8a66\u6599\u3092\u76f4\u63a5\u5206\u6790\u3059\u308b\u5834\u5408\u306e\u4e3b\u306a\u96e3\u70b9\u3067\u3042\u308b\u3002\u7d50\u6676\u3084\u7c89\u672b\u72b6\u306e\u56fa\u4f53\u306f\u7121\u6570\u306e\u5c0f\u3055\u306a\u7c92\u5b50\u304b\u3089\u69cb\u6210\u3055\u308c\u3066\u304a\u308a\u3001\u305d\u308c\u305e\u308c\u304c\u8d64\u5916\u7dda\u30d3\u30fc\u30e0\u3092\u53cd\u5c04\u3057\u305f\u308a\u5c48\u6298\u3057\u305f\u308a\u3059\u308b\u8868\u9762\u3092\u6301\u3064\u3002\u30df\u30fc\u6563\u4e71\u3068\u3057\u3066\u77e5\u3089\u308c\u308b\u3053\u306e\u73fe\u8c61\u306f\u3001\u7c92\u5b50\u5f84\u304c\u8d64\u5916\u5149\u306e\u6ce2\u9577\u306b\u8fd1\u3044\u5834\u5408\u306b\u7279\u306b\u554f\u984c\u3068\u306a\u308a\u307e\u3059\u3002\u5149\u306f\u6e2c\u5b9a\u3059\u308b\u30b5\u30f3\u30d7\u30eb\u3092\u901a\u904e\u3059\u308b\u306e\u3067\u306f\u306a\u304f\u3001\u691c\u51fa\u5668\u304b\u3089\u9060\u3056\u304b\u308b\u65b9\u5411\u306b\u504f\u5411\u3055\u308c\u308b\u305f\u3081\u3001\u30d9\u30fc\u30b9\u30e9\u30a4\u30f3\u304c\u50be\u304d\u3001\u6b6a\u3093\u3067\u4fe1\u53f7\u5f37\u5ea6\u304c\u4f4e\u4e0b\u3057\u3001\u5fae\u5999\u306a\u5438\u53ce\u5e2f\u304c\u30de\u30b9\u30af\u3055\u308c\u308b\u53ef\u80fd\u6027\u304c\u3042\u308a\u307e\u3059\u3002<\/p>\n<p>\u3055\u3089\u306b\u3001\u5438\u5149\u5ea6\u3068\u6fc3\u5ea6\u306e\u95a2\u4fc2\u3092\u652f\u914d\u3059\u308bBeer&#039;s\u306e\u6cd5\u5247\u306f\u3001\u5747\u4e00\u306a\u7d4c\u8def\u9577\u3092\u524d\u63d0\u3068\u3057\u3066\u3044\u308b\u3002\u56fa\u4f53\u3067\u306f\u3001\u3069\u3046\u3084\u3063\u3066\u3053\u308c\u3092\u30b3\u30f3\u30c8\u30ed\u30fc\u30eb\u3067\u304d\u308b\u306e\u3060\u308d\u3046\u304b\uff1f\u539a\u3059\u304e\u308b\u7269\u8cea\u306e\u584a\u306f\u3001\u3059\u3079\u3066\u306e\u5149\u3092\u5438\u53ce\u3057\u3066\u3057\u307e\u3044\u3001\u4f7f\u7528\u53ef\u80fd\u306a\u60c5\u5831\u306e\u306a\u3044\u300c\u30d6\u30e9\u30c3\u30af\u30a2\u30a6\u30c8\u300d\u30b9\u30da\u30af\u30c8\u30eb\u3068\u306a\u308b\u3002\u8584\u3059\u304e\u308b\u30b5\u30f3\u30d7\u30eb\u306f\u3001\u691c\u51fa\u53ef\u80fd\u306a\u30b7\u30b0\u30ca\u30eb\u3092\u751f\u6210\u3059\u308b\u306e\u306b\u5341\u5206\u306a\u5206\u5b50\u3092\u30d3\u30fc\u30e0\u306e\u7d4c\u8def\u306b\u542b\u307e\u306a\u3044\u304b\u3082\u3057\u308c\u306a\u3044\u3002\u305d\u3053\u3067\u8ab2\u984c\u3068\u306a\u308b\u306e\u306f\u3001\u56fa\u4f53\u8a66\u6599\u3092\u3001\u30b7\u30b0\u30ca\u30eb\u3092\u751f\u6210\u3059\u308b\u306e\u306b\u5341\u5206\u306a\u6fc3\u5ea6\u3068\u3001\u904e\u5270\u306a\u6563\u4e71\u306a\u3057\u306b\u5149\u3092\u901a\u904e\u3055\u305b\u308b\u306e\u306b\u5341\u5206\u306a\u900f\u660e\u5ea6\u3092\u4f75\u305b\u6301\u3064\u5f62\u3067\u5206\u5149\u8a08\u306b\u63d0\u793a\u3059\u308b\u3053\u3068\u3067\u3042\u308b\u3002\u3053\u308c\u306f\u3001\u56fa\u4f53\u8a66\u6599\u8abf\u88fd\u306e\u3042\u3089\u3086\u308b\u65b9\u6cd5\u304c\u89e3\u6c7a\u3057\u3088\u3046\u3068\u3059\u308b\u4e2d\u5fc3\u7684\u306a\u554f\u984c\u3067\u3042\u308b\u3002<\/p>\n<h3 id=\"the-goal-a-homogeneous-transparent-medium\">\u76ee\u6a19\uff1a\u5747\u8cea\u3067\u900f\u660e\u306a\u5a92\u4f53<\/h3>\n<p>\u3042\u3089\u3086\u308b\u56fa\u4f53\u30b5\u30f3\u30d7\u30ea\u30f3\u30b0\u6280\u8853\u306e\u5305\u62ec\u7684\u306a\u76ee\u6a19\u306f\u3001\u30b5\u30f3\u30d7\u30eb\u304c\u5747\u4e00\u306b\u5206\u6563\u3057\u3001\u7c92\u5b50\u5f84\u304c\u4f7f\u7528\u3055\u308c\u308b\u8d64\u5916\u7dda\u306e\u6ce2\u9577\uff08\u901a\u5e382.5\uff5e25 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id=\"method-1-the-kbr-pellet-technique-a-classic-for-a-reason\">\u65b9\u6cd51\uff1aKBr\u30da\u30ec\u30c3\u30c8\u6cd5-\u53e4\u5178\u306b\u306f\u7406\u7531\u304c\u3042\u308b<\/h2>\n<p>\u81ed\u5316\u30ab\u30ea\u30a6\u30e0\uff08KBr\uff09\u30da\u30ec\u30c3\u30c8\u6cd5\u306f\u3001\u8d64\u5916\u5206\u5149\u6cd5\u306b\u304a\u3051\u308b\u56fa\u4f53\u8a66\u6599\u5206\u6790\u306e\u6700\u3082\u4f1d\u7d71\u7684\u306a\u624b\u6cd5\u3067\u3042\u308d\u3046\u3002\u30b3\u30f3\u30bb\u30d7\u30c8\u306f\u7f8e\u3057\u304f\u30b7\u30f3\u30d7\u30eb\u3060\u304c\u3001\u5b9f\u884c\u306b\u306f\u3042\u308b\u7a2e\u306e\u6280\u8853\u3068\u5fcd\u8010\u304c\u8981\u6c42\u3055\u308c\u308b\u65b9\u6cd5\u3067\u3042\u308b\u3002\u76ee\u7684\u306f\u3001\u5c0f\u3055\u306a\u7a93\u306e\u3088\u3046\u306a\u900f\u660e\u306a\u5186\u76e4\u3092\u4f5c\u308a\u3001\u305d\u306e\u4e2d\u306b\u76ee\u7684\u306e\u56fa\u4f53\u3092\u7d30\u304b\u304f\u5206\u6563\u3055\u305b\u308b\u3053\u3068\u3067\u3042\u308b\u3002\u3053\u306e \"\u7a93 \"\u3092\u5206\u5149\u8a08\u306e\u30b5\u30f3\u30d7\u30eb\u30db\u30eb\u30c0\u30fc\u306b\u76f4\u63a5\u30bb\u30c3\u30c8\u3057\u3001\u900f\u904e\u5206\u6790\u3092\u884c\u3046\u3002\u3053\u306e\u65b9\u6cd5\u306e\u6210\u529f\u306f\u3001\u4e0d\u5747\u4e00\u306a\u7c89\u672b\u3092\u64ec\u4f3c\u7684\u306a\u30ac\u30e9\u30b9\u72b6\u306e\u56fa\u4f53\u6eb6\u6db2\u306b\u5909\u3048\u308b\u3053\u3068\u306b\u304b\u304b\u3063\u3066\u3044\u308b\u3002<\/p>\n<h3 id=\"the-underlying-principle-creating-a-glass-window\">\u57fa\u672c\u539f\u5247\u30ac\u30e9\u30b9 \"\u306e\u7a93\u3092\u4f5c\u308b<\/h3>\n<p>\u306a\u305cKBr\u306a\u306e\u304b\uff1f\u81ed\u5316\u30ab\u30ea\u30a6\u30e0\u306e\u9078\u629e\u306f\u610f\u56f3\u7684\u304b\u3064\u72ec\u5275\u7684\u3067\u3042\u308b\u3002KBr\u306e\u3088\u3046\u306a\u30cf\u30ed\u30b2\u30f3\u5316\u30a2\u30eb\u30ab\u30ea\uff08KCl\u3084CsI\u3082\u540c\u69d8\uff09\u306b\u306f\u3001\u7279\u6b8a\u3067\u975e\u5e38\u306b\u6709\u7528\u306a\u7279\u6027\u304c\u3042\u308b\u3002\u305d\u308c\u306f\u3001\u4e2d\u8d64\u5916\u9818\u57df\uff084000\uff5e400cm-\u00b9\uff09\u5168\u4f53\u306b\u308f\u305f\u3063\u3066\u8d64\u5916\u7dda\u306b\u5bfe\u3057\u3066\u900f\u660e\u3067\u3042\u308b\u3053\u3068\u3060\u3002\u3053\u306e\u9818\u57df\u306b\u306f\u5206\u5b50\u632f\u52d5\u304c\u306a\u3044\u305f\u3081\u3001\u30b9\u30da\u30af\u30c8\u30eb\u306b\u5e72\u6e09\u3059\u308b\u5438\u53ce\u5e2f\u304c\u306a\u3044\u3002\u7b2c\u4e8c\u306b\u3001\u9ad8\u5727\u4e0b\u3067\u306fKBr\u306f\u300c\u6d41\u52d5\u300d\u3057\u3001\u53ef\u5851\u6027\u3092\u6301\u3064\u3002\u3053\u308c\u306b\u3088\u308a\u3001\u5fae\u7c89\u7815\u3055\u308c\u305f\u8a66\u6599\u7c92\u5b50\u3092\u5305\u307f\u8fbc\u3080\u56fa\u4f53\u306e\u900f\u660e\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u3092\u5f62\u6210\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002<\/p>\n<p>\u305d\u306e\u539f\u7406\u306f\u3001\u3054\u304f\u5c11\u91cf\u306e\u8a66\u6599\uff08\u901a\u5e381\uff5e2mg\uff09\u3092\u3001\u9aa8\u307e\u3067\u4e7e\u71e5\u3057\u305f\u5206\u5149\u5b66\u30b0\u30ec\u30fc\u30c9\u306eKBr\u7c89\u672b\uff08\u7d04100\uff5e200mg\uff09\u3068\u6df7\u5408\u3059\u308b\u3002\u3053\u306e\u6df7\u5408\u7269\u3092\u5fb9\u5e95\u7684\u306b\u7c89\u7815\u3057\u3001\u8a66\u6599\u306e\u7c92\u5f84\u30922\u03bcm\u4ee5\u4e0b\u306b\u3059\u308b\u3002\u3053\u306e\u6df7\u5408\u7269\u3092\u91d1\u578b\u306b\u5165\u308c\u3001\u975e\u5e38\u306b\u9ad8\u3044\u5727\u529b\uff08\u7d048\uff5e10\u30c8\u30f3\uff09\u3092\u304b\u3051\u308b\u3068\u3001KBr\u304c\u878d\u89e3\u3057\u3066\u900f\u660e\u306a\u5186\u76e4\u72b6\u306b\u306a\u308a\u3001\u8a66\u6599\u7c92\u5b50\u304c\u305d\u306e\u4e2d\u306b\u9589\u3058\u8fbc\u3081\u3089\u308c\u308b\u3002\u51fa\u6765\u4e0a\u304c\u3063\u305f\u30da\u30ec\u30c3\u30c8\u306f\u5149\u5b66\u7684\u306b\u900f\u660e\u3067\u3001\u8d64\u5916\u7dda\u30d3\u30fc\u30e0\u304c\u6700\u5c0f\u9650\u306e\u6563\u4e71\u3067\u901a\u904e\u3067\u304d\u308b\u3002<\/p>\n<h3 id=\"step-by-step-guide-to-preparing-a-kbr-pellet\">KBr\u30da\u30ec\u30c3\u30c8\u306e\u4f5c\u6210\u30b9\u30c6\u30c3\u30d7\u30ac\u30a4\u30c9<\/h3>\n<p>KBr\u6cd5\u306b\u3088\u308bIR\u5206\u6790\u306e\u305f\u3081\u306e\u56fa\u4f53\u30b5\u30f3\u30d7\u30eb\u306e\u8abf\u88fd\u65b9\u6cd5\u3092\u30de\u30b9\u30bf\u30fc\u3059\u308b\u3053\u3068\u306f\u3001\u591a\u304f\u306e\u5316\u5b66\u8005\u306b\u3068\u3063\u3066\u901a\u904e\u5100\u793c\u3067\u3042\u308b\u3002\u3042\u3089\u3086\u308b\u6bb5\u968e\u3067\u7d30\u90e8\u3078\u306e\u6ce8\u610f\u304c\u5fc5\u8981\u3067\u3042\u308b\u3002<\/p>\n<h4 id=\"grinding-the-art-of-pulverization\">\u7c89\u7815\uff1a\u7c89\u7815\u306e\u6280\u8853<\/h4>\n<p>\u3053\u308c\u306f\u9593\u9055\u3044\u306a\u304f\u6700\u3082\u91cd\u8981\u306a\u30b9\u30c6\u30c3\u30d7\u3067\u3042\u308b\u3002\u305d\u306e\u76ee\u7684\u306f\u3001\u6563\u4e71\u3092\u9632\u3050\u305f\u3081\u306b\u3001\u4f7f\u7528\u3059\u308b\u8d64\u5916\u5149\u306e\u6700\u77ed\u6ce2\u9577\u3088\u308a\u3082\u5c0f\u3055\u3044\u30b5\u30a4\u30ba\u307e\u3067\u8a66\u6599\u7c92\u5b50\u3092\u5c0f\u3055\u304f\u3059\u308b\u3053\u3068\u3067\u3042\u308b\u3002<\/p>\n<ol>\n<li><strong>\u4e7e\u71e5\u3055\u305b\u308b\uff1a<\/strong> \u5206\u5149\u5b66\u30b0\u30ec\u30fc\u30c9\u306eKBr\u7c89\u672b\u304b\u3089\u59cb\u3081\u308b\u3002\u4e7e\u71e5\u3057\u305f\u300dKBr\u3067\u3082\u5438\u6e7f\u6027\u304c\u3042\u308a\u3001\u5927\u6c17\u4e2d\u306e\u6c34\u5206\u3092\u5438\u53ce\u3059\u308b\u3002KBr\u3092110\u2103\u306e\u30aa\u30fc\u30d6\u30f3\u3067\u6570\u6642\u9593\u4e7e\u71e5\u3055\u305b\u3001\u4f7f\u7528\u3059\u308b\u307e\u3067\u30c7\u30b7\u30b1\u30fc\u30bf\u30fc\u3067\u4fdd\u7ba1\u3059\u308b\u306e\u304c\u30d9\u30b9\u30c8\u3067\u3042\u308b\u3002<\/li>\n<li><strong>\u8a08\u6e2c\u3059\u308b\uff1a<\/strong> \u7d041\uff5e2mg\u306e\u56fa\u4f53\u8a66\u6599\u3068100\uff5e200mg\u306e\u4e7e\u71e5KBr\u3092\u79e4\u91cf\u3059\u308b\u3002 \u7d041:100\u306e\u5272\u5408\u304c\u51fa\u767a\u70b9\u3068\u3057\u3066\u826f\u3044\u3002<\/li>\n<li><strong>\u7814\u78e8\uff1a<\/strong> \u3053\u308c\u306b\u6700\u9069\u306a\u9053\u5177\u306f\u3001\u30e1\u30ce\u30a6\u306e\u4e73\u9262\u3068\u4e73\u68d2\u3060\u3002\u30e1\u30ce\u30a6\u306f\u975e\u5e38\u306b\u786c\u304f\u3001\u591a\u5b54\u8cea\u3067\u306a\u3044\u305f\u3081\u3001\u6c5a\u67d3\u3092\u6700\u5c0f\u9650\u306b\u6291\u3048\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002\u4e73\u9262\u306bKBr\u3068\u8a66\u6599\u3092\u5165\u308c\u308b\u3002\u512a\u3057\u304f\u3001\u3057\u304b\u3057\u3057\u3063\u304b\u308a\u3068\u5186\u3092\u63cf\u304f\u3088\u3046\u306b\u3059\u308a\u6df7\u305c\u308b\u3002\u305f\u3060\u6df7\u305c\u308b\u306e\u3067\u306f\u306a\u304f\u3001\u305b\u3093\u65ad\u529b\u3092\u52a0\u3048\u3066\u7c92\u5b50\u3092\u7815\u304f\u3002\u6df7\u5408\u7269\u306f\u7d30\u304b\u304f\u3001\u5c0f\u9ea6\u7c89\u306e\u3088\u3046\u306a\u56fa\u3055\u306b\u306a\u308b\u306f\u305a\u3067\u3059\u3002\u4e0a\u624b\u306b\u633d\u304f\u306b\u306f\u30013\uff5e5\u5206\u7d9a\u3051\u308b\u5fc5\u8981\u304c\u3042\u308b\u3002\u7406\u60f3\u7684\u306a\u30c6\u30af\u30b9\u30c1\u30e3\u30fc\u3092 \"\u30d5\u30ef\u30d5\u30ef \"\u3068\u8868\u73fe\u3059\u308b\u30a2\u30ca\u30ea\u30b9\u30c8\u3082\u3044\u308b\u3002<\/li>\n<\/ol>\n<h4 id=\"mixing-the-pursuit-of-homogeneity\">\u30df\u30ad\u30b7\u30f3\u30b0\u5747\u8cea\u6027\u306e\u8ffd\u6c42<\/h4>\n<p>\u3059\u308a\u6f70\u3059\u3068\u540c\u6642\u306b\u3001\u6df7\u5408\u3082\u884c\u3046\u3002\u8a66\u6599\u304cKBr\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u5168\u4f53\u306b\u5747\u7b49\u306b\u884c\u304d\u6e21\u308b\u3088\u3046\u306b\u3001\u4e73\u9262\u306e\u5074\u9762\u304b\u3089\u4e2d\u5fc3\u90e8\u3078\u5b9a\u671f\u7684\u306b\u8a66\u6599\u3092\u304b\u304d\u51fa\u3059\u3088\u3046\u306b\u3059\u308b\u3002\u6fc3\u7e2e\u3055\u308c\u305f\u8a66\u6599\u306e\u584a\u304c\u3042\u308b\u3068\u3001\u30d4\u30fc\u30af\u304c\u6b6a\u307f\u3001\u8cea\u306e\u60aa\u3044\u30b9\u30da\u30af\u30c8\u30eb\u306b\u306a\u308a\u307e\u3059\u3002<\/p>\n<h4 id=\"pressing-forging-the-pellet\">\u30d7\u30ec\u30b9\u30da\u30ec\u30c3\u30c8\u306e\u935b\u9020<\/h4>\n<p>\u3053\u306e\u30b9\u30c6\u30c3\u30d7\u306b\u306f\u3001\u5c02\u7528\u306eKBr\u30da\u30ec\u30c3\u30c8\u30c0\u30a4\u3068\u6cb9\u5727\u30d7\u30ec\u30b9\u304c\u5fc5\u8981\u3067\u3042\u308b\u3002\u3053\u308c\u3089\u306f\u9811\u4e08\u306a\u8a2d\u5099\u3067\u3042\u308a\u3001\u53d6\u308a\u6271\u3044\u306b\u306f\u6ce8\u610f\u304c\u5fc5\u8981\u3067\u3042\u308b\u3002<\/p>\n<ol>\n<li><strong>\u7d44\u307f\u7acb\u3066\uff1a<\/strong> \u30e1\u30fc\u30ab\u30fc\u306e\u6307\u793a\u306b\u5f93\u3063\u3066\u91d1\u578b\u3092\u7d44\u307f\u7acb\u3066\u307e\u3059\u3002\u3053\u306e\u4f5c\u696d\u3067\u306f\u901a\u5e38\u3001\u7814\u78e8\u3057\u305f\u4e0b\u30a2\u30f3\u30d3\u30eb\u3092\u672c\u4f53\u306b\u30bb\u30c3\u30c8\u3057\u307e\u3059\u3002<\/li>\n<li><strong>\u30ed\u30fc\u30c7\u30a3\u30f3\u30b0\uff1a<\/strong> \u7c89\u7815\u3057\u305fKBr\u3068\u8a66\u6599\u306e\u6df7\u5408\u7269\u306e\u4e00\u90e8\u3092\u3001\u539a\u3055\u7d041\uff5e2 mm\u306e\u30da\u30ec\u30c3\u30c8\u306b\u306a\u308b\u3088\u3046\u306b\u614e\u91cd\u306b\u30c0\u30a4\u30d0\u30ec\u30eb\u306b\u79fb\u3059\u3002\u30c0\u30a4\u3092\u8efd\u304f\u305f\u305f\u3044\u3066\u7c89\u672b\u3092\u5747\u3059\u3002<\/li>\n<li><strong>\u5727\u529b\u3092\u304b\u3051\u308b\uff1a<\/strong> \u4e0a\u90e8\u30a2\u30f3\u30d3\u30eb\u3092\u30d0\u30ec\u30eb\u306b\u5165\u308c\u3001\u30a2\u30bb\u30f3\u30d6\u30ea\u5168\u4f53\u3092\u6cb9\u5727\u30d7\u30ec\u30b9\u306b\u79fb\u3057\u307e\u3059\u3002\u63a8\u5968\u5024\uff08\u901a\u5e388\uff5e10\u30c8\u30f3\uff08\uff5e10,000psi\uff09\uff09\u306b\u9054\u3059\u308b\u307e\u3067\u3001\u3086\u3063\u304f\u308a\u3068\u5727\u529b\u3092\u304b\u3051\u307e\u3059\u3002\u3053\u306e\u5727\u529b\u30921\uff5e2\u5206\u9593\u4fdd\u6301\u3059\u308b\u3002\u3053\u308c\u306b\u3088\u308a\u3001KBr\u304c\u30b3\u30fc\u30eb\u30c9\u30d5\u30ed\u30fc\u3057\u3001\u900f\u660e\u306a\u30c7\u30a3\u30b9\u30af\u304c\u5f62\u6210\u3055\u308c\u308b\u3002<\/li>\n<li><strong>\u5727\u529b\u3092\u89e3\u653e\u3059\u308b\uff1a<\/strong> \u91cd\u8981\u306a\u306e\u306f\u3001\u3086\u3063\u304f\u308a\u3068\u5727\u529b\u3092\u89e3\u653e\u3059\u308b\u3053\u3068\u3067\u3059\u3002\u5727\u529b\u304c\u65e9\u3059\u304e\u308b\u3068\u3001\u65b0\u3057\u304f\u5f62\u6210\u3055\u308c\u305f\u30da\u30ec\u30c3\u30c8\u306b\u3072\u3073\u304c\u5165\u3063\u305f\u308a\u3001\u7815\u3051\u305f\u308a\u3059\u308b\u3053\u3068\u304c\u3042\u308a\u307e\u3059\u3002<\/li>\n<\/ol>\n<h4 id=\"inspecting-judging-the-quality\">\u691c\u67fb\u3059\u308b\u54c1\u8cea\u306e\u5224\u5b9a<\/h4>\n<p>\u30c0\u30a4\u304b\u3089\u30da\u30ec\u30c3\u30c8\u3092\u6ce8\u610f\u6df1\u304f\u53d6\u308a\u51fa\u3057\u305f\u3089\u3001\u5149\u306b\u304b\u3056\u3059\u3002\u826f\u3044\u30da\u30ec\u30c3\u30c8\u306f\u3001\u30b9\u30e2\u30fc\u30af\u30ac\u30e9\u30b9\u306e\u3088\u3046\u306b\u5747\u4e00\u306a\u534a\u900f\u660e\u304b\u900f\u660e\u3067\u3042\u308b\u3079\u304d\u3067\u3059\u3002\u4e0d\u900f\u660e\u3067\u3042\u3063\u305f\u308a\u3001\u6fc1\u3063\u3066\u3044\u305f\u308a\u3001\u3072\u3073\u5272\u308c\u3084 \"\u30d5\u30a3\u30c3\u30b7\u30e5\u30a2\u30a4\"\uff08\u633d\u304d\u6b8b\u3057\u306e\u7c92\u5b50\uff09\u304c\u898b\u3048\u305f\u308a\u3057\u3066\u306f\u306a\u3089\u306a\u3044\u3002<\/p>\n<h3 id=\"common-pitfalls-and-how-to-troubleshoot-them\">\u3088\u304f\u3042\u308b\u843d\u3068\u3057\u7a74\u3068\u30c8\u30e9\u30d6\u30eb\u30b7\u30e5\u30fc\u30c6\u30a3\u30f3\u30b0\u65b9\u6cd5<\/h3>\n<p>\u614e\u91cd\u306a\u6280\u8853\u3092\u6301\u3063\u3066\u3057\u3066\u3082\u3001\u554f\u984c\u304c\u751f\u3058\u308b\u3053\u3068\u306f\u3042\u308b\u3002\u305d\u306e\u539f\u56e0\u3092\u7406\u89e3\u3059\u308b\u3053\u3068\u304c\u3001\u554f\u984c\u3092\u89e3\u6c7a\u3059\u308b\u9375\u3068\u306a\u308b\u3002<\/p>\n<ul>\n<li><strong>\u767d\u6fc1\u307e\u305f\u306f\u4e0d\u900f\u660e\u306a\u30da\u30ec\u30c3\u30c8\uff1a<\/strong> \u3053\u308c\u306f\u6700\u3082\u4e00\u822c\u7684\u306a\u554f\u984c\u3067\u3042\u308b\u3002\u4e3b\u306a\u539f\u56e0\u306f\u7814\u78e8\u4e0d\u8db3\u3002\u5927\u304d\u306a\u7c92\u5b50\u304c\u307e\u3060\u5149\u3092\u6563\u4e71\u3055\u305b\u3066\u3044\u308b\u306e\u3060\u3002\u89e3\u6c7a\u7b56\u306f\u3001\u7c89\u7815\u306e\u6bb5\u968e\u306b\u623b\u308b\u3053\u3068\u3060\u3002\u3082\u3046\u4e00\u3064\u306e\u5927\u304d\u306a\u539f\u56e0\u306f\u6c34\u5206\u3067\u3042\u308b\u3002KBr\u306b\u5438\u53ce\u3055\u308c\u305f\u6c34\u5206\u306f\u4e0d\u900f\u660e\u5316\u3092\u5f15\u304d\u8d77\u3053\u3057\u3001\u3055\u3089\u306b\u60aa\u3044\u3053\u3068\u306b\u30013400 cm-\u00b9\uff08O-H\u30b9\u30c8\u30ec\u30c3\u30c1\uff09\u4ed8\u8fd1\u306e\u975e\u5e38\u306b\u30d6\u30ed\u30fc\u30c9\u3067\u5f37\u3044\u5438\u53ce\u5e2f\u3068\u30011640 cm-\u00b9\uff08H-O-H\u30d9\u30f3\u30c9\uff09\u4ed8\u8fd1\u306e\u5f31\u3044\u5438\u53ce\u5e2f\u304c\u751f\u3058\u3001\u91cd\u8981\u306a\u30b5\u30f3\u30d7\u30eb\u306e\u30d4\u30fc\u30af\u304c\u4e0d\u660e\u77ad\u306b\u306a\u308a\u307e\u3059\u3002\u5e38\u306b\u5341\u5206\u306b\u4e7e\u71e5\u3055\u305b\u305fKBr\u3092\u4f7f\u7528\u3057\u3001\u7d20\u65e9\u304f\u4f5c\u696d\u3059\u308b\u3002<\/li>\n<li><strong>\u3072\u3073\u5272\u308c\u305f\u308a\u3001\u3082\u308d\u304f\u306a\u3063\u305f\u30da\u30ec\u30c3\u30c8\uff1a<\/strong> \u3053\u308c\u306f\u3001\u5727\u529b\u306e\u89e3\u653e\u304c\u65e9\u3059\u304e\u308b\u305f\u3081\u306b\u8d77\u3053\u308a\u307e\u3059\u3002\u52a0\u5727\u524d\u306b\u30c0\u30a4\u3092\u8efd\u304f\u305f\u305f\u304f\u3068\u52b9\u679c\u7684\u3067\u3059\u3002\u307e\u305f\u3001\u8a66\u6599\u304c\u591a\u3059\u304e\u308b\u3068\u30da\u30ec\u30c3\u30c8\u304c\u3082\u308d\u304f\u306a\u308a\u307e\u3059\u3002<\/li>\n<li><strong>\u5e72\u6e09\u306e\u30d4\u30fc\u30af\uff1a<\/strong> \u4e0a\u8a18\u306e\u6c34\u306e\u30d4\u30fc\u30af\u306e\u4ed6\u306b\u3001\u4e88\u671f\u305b\u306c\u5438\u53ce\u304c\u898b\u3089\u308c\u308b\u304b\u3082\u3057\u308c\u306a\u3044\u3002\u67d4\u3089\u304b\u3044\u4e73\u9262\u306e\u6750\u6599\u3067\u7a4d\u6975\u7684\u306b\u633d\u304d\u3059\u304e\u308b\u3068\u3001\u6c5a\u67d3\u7269\u8cea\u304c\u6df7\u5165\u3059\u308b\u53ef\u80fd\u6027\u304c\u3042\u308a\u307e\u3059\u3002\u4e73\u9262\u3068\u4e73\u68d2\u306f\u3001\u8a66\u6599\u3068\u8a66\u6599\u306e\u9593\u306b\u5fc5\u305a\u5165\u5ff5\u306b\u6d17\u6d44\u3057\u3066\u304f\u3060\u3055\u3044\u3002\u901a\u5e38\u3001\u5c11\u91cf\u306e\u6e05\u6d44\u306aKBr\u3092\u633d\u304d\u3001\u305d\u308c\u3092\u5ec3\u68c4\u3057\u307e\u3059\u3002<\/li>\n<\/ul>\n<h3 id=\"when-to-choose-and-avoid-the-kbr-pellet-method\">KBr\u30da\u30ec\u30c3\u30c8\u6cd5\u3092\u9078\u3076\u3079\u304d\u6642\uff08\u305d\u3057\u3066\u907f\u3051\u308b\u3079\u304d\u6642<\/h3>\n<p>KBr\u6cd5\u306f\u3001\u6b63\u3057\u304f\u884c\u3048\u3070\u512a\u308c\u305f\u9ad8\u5206\u89e3\u80fd\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5f97\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002\u5e45\u5e83\u3044\u5b89\u5b9a\u3057\u305f\u975e\u53cd\u5fdc\u6027\u306e\u6709\u6a5f\u304a\u3088\u3073\u7121\u6a5f\u5316\u5408\u7269\u306b\u9069\u3057\u3066\u3044\u308b\u3002\u3057\u304b\u3057\u3001\u4e07\u80fd\u3067\u306f\u306a\u3044\u3002\u9ad8\u5727\u304c\u7d50\u6676\u6027\u7269\u8cea\u306e\u76f8\u5909\u5316\u3084\u591a\u5f62\u5909\u63db\u3092\u5f15\u304d\u8d77\u3053\u3057\u3001\u7570\u306a\u308b\u5f62\u614b\u306e\u7269\u8cea\u306e\u30b9\u30da\u30af\u30c8\u30eb\u306b\u3064\u306a\u304c\u308b\u3053\u3068\u304c\u3042\u308b\u305f\u3081\u3067\u3042\u308b(Giron, 2002)\u3002\u307e\u305f\u3001KBr\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u305d\u306e\u3082\u306e\u3068\u76f8\u4e92\u4f5c\u7528\u3059\u308b\u53ef\u80fd\u6027\u306e\u3042\u308b\u3001\u5438\u6e7f\u6027\u306e\u9ad8\u3044\u8a66\u6599\u3084\u53cd\u5fdc\u6027\u306e\u9ad8\u3044\u8a66\u6599\u306b\u3082\u9069\u3055\u306a\u3044\u3002\u3053\u306e\u3088\u3046\u306a\u30c7\u30ea\u30b1\u30fc\u30c8\u306a\u5834\u5408\u306b\u306f\u3001\u3088\u308a\u7a4f\u3084\u304b\u306a\u65b9\u6cd5\u306b\u983c\u3089\u3056\u308b\u3092\u5f97\u306a\u3044\u3002<\/p>\n<table class=\"mce-item-table\" style=\"width:100%; border-collapse: collapse;\" border=\"1\">\n<thead>\n<tr>\n<th style=\"text-align:left;\">\u7279\u5fb4<\/th>\n<th style=\"text-align:left;\">KBr\u30da\u30ec\u30c3\u30c8\u6cd5<\/th>\n<th style=\"text-align:left;\">\u30cc\u30b8\u30e7\u30eb\u30fb\u30de\u30eb\u30fb\u30e1\u30bd\u30c3\u30c9<\/th>\n<\/tr>\n<\/thead>\n<tbody>\n<tr>\n<td style=\"text-align:left;\"><strong>\u539f\u5247<\/strong><\/td>\n<td style=\"text-align:left;\">\u56fa\u4f53\u306e\u30cf\u30ed\u30b2\u30f3\u5316\u30a2\u30eb\u30ab\u30ea\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u306b\u5206\u6563\u3057\u305f\u8a66\u6599\u3002<\/td>\n<td style=\"text-align:left;\">\u30df\u30cd\u30e9\u30eb\u30aa\u30a4\u30eb\u306b\u5fae\u7c92\u5b50\u3068\u3057\u3066\u61f8\u6fc1\u3055\u308c\u305f\u30b5\u30f3\u30d7\u30eb\u3002<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u6e96\u5099<\/strong><\/td>\n<td style=\"text-align:left;\">\u7c89\u7815\u3001KBr\u3068\u306e\u6df7\u5408\u3001\u9ad8\u5727\u30d7\u30ec\u30b9\u3002<\/td>\n<td style=\"text-align:left;\">\u3059\u308a\u3064\u3076\u3057\u3001\u30cc\u30b8\u30e7\u30fc\u30eb\u3092\u4e00\u6ef4\u5782\u3089\u3057\u3066\u6df7\u305c\u3001\u5869\u306e\u76bf\u306b\u5857\u308b\u3002<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u30b5\u30f3\u30d7\u30eb\u91cf<\/strong><\/td>\n<td style=\"text-align:left;\">1-2 mg<\/td>\n<td style=\"text-align:left;\">2-5 mg<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u30e1\u30ea\u30c3\u30c8<\/strong><\/td>\n<td style=\"text-align:left;\">\u6eb6\u5a92\u30d4\u30fc\u30af\u304c\u306a\u304f\uff08\u6c5a\u67d3\u7269\u8cea\u3092\u9664\u304f\uff09\u3001\u9ad8\u5206\u89e3\u80fd\u30b9\u30da\u30af\u30c8\u30eb\u304c\u53ef\u80fd\u3002<\/td>\n<td style=\"text-align:left;\">\u9ad8\u5727\u3092\u4f7f\u7528\u3057\u306a\u3044\u305f\u3081\u3001\u611f\u5727\u6027\u30b5\u30f3\u30d7\u30eb\u3084\u6e7f\u6f64\u6027\u30b5\u30f3\u30d7\u30eb\u306b\u9069\u3057\u3066\u3044\u308b\u3002<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u30c7\u30e1\u30ea\u30c3\u30c8<\/strong><\/td>\n<td style=\"text-align:left;\">KBr\u306e\u5438\u6e7f\u6027\u3001\u5727\u529b\u306b\u3088\u308b\u5909\u5316\u306e\u53ef\u80fd\u6027\u3002<\/td>\n<td style=\"text-align:left;\">\u30de\u30ea\u30f3\u30b0\u5264\u306b\u306f\u72ec\u81ea\u306e\u30d4\u30fc\u30af\uff08C-H\u306e\u4f38\u7e2e\uff0f\u5c48\u66f2\uff09\u304c\u3042\u308a\u3001\u6563\u4e71\u306e\u53ef\u80fd\u6027\u304c\u3042\u308b\uff08\u30af\u30ea\u30b9\u30c1\u30e3\u30f3\u30bb\u30f3\u52b9\u679c\uff09\u3002<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u6700\u9069<\/strong><\/td>\n<td style=\"text-align:left;\">\u5b89\u5b9a\u3057\u305f\u3001\u975e\u53cd\u5fdc\u6027\u306e\u6709\u6a5f\u304a\u3088\u3073\u7121\u6a5f\u56fa\u4f53\uff1b\u5b9a\u91cf\u5206\u6790\uff08\u6ce8\u610f\u3092\u8981\u3059\u308b\uff09\uff1b\u9ad8\u54c1\u8cea\u306e\u53c2\u7167\u30b9\u30da\u30af\u30c8\u30eb\u306e\u53d6\u5f97\u3002<\/td>\n<td style=\"text-align:left;\">\u591a\u5f62\u7269\u8cea; \u6c34\u548c\u7269; \u53cd\u5fdc\u6027\u5316\u5408\u7269; \u8fc5\u901f\u306a\u5b9a\u6027\u30b9\u30ad\u30e3\u30f3\u3002<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<h2 id=\"method-2-the-nujol-mull-an-alternative-for-delicate-samples\">\u65b9\u6cd52\uff1a\u30cc\u30b8\u30e7\u30eb\u30fb\u30de\u30eb-\u30c7\u30ea\u30b1\u30fc\u30c8\u306a\u30b5\u30f3\u30d7\u30eb\u306e\u305f\u3081\u306e\u4ee3\u66ff\u6cd5<\/h2>\n<p>\u3082\u3057\u8a66\u6599\u304c\u7e4a\u7d30\u306a\u7d50\u6676\u306e\u3088\u3046\u306a\u3082\u306e\u3067\u3001KBr\u30d7\u30ec\u30b9\u306e\u5de8\u5927\u306a\u5727\u529b\u3067\u305d\u306e\u6027\u8cea\u304c\u5909\u308f\u3063\u3066\u3057\u307e\u3046\u3068\u3057\u305f\u3089\uff1f\u3042\u308b\u3044\u306f\u3001\u305d\u308c\u304c\u6c34\u548c\u7269\u3067\u3001\u5438\u6e7f\u6027\u306e\u3042\u308bKBr\u3067\u7c89\u7815\u3059\u308b\u3068\u3001\u5fc5\u8981\u306a\u6c34\u5206\u5b50\u3092\u53d6\u308a\u9664\u3044\u3066\u3057\u307e\u3046\u304b\u3082\u3057\u308c\u306a\u3044\u3002\u305d\u306e\u3088\u3046\u306a\u72b6\u6cc1\u306b\u5bfe\u3057\u3066\u3001Nujol\u306e\u30de\u30eb\u30fb\u30c6\u30af\u30cb\u30c3\u30af\u306f\u7a4f\u3084\u304b\u3067\u52b9\u679c\u7684\u306a\u4ee3\u66ff\u624b\u6bb5\u3092\u63d0\u4f9b\u3059\u308b\u3002\u9ad8\u5727\u3068\u53cd\u5fdc\u6027\u5869\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u3092\u4f7f\u7528\u305b\u305a\u3001\u4ee3\u308f\u308a\u306b\u30b5\u30f3\u30d7\u30eb\u3092\u6cb9\u6027\u5a92\u4f53\u306b\u61f8\u6fc1\u3055\u305b\u308b\u3002<\/p>\n<h3 id=\"the-concept-of-mulling-suspending-particles-in-oil\">\u30de\u30ea\u30f3\u30b0\u306e\u6982\u5ff5\u6cb9\u4e2d\u306b\u5fae\u7c92\u5b50\u3092\u61f8\u6fc1\u3055\u305b\u308b<\/h3>\n<p>\u7c92\u5b50\u5f84\u3092\u5c0f\u3055\u304f\u3059\u308b\u3053\u3068\u3067\u5149\u306e\u6563\u4e71\u3092\u6700\u5c0f\u9650\u306b\u6291\u3048\u308b\u3002\u305f\u3060\u3057\u3001\u7c92\u5b50\u3092\u56fa\u4f53\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u306b\u57cb\u3081\u8fbc\u3080\u306e\u3067\u306f\u306a\u304f\u3001\u5c48\u6298\u7387\u304c\u8fd1\u3044\u6db2\u4f53\u306b\u61f8\u6fc1\u3055\u305b\u308b\u3002\u3053\u308c\u304c \"\u30de\u30ea\u30f3\u30b0\u5264 \"\u306e\u5f79\u5272\u3067\u3059\u3002\u5149\u3092\u540c\u3058\u3088\u3046\u306b\u66f2\u3052\u308b\u6db2\u4f53\u3067\u30b5\u30f3\u30d7\u30eb\u7c92\u5b50\u3092\u53d6\u308a\u56f2\u3080\u3053\u3068\u3067\u3001\u7c92\u5b50\u3068\u6db2\u4f53\u306e\u754c\u9762\u306b\u304a\u3051\u308bIR\u30d3\u30fc\u30e0\u306e\u6563\u4e71\u304c\u5927\u5e45\u306b\u6e1b\u5c11\u3059\u308b\u3002<\/p>\n<p>\u53e4\u5178\u7684\u306a\u30de\u30ea\u30f3\u30b0\u5264\u306f\u30cc\u30b8\u30e7\u30fc\u30eb\u3067\u3001\u91cd\u304f\u7c98\u6027\u306e\u3042\u308b\u9271\u6cb9\u306e\u5546\u54c1\u540d\u3067\u3042\u308b\u3002\u30cc\u30b8\u30e7\u30fc\u30eb\u306f\u57fa\u672c\u7684\u306b\u9577\u9396\u98fd\u548c\u70ad\u5316\u6c34\u7d20\uff08\u30a2\u30eb\u30ab\u30f3\uff09\u306e\u6df7\u5408\u7269\u3067\u3042\u308b\u3002\u305d\u306e\u4e3b\u306a\u5229\u70b9\u306f\u3001\u4e2d\u8d64\u5916\u9818\u57df\u3067\u307b\u307c\u900f\u660e\u3067\u3042\u308b\u3053\u3068\u3067\u3042\u308b\u3002\u305d\u306e\u30b9\u30da\u30af\u30c8\u30eb\u306f\u975e\u5e38\u306b\u5358\u7d14\u3067\u3001C-H\u4f38\u7e2e\uff08\uff5e2950\uff5e2850cm-\u00b9\uff09\u3068C-H\u5c48\u66f2\uff08\uff5e1460\u304a\u3088\u30731375cm-\u00b9\uff09\u304b\u3089\u306e\u5438\u53ce\u306e\u307f\u304b\u3089\u306a\u308b\u3002\u3053\u308c\u3089\u306e\u30d4\u30fc\u30af\u306f\u3088\u304f\u77e5\u3089\u308c\u305f\u92ed\u3044\u30d4\u30fc\u30af\u3067\u3042\u308b\u305f\u3081\u3001\u5206\u6790\u8005\u306f\u901a\u5e38\u3001\u8a66\u6599\u306e\u5438\u53ce\u3068\u533a\u5225\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002<\/p>\n<h3 id=\"step-by-step-guide-to-preparing-a-nujol-mull\">\u30cc\u30b8\u30e7\u30eb\u30fb\u30df\u30e5\u30eb\u306e\u6e96\u5099\u306e\u30b9\u30c6\u30c3\u30d7\u30fb\u30d0\u30a4\u30fb\u30b9\u30c6\u30c3\u30d7\u30fb\u30ac\u30a4\u30c9<\/h3>\n<p>\u30de\u30eb\u6cd5\u306f\u3001KBr\u30da\u30ec\u30c3\u30c8\u6cd5\u3088\u308a\u3082\u8fc5\u901f\u3067\u3001\u5c02\u9580\u7684\u306a\u88c5\u7f6e\u3082\u5fc5\u8981\u306a\u3044\u3053\u3068\u304c\u591a\u3044\u305f\u3081\u3001\u8fc5\u901f\u306a\u5b9a\u6027\u30c1\u30a7\u30c3\u30af\u306b\u3088\u304f\u4f7f\u308f\u308c\u308b\u3002<\/p>\n<h4 id=\"grinding-the-sample\">\u30b5\u30f3\u30d7\u30eb\u306e\u7814\u78e8<\/h4>\n<p>KBr\u6cd5\u3068\u540c\u69d8\u3001\u3053\u306e\u30b9\u30c6\u30c3\u30d7\u306f\u6975\u3081\u3066\u91cd\u8981\u3067\u3042\u308b\u3002\u30e1\u30ce\u30a6\u4e73\u9262\u3068\u4e73\u68d2\u3092\u4f7f\u3063\u3066\u3001\u56fa\u5f62\u8a66\u6599\uff08\u901a\u5e382\uff5e5mg\uff09\u3092\u975e\u5e38\u306b\u7d30\u304b\u3044\u7c89\u672b\u306b\u3059\u308b\u5fc5\u8981\u304c\u3042\u308b\u3002\u76ee\u6a19\u306f2\u03bcm\u4ee5\u4e0b\u306e\u7c92\u5b50\u5f84\u3067\u3042\u308b\u3002\u7c92\u5b50\u304c\u7c97\u3044\u3068\u6563\u4e71\u304c\u3072\u3069\u304f\u306a\u308b\u3002<\/p>\n<h4 id=\"adding-the-mulling-agent\">\u30de\u30ea\u30f3\u30b0\u5264\u3092\u52a0\u3048\u308b<\/h4>\n<p>\u30b5\u30f3\u30d7\u30eb\u304c\u7d30\u304b\u3044\u30d1\u30a6\u30c0\u30fc\u306b\u306a\u3063\u305f\u3089\u3001\u3054\u304f\u5c11\u91cf\u306e\u30cc\u30b8\u30e7\u30fc\u30eb\u3092\u52a0\u3048\u308b\u3002\u76ee\u6a19\u306f\u3001\u30da\u30fc\u30b9\u30c8\u3092\u4f5c\u308b\u306e\u306b\u5fc5\u8981\u306a\u7d76\u5bfe\u6700\u5c0f\u91cf\u306e\u30aa\u30a4\u30eb\u3092\u4f7f\u7528\u3059\u308b\u3053\u3068\u3067\u3042\u308b\u3002\u30aa\u30a4\u30eb\u304c\u591a\u3059\u304e\u308b\u3068\u8a66\u6599\u304c\u904e\u5ea6\u306b\u5e0c\u91c8\u3055\u308c\u3001Nujol\u306e\u30d4\u30fc\u30af\u304c\u652f\u914d\u7684\u306a\u5f31\u3044\u30b9\u30da\u30af\u30c8\u30eb\u306b\u306a\u308b\u3002<\/p>\n<h4 id=\"creating-the-paste\">\u30da\u30fc\u30b9\u30c8\u306e\u4f5c\u6210<\/h4>\n<p>\u4e73\u68d2\u3092\u4f7f\u3044\u3001\u6df7\u5408\u7269\u3092\u633d\u304d\u7d9a\u3051\u308b\u3002Nujol\u304c\u6f64\u6ed1\u6cb9\u306e\u5f79\u5272\u3092\u679c\u305f\u3057\u3001\u7c89\u304c\u3059\u3050\u306b\u6fc3\u539a\u3067\u6ed1\u3089\u304b\u306a\u30da\u30fc\u30b9\u30c8\u72b6\u306b\u5909\u5316\u3059\u308b\u3002\u7406\u60f3\u7684\u306a\u56fa\u3055\u306f\u3001\u3088\u304f\u6b6f\u78e8\u304d\u7c89\u3084\u30ef\u30bb\u30ea\u30f3\u3068\u6bd4\u8f03\u3055\u308c\u308b\u3002\u5747\u4e00\u3067\u3001\u76ee\u306b\u898b\u3048\u308b\u7c92\u5b50\u304c\u306a\u3044\u3053\u3068\u304c\u671b\u307e\u3057\u3044\u3002<\/p>\n<h4 id=\"application\">\u7533\u3057\u8fbc\u307f<\/h4>\n<p>\u30e0\u30eb\u306f\u3001\u5e73\u3089\u306b\u78e8\u304b\u308c\u305f2\u679a\u306e\u5869\u30d7\u30ec\u30fc\u30c8\u306e\u9593\u3067\u5206\u6790\u3055\u308c\u308b\u3002\u3053\u308c\u3089\u306e\u30d7\u30ec\u30fc\u30c8\u306f\u901a\u5e38\u3001\u5869\u5316\u30ca\u30c8\u30ea\u30a6\u30e0\uff08NaCl\uff09\u307e\u305f\u306f\u81ed\u5316\u30ab\u30ea\u30a6\u30e0\uff08KBr\uff09\u3067\u3067\u304d\u3066\u304a\u308a\u3001\u8d64\u5916\u7dda\u306b\u5bfe\u3057\u3066\u900f\u660e\u3067\u3042\u308b\u3002<\/p>\n<ol>\n<li><strong>\u79fb\u7c4d\u3059\u308b\uff1a<\/strong> \u5c0f\u3055\u306a\u30d8\u30e9\u3092\u4f7f\u3063\u3066\u3001\u5869\u306e\u76bf\u306e\u4e2d\u592e\u306b\u30e0\u30eb\u30da\u30fc\u30b9\u30c8\u3092\u3072\u3068\u305f\u3089\u3057\u3059\u308b\u3002<\/li>\n<li><strong>\u30b5\u30f3\u30c9\u30a4\u30c3\u30c1\uff1a<\/strong> 2\u679a\u76ee\u306e\u30bd\u30eb\u30c8\u30d7\u30ec\u30fc\u30c8\u30921\u679a\u76ee\u306e\u4e0a\u306b\u7f6e\u304d\u3001\u8efd\u304f\u56de\u8ee2\u3055\u305b\u308b\u3002\u3053\u3046\u3059\u308b\u3053\u3068\u3067\u3001\u5869\u306e\u819c\u304c\u8584\u304f\u5747\u4e00\u306b\u306a\u308b\u3002\u819c\u306f\u308f\u305a\u304b\u306b\u534a\u900f\u660e\u306b\u898b\u3048\u307e\u3059\u304c\u3001\u900f\u3051\u3066\u898b\u3048\u306a\u3044\u307b\u3069\u539a\u304f\u306f\u306a\u308a\u307e\u305b\u3093\u3002<\/li>\n<li><strong>\u30de\u30a6\u30f3\u30c8\u3060\uff1a<\/strong> \u30d7\u30ec\u30fc\u30c8\u306e \"\u30b5\u30f3\u30c9\u30a4\u30c3\u30c1 \"\u3092\u53d6\u308a\u5916\u3057\u53ef\u80fd\u306a\u30bb\u30eb\u30db\u30eb\u30c0\u30fc\u306b\u5165\u308c\u3001\u305d\u308c\u3092\u5206\u5149\u8a08\u306e\u30b5\u30f3\u30d7\u30eb\u30b3\u30f3\u30d1\u30fc\u30c8\u30e1\u30f3\u30c8\u306b\u5165\u308c\u308b\u3002<\/li>\n<\/ol>\n<h3 id=\"navigating-the-challenges-of-mulls\">\u30de\u30eb\u306e\u8ab2\u984c\u3092\u514b\u670d\u3059\u308b\u305f\u3081\u306b<\/h3>\n<p>\u5358\u7d14\u306a\u9762\u3082\u3042\u308b\u304c\u3001\u30de\u30eb\u30fb\u30c6\u30af\u30cb\u30c3\u30af\u306b\u306f\u89e3\u91c8\u4e0a\u306e\u8ab2\u984c\u304c\u3042\u308b\u3002<\/p>\n<h4 id=\"nujol-s-own-spectrum\">\u30cc\u30b8\u30e7\u30eb\u72ec\u81ea\u306e\u30b9\u30da\u30af\u30c8\u30e9\u30e0<\/h4>\n<p>\u6700\u3082\u660e\u767d\u306a\u554f\u984c\u306f\u3001\u30cc\u30b8\u30e7\u30fc\u30eb\u30d4\u30fc\u30af\u306e\u5b58\u5728\u3067\u3042\u308b\u3002\u5f37\u3044C-H\u4f38\u7e2e\u30d0\u30f3\u30c9\u3068\u5c48\u66f2\u30d0\u30f3\u30c9\u304c\u5e38\u306b\u5b58\u5728\u3057\u307e\u3059\u3002\u3053\u308c\u306f\u3001\u30b5\u30f3\u30d7\u30eb\u306eC-H\u632f\u52d5\u3092\u78ba\u5b9f\u306b\u5206\u6790\u3067\u304d\u306a\u3044\u3053\u3068\u3092\u610f\u5473\u3057\u307e\u3059\u3002C-H\u9818\u57df\u306b\u6b63\u78ba\u306b\u8208\u5473\u304c\u3042\u308b\u5834\u5408\u3001Nujol mull\u306f\u4e0d\u9069\u5207\u306a\u9078\u629e\u3067\u3059\u3002<\/p>\n<h4 id=\"alternative-mulling-agents\">\u4ee3\u66ff\u30de\u30ea\u30f3\u30b0\u30fb\u30a8\u30fc\u30b8\u30a7\u30f3\u30c8<\/h4>\n<p>\u3053\u306e\u5236\u9650\u3092\u514b\u670d\u3059\u308b\u305f\u3081\u306b\u3001\u88dc\u5b8c\u7684\u306a\u30de\u30ea\u30f3\u30b0\u5264\u3092\u4f7f\u7528\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002Fluorolube\u306f\u4e00\u822c\u7684\u306a\u9078\u629e\u80a2\u3067\u3042\u308b\u3002\u3053\u308c\u306f\u30d5\u30c3\u7d20\u5316\u70ad\u5316\u6c34\u7d20\u306e\u6df7\u5408\u7269\u3067\u3042\u308b\u3002C-H\u7d50\u5408\u3092\u542b\u307e\u306a\u3044\u305f\u3081\u3001\u305d\u306e\u30b9\u30da\u30af\u30c8\u30eb\u306b\u306fC-H\u4f38\u7e2e\u9818\u57df\u306e\u5438\u53ce\u304c\u306a\u3044\u3002\u3057\u304b\u3057\u3001\u4f4e\u5468\u6ce2\u6570\u9818\u57df\uff08\uff5e1300cm-\u00b9\u4ee5\u4e0b\uff09\u306b\u306f\u5f37\u3044C-F\u5438\u53ce\u304c\u3042\u308b\u30021\u3064\u306fNujol\u3067\u4f4e\u5468\u6ce2\u6570\u9818\u57df\u3092\u660e\u77ad\u306b\u898b\u308b\u305f\u3081\u3001\u3082\u30461\u3064\u306fFluorolube\u3067C-H\u9818\u57df\u3092\u660e\u77ad\u306b\u898b\u308b\u305f\u3081\u3067\u3059\u3002\u4e21\u65b9\u304b\u3089\u306e\u60c5\u5831\u3092\u7d44\u307f\u5408\u308f\u305b\u308b\u3053\u3068\u3067\u3001\u5168\u4f53\u50cf\u3092\u7d44\u307f\u7acb\u3066\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002<\/p>\n<h4 id=\"the-christiansen-effect\">\u30af\u30ea\u30b9\u30c1\u30e3\u30f3\u30bb\u30f3\u52b9\u679c<\/h4>\n<p>\u6ce8\u610f\u6df1\u304f\u7814\u78e8\u3057\u3066\u3082\u3001\u30de\u30eb\u30b9\u30da\u30af\u30c8\u30eb\u304c\u6b6a\u3093\u3060\u975e\u5bfe\u79f0\u306e\u30d4\u30fc\u30af\u3092\u793a\u3057\u3001\u9ad8\u3044\u5468\u6ce2\u6570\u3067\u30d9\u30fc\u30b9\u30e9\u30a4\u30f3\u304c\u4e0a\u6607\u3059\u308b\u3053\u3068\u304c\u3042\u308b\u3002\u3053\u308c\u306fChristiansen\u52b9\u679c\u306b\u3088\u308b\u3053\u3068\u304c\u591a\u304f\u3001\u56fa\u4f53\u7c92\u5b50\u3068\u30df\u30e5\u30fc\u30ea\u30f3\u30b0\u5264\u306e\u5c48\u6298\u7387\u304c\u7279\u5b9a\u306e\u6ce2\u9577\u3067\u4e00\u81f4\u3059\u308b\u5834\u5408\u306b\u8d77\u3053\u308a\u307e\u3059\uff08Christiansen, 1884\uff09\u3002\u3053\u306e\u6ce2\u9577\u3067\u306f\u6563\u4e71\u306f\u6700\u5c0f\u5316\u3055\u308c\u308b\u304c\u3001\u5c48\u6298\u7387\u304c\u767a\u6563\u3059\u308b\u4ed6\u306e\u6ce2\u9577\u3067\u306f\u6563\u4e71\u304c\u5897\u52a0\u3059\u308b\u3002\u3053\u308c\u306f\u3001\u7c92\u5b50\u5f84\u3092\u3055\u3089\u306b\u5c0f\u3055\u304f\u3059\u308b\u305f\u3081\u306b\u3088\u308a\u5fb9\u5e95\u7684\u306a\u7c89\u7815\u3092\u884c\u3046\u304b\u3001\u5c48\u6298\u7387\u304c\u8a66\u6599\u306e\u5c48\u6298\u7387\u306b\u8fd1\u3044\u30de\u30ea\u30f3\u30b0\u5264\u3092\u898b\u3064\u3051\u308b\u3088\u3046\u306b\u3059\u308b\u3053\u3068\u3067\u6700\u5c0f\u9650\u306b\u6291\u3048\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u304c\u3001\u73fe\u5b9f\u7684\u3067\u306a\u3044\u3053\u3068\u304c\u591a\u3044\u3002<\/p>\n<h3 id=\"comparing-kbr-pellets-and-nujol-mulls\">KBr\u30da\u30ec\u30c3\u30c8\u3068\u30cc\u30b8\u30e7\u30fc\u30eb\u30de\u30eb\u306e\u6bd4\u8f03<\/h3>\n<p>\u3053\u308c\u30892\u3064\u306e\u53e4\u5178\u7684\u306a\u900f\u904e\u6cd5\u306e\u3069\u3061\u3089\u3092\u9078\u3076\u304b\u306f\u3001\u30c8\u30ec\u30fc\u30c9\u30aa\u30d5\u306e\u95a2\u4fc2\u306b\u3042\u308b\u3002KBr\u30da\u30ec\u30c3\u30c8\u306f\u3001\u5168\u9818\u57df\u306b\u308f\u305f\u3063\u3066\u300c\u3088\u308a\u304d\u308c\u3044\u306a\u300d\u30b9\u30da\u30af\u30c8\u30eb\u304c\u5f97\u3089\u308c\u308b\u53ef\u80fd\u6027\u304c\u3042\u308b\u304c\u3001\u305d\u306e\u4ee3\u511f\u3068\u3057\u3066\u3001\u3088\u308a\u591a\u304f\u306e\u52b4\u529b\u3068\u8a66\u6599\u3078\u306e\u6f5c\u5728\u7684\u306a\u30c0\u30e1\u30fc\u30b8\u304c\u304b\u304b\u308b\u3002Nujol mull\u306f\u3001\u3088\u308a\u8fc5\u901f\u3067\u7a4f\u3084\u304b\u3060\u304c\u3001\u72ec\u81ea\u306e\u30b9\u30da\u30af\u30c8\u30eb\u306e\u7279\u5fb4\u304c\u73fe\u308c\u308b\u3002\u4e26\u3079\u3066\u6bd4\u8f03\u3059\u308b\u3053\u3068\u3067\u3001\u305d\u308c\u305e\u308c\u306e\u9577\u6240\u3068\u77ed\u6240\u304c\u660e\u3089\u304b\u306b\u306a\u308a\u3001\u5206\u6790\u8005\u306e\u6c7a\u65ad\u306e\u6307\u91dd\u3068\u306a\u308a\u307e\u3059\u3002\u4e0a\u306e\u8868\u306f\u3001\u3053\u308c\u30892\u3064\u306e\u57fa\u672c\u7684\u306a\u6280\u8853\u3092\u69cb\u9020\u7684\u306b\u6bd4\u8f03\u3057\u305f\u3082\u306e\u3067\u3059\u3002<\/p>\n<h2 id=\"method-3-attenuated-total-reflectance-atr-the-modern-powerhouse\">\u65b9\u6cd53\uff1a\u6e1b\u8870\u5168\u53cd\u5c04\u7387\uff08ATR\uff09 - \u73fe\u4ee3\u306e\u30d1\u30ef\u30fc\u30cf\u30a6\u30b9<\/h2>\n<p>\u4f55\u5341\u5e74\u3082\u306e\u9593\u3001KBr\u30da\u30ec\u30c3\u30c8\u3068Nujol\u30de\u30eb\u306f\u3001\u56fa\u4f53\u8a66\u6599FTIR\u306e\u4e3b\u529b\u88fd\u54c1\u3068\u3057\u3066\u77e5\u3089\u308c\u3066\u3044\u305f\u3002\u3053\u308c\u3089\u306f\u5f37\u529b\u3060\u304c\u3001\u624b\u9593\u304c\u304b\u304b\u308a\u3001\u7834\u58ca\u7684\u3067\u3042\u308b\u3002\u30eb\u30fc\u30c1\u30f3\u5206\u6790\u306e\u72b6\u6cc1\u306f\u3001\u6e1b\u8870\u5168\u53cd\u5c04\u6cd5\uff08ATR\uff09\u306e\u6539\u826f\u3068\u666e\u53ca\u306b\u3088\u3063\u3066\u5287\u7684\u306b\u5909\u5316\u3057\u305f\u3002\u3053\u306e\u6280\u6cd5\u306f\u3001\u3057\u3070\u3057\u3070\u6700\u65b0\u306eFTIR\u306e\u6a19\u6e96\u6a5f\u80fd\u3068\u3057\u3066\u898b\u3089\u308c\u308b\u3002 <a href=\"https:\/\/www.hcftir.com\/ir-sample-preparation-category\/\" rel=\"nofollow\">\u30d5\u30fc\u30ea\u30a8\u5909\u63db\u8d64\u5916\u5206\u5149\u8a08<\/a>ATR\u306f\u3001\u606f\u3092\u306e\u3080\u3088\u3046\u306a\u30b7\u30f3\u30d7\u30eb\u3055\u3068\u30b9\u30d4\u30fc\u30c9\u3092\u63d0\u4f9b\u3057\u3001\u5f93\u6765\u306e\u65b9\u6cd5\u306e\u3088\u3046\u306a\u9aa8\u306e\u6298\u308c\u308b\u7814\u78e8\u3084\u30d7\u30ec\u30b9\u306f\u307b\u3068\u3093\u3069\u5fc5\u8981\u306a\u3044\u30022025\u5e74\u306b\u304a\u3051\u308b\u591a\u304f\u306e\u7528\u9014\u3067\u3001ATR\u306f\u6700\u521d\u306e\u9078\u629e\u80a2\u3068\u306a\u308b\u3002<\/p>\n<h3 id=\"the-physics-of-atr-an-evanescent-wave-at-work\">ATR\u306e\u7269\u7406\u5b66\uff1a\u30a8\u30d0\u30cd\u30c3\u30bb\u30f3\u30c8\u6ce2\u306e\u4ed5\u4e8b<\/h3>\n<p>IR\u30d3\u30fc\u30e0\u304c\u30b5\u30f3\u30d7\u30eb\u3092\u901a\u904e\u3059\u308b\u900f\u904e\u6cd5\u3068\u306f\u7570\u306a\u308a\u3001ATR\u306f\u5185\u90e8\u53cd\u5c04\u73fe\u8c61\u306b\u57fa\u3065\u304f\u8868\u9762\u6280\u8853\u3067\u3059\u3002\u9ad8\u5bc6\u5ea6\u306e\u5a92\u8cea\uff08\u30c0\u30a4\u30e4\u30e2\u30f3\u30c9\u306a\u3069\uff09\u3092\u901a\u904e\u3059\u308b\u5149\u30d3\u30fc\u30e0\u304c\u3001\u9ad8\u89d2\u5ea6\u3067\u4f4e\u5bc6\u5ea6\u306e\u5a92\u8cea\uff08\u8a66\u6599\u306a\u3069\uff09\u3068\u306e\u5883\u754c\u306b\u5f53\u305f\u308b\u3068\u3057\u307e\u3059\u3002\u3053\u306e\u3068\u304d\u3001\u5149\u306f\u8a66\u6599\u306e\u4e2d\u3092\u901a\u904e\u3059\u308b\u306e\u3067\u306f\u306a\u304f\u3001\u5b8c\u5168\u306b\u53cd\u5c04\u3057\u3066\u30c0\u30a4\u30e4\u30e2\u30f3\u30c9\u306e\u4e2d\u306b\u623b\u3063\u3066\u304d\u307e\u3059\u3002\u3053\u308c\u304c\u5168\u53cd\u5c04\u3067\u3059\u3002<\/p>\n<p>\u53cd\u5c04\u306e\u30dd\u30a4\u30f3\u30c8\u3067\u306f\u3001\u30a8\u30d0\u30cd\u30c3\u30bb\u30f3\u30c8\u6ce2\u3068\u3057\u3066\u77e5\u3089\u308c\u308b\u96fb\u78c1\u5834\u304c\u3001\u5b9f\u969b\u306b\u306f\u975e\u5e38\u306b\u77ed\u3044\u8ddd\u96e2\uff08\u901a\u5e380.5\uff5e2 \u00b5m\uff09\u3067\u3001\u5bc6\u5ea6\u306e\u4f4e\u3044\u5a92\u8cea\uff08\u8a66\u6599\uff09\u306b\u6d78\u900f\u3059\u308b\u3002\u3053\u306e\u6ce2\u306f\u5f93\u6765\u306e\u610f\u5473\u3067\u306e\u4f1d\u64ad\u5149\u3067\u306f\u306a\u304f\u3001\u8868\u9762\u304b\u3089\u306e\u8ddd\u96e2\u306b\u5fdc\u3058\u3066\u6307\u6570\u95a2\u6570\u7684\u306b\u6e1b\u8870\u3059\u308b\u975e\u653e\u5c04\u5834\u3067\u3042\u308b\u3002\u30b5\u30f3\u30d7\u30eb\u306b\u7279\u5b9a\u306e\u8d64\u5916\u5468\u6ce2\u6570\u3067\u5438\u53ce\u3059\u308b\u5b98\u80fd\u57fa\u304c\u3042\u308b\u5834\u5408\u3001\u30a8\u30d0\u30cd\u30c3\u30bb\u30f3\u30c8\u6ce2\u306f\u305d\u306e\u5468\u6ce2\u6570\u3067\u300c\u6e1b\u8870\u300d\u307e\u305f\u306f\u5f31\u307e\u308a\u307e\u3059\u3002\u53cd\u5c04\u3055\u308c\u305f\u30d3\u30fc\u30e0\u306f\u3001\u3053\u306e\u6e1b\u8870\u306e \"\u523b\u5370 \"\u3092\u6301\u3061\u3001\u691c\u51fa\u5668\u3078\u3068\u5411\u304b\u3046\u3002\u7d50\u679c\u3068\u3057\u3066\u5f97\u3089\u308c\u308b\u30b9\u30da\u30af\u30c8\u30eb\u306f\u3001\u5f93\u6765\u306e\u900f\u904e\u30b9\u30da\u30af\u30c8\u30eb\u3068\u975e\u5e38\u306b\u3088\u304f\u4f3c\u3066\u3044\u308b\u304c\u3001\u30b5\u30f3\u30d7\u30eb\u306e\u3054\u304f\u8868\u9762\u5c64\u306e\u307f\u3092\u8868\u3057\u3066\u3044\u308b\u3002<\/p>\n<h4 id=\"the-atr-crystal\">ATR\u30af\u30ea\u30b9\u30bf\u30eb<\/h4>\n<p>ATR\u30a2\u30af\u30bb\u30b5\u30ea\u30fc\u306e\u5fc3\u81d3\u90e8\u306f\u7d50\u6676\u3067\u3042\u308a\u3001\u5185\u90e8\u53cd\u5c04\u304c\u8d77\u3053\u308b\u9ad8\u5bc6\u5ea6\u306e\u5a92\u4f53\u3067\u3059\u3002\u7d50\u6676\u306e\u9078\u629e\u306f\u91cd\u8981\u3067\u3042\u308a\u3001\u30b5\u30f3\u30d7\u30eb\u306e\u7279\u6027\u3084\u5e0c\u671b\u3059\u308b\u30b9\u30da\u30af\u30c8\u30eb\u7bc4\u56f2\u306b\u3088\u3063\u3066\u7570\u306a\u308a\u307e\u3059\u3002<\/p>\n<ul>\n<li><strong>\u30c0\u30a4\u30e4\u30e2\u30f3\u30c9<\/strong> \u6c4e\u7528ATR\u3068\u3057\u3066\u6700\u3082\u30dd\u30d4\u30e5\u30e9\u30fc\u306a\u9078\u629e\u80a2\u3067\u3059\u3002\u9a5a\u304f\u307b\u3069\u786c\u304f\u3001\u5316\u5b66\u7684\u306b\u4e0d\u6d3b\u6027\u3067\u3042\u308b\u305f\u3081\u3001\u786c\u3044\u7c89\u4f53\u3001\u8150\u98df\u6027\u7269\u8cea\u3001\u7814\u78e8\u6027\u56fa\u4f53\u306e\u5206\u6790\u306b\u6700\u9069\u3067\u3059\u3002\u826f\u597d\u306a\u63a5\u89e6\u3092\u78ba\u4fdd\u3059\u308b\u305f\u3081\u306b\u5fc5\u8981\u306a\u9ad8\u5727\u306b\u3082\u8010\u3048\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002\u4e3b\u306a\u5236\u9650\u306f\u3001\u5358\u4e00\u53cd\u5c04\u30e6\u30cb\u30c3\u30c8\u306e\u5834\u5408\u3001\uff5e1000 cm-\u00b9\u4ee5\u4e0b\u306e\u30b9\u30eb\u30fc\u30d7\u30c3\u30c8\u304c\u4f4e\u3044\u3053\u3068\u3067\u3042\u308b\u3002<\/li>\n<li><strong>\u30bb\u30ec\u30f3\u5316\u4e9c\u925b\uff08ZnSe\uff09\uff1a<\/strong> \u4e00\u822c\u7684\u3067\u30b3\u30b9\u30c8\u30d1\u30d5\u30a9\u30fc\u30de\u30f3\u30b9\u306e\u9ad8\u3044\u7d50\u6676\u3002\u67d4\u3089\u304b\u3044\u56fa\u4f53\u3001\u6db2\u4f53\u3001\u30da\u30fc\u30b9\u30c8\u306b\u9069\u3057\u3066\u3044\u308b\u3002\u3057\u304b\u3057\u3001\u8edf\u3089\u304b\u3044\u306e\u3067\u786c\u3044\u8a66\u6599\u3067\u306f\u50b7\u304c\u3064\u304d\u3084\u3059\u3044\u3002\u307e\u305f\u3001\u5f37\u9178\u3084\u5f37\u5869\u57fa\u306b\u4fb5\u3055\u308c\u3084\u3059\u3044\u3002<\/li>\n<li><strong>\u30b2\u30eb\u30de\u30cb\u30a6\u30e0\uff08Ge\uff09\uff1a<\/strong> \u3053\u306e\u7d50\u6676\u306f\u5c48\u6298\u7387\u304c\u975e\u5e38\u306b\u9ad8\u3044\u3002\u305d\u306e\u305f\u3081\u3001\u30a8\u30d0\u30cd\u30c3\u30bb\u30f3\u30c8\u6ce2\u306e\u900f\u904e\u6df1\u5ea6\u304c\u975e\u5e38\u306b\u6d45\u304f\u306a\u308a\u307e\u3059\uff081 \u00b5m\u672a\u6e80\uff09\u3002\u3053\u306e\u305f\u3081\u3001\u4ed6\u306e\u7d50\u6676\u3067\u306f\u30d3\u30fc\u30e0\u3092\u5b8c\u5168\u306b\u5438\u53ce\u3057\u3066\u3057\u307e\u3046\u3088\u3046\u306a\u9ad8\u5438\u53ce\u30b5\u30f3\u30d7\u30eb\uff08\u70ad\u7d20\u5145\u586b\u30dd\u30ea\u30de\u30fc\u306a\u3069\uff09\u306e\u5206\u6790\u306b\u6700\u9069\u3067\u3059\u3002\u307e\u305f\u3001\u4e0b\u306e\u30d0\u30eb\u30af\u6750\u6599\u304b\u3089\u306e\u5e72\u6e09\u3092\u53d7\u3051\u305a\u306b\u3001\u8584\u3044\u8868\u9762\u5c64\u306e\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5f97\u308b\u306e\u306b\u3082\u6709\u7528\u3067\u3042\u308b\u3002<\/li>\n<\/ul>\n<h3 id=\"a-practical-guide-to-atr-ftir-analysis\">ATR-FTIR\u5206\u6790\u5b9f\u8df5\u30ac\u30a4\u30c9<\/h3>\n<p>ATR\u306e\u30ef\u30fc\u30af\u30d5\u30ed\u30fc\u306f\u975e\u5e38\u306b\u30b7\u30f3\u30d7\u30eb\u3067\u3042\u308a\u3001\u3053\u308c\u304c\u5e83\u304f\u63a1\u7528\u3055\u308c\u3066\u3044\u308b\u4e3b\u306a\u7406\u7531\u3067\u3042\u308b\u3002ATR\u3092\u4f7f\u7528\u3057\u305fIR\u5206\u6790\u306e\u305f\u3081\u306e\u56fa\u4f53\u30b5\u30f3\u30d7\u30eb\u306e\u8abf\u88fd\u65b9\u6cd5\u3092\u5b66\u3076\u3053\u3068\u306f\u3001\u307b\u3068\u3093\u3069\u306e\u5834\u5408\u3001\u826f\u597d\u306a\u63a5\u89e6\u3092\u78ba\u4fdd\u3059\u308b\u3053\u3068\u3067\u3042\u308b\u3002<\/p>\n<ol>\n<li><strong>\u30af\u30ea\u30b9\u30bf\u30eb\u3092\u6383\u9664\u3059\u308b\uff1a<\/strong> \u3053\u308c\u306f\u3059\u3079\u3066\u306e\u6e2c\u5b9a\u306e\u6700\u521d\u3067\u6700\u5f8c\u306e\u30b9\u30c6\u30c3\u30d7\u3067\u3059\u3002\u7d50\u6676\u8868\u9762\u306f\u6e05\u6d44\u3067\u306a\u3051\u308c\u3070\u306a\u308a\u307e\u305b\u3093\u3002\u4ee5\u524d\u306e\u30b5\u30f3\u30d7\u30eb\u306e\u6b8b\u7559\u7269\u304c\u3042\u308b\u3068\u3001\u73fe\u5728\u306e\u30b9\u30da\u30af\u30c8\u30eb\u306b\u73fe\u308c\u307e\u3059\u3002\u9069\u5207\u306a\u6eb6\u5a92\uff08\u30a4\u30bd\u30d7\u30ed\u30d1\u30ce\u30fc\u30eb\u3084\u30e1\u30bf\u30ce\u30fc\u30eb\u306a\u3069\uff09\u3067\u6e7f\u3089\u305b\u305f\u7cf8\u304f\u305a\u306e\u51fa\u306a\u3044\u67d4\u3089\u304b\u3044\u5e03\u3067\u7d50\u6676\u3092\u62ed\u304d\u3001\u5b8c\u5168\u306b\u4e7e\u71e5\u3055\u305b\u307e\u3059\u3002<\/li>\n<li><strong>\u80cc\u666f\u30b9\u30da\u30af\u30c8\u30eb\u3092\u53ce\u96c6\u3059\u308b\uff1a<\/strong> \u8a66\u6599\u3092\u5c0e\u5165\u3059\u308b\u524d\u306b\u3001\u30d0\u30c3\u30af\u30b0\u30e9\u30a6\u30f3\u30c9\u30b9\u30da\u30af\u30c8\u30eb\u3092\u53ce\u96c6\u3059\u308b\u5fc5\u8981\u304c\u3042\u308a\u307e\u3059\u3002\u3053\u308c\u306f\u3001\u304d\u308c\u3044\u3067\u4e7e\u71e5\u3057\u305f\u7d50\u6676\u3092\u7a7a\u6c17\u306b\u3055\u3089\u3057\u305f\u72b6\u614b\u3067\u884c\u3044\u307e\u3059\u3002\u5206\u5149\u8a08\u306f\u3001\u7d50\u6676\u3001\u5468\u56f2\u306e\u5927\u6c17\uff08\u6c34\u84b8\u6c17\u3068CO\u2082\uff09\u3001\u88c5\u7f6e\u81ea\u4f53\u306e\u30b9\u30da\u30af\u30c8\u30eb\u3092\u6e2c\u5b9a\u3057\u307e\u3059\u3002\u3053\u306e\u30d0\u30c3\u30af\u30b0\u30e9\u30a6\u30f3\u30c9\u306f\u3001\u6b21\u306b\u30b5\u30f3\u30d7\u30eb\u30b9\u30da\u30af\u30c8\u30eb\u304b\u3089\u30c7\u30b8\u30bf\u30eb\u7684\u306b\u5dee\u3057\u5f15\u304b\u308c\u3001\u4e0d\u8981\u306a\u4fe1\u53f7\u304c\u3059\u3079\u3066\u53d6\u308a\u9664\u304b\u308c\u307e\u3059\u3002<\/li>\n<li><strong>\u30b5\u30f3\u30d7\u30eb\u3092\u9069\u7528\u3059\u308b\uff1a<\/strong> \u5c11\u91cf\u306e\u56fa\u4f53\u8a66\u6599\u3092\u7d50\u6676\u306e\u4e0a\u306b\u76f4\u63a5\u7f6e\u304d\u307e\u3059\u3002\u7c89\u672b\u306e\u5834\u5408\u306f\u3001\u7d50\u6676\u306e\u8868\u9762\uff08\u76f4\u5f841\uff5e2mm\u7a0b\u5ea6\u3067\u3042\u308b\u3053\u3068\u304c\u591a\u3044\uff09\u3092\u8986\u3046\u3060\u3051\u306e\u91cf\u304c\u5fc5\u8981\u3067\u3059\u3002\u3088\u308a\u5927\u304d\u306a\u56fa\u4f53\u8a66\u6599\u306e\u5834\u5408\u306f\u3001\u7d50\u6676\u306e\u4e0a\u306b\u7f6e\u304f\u3060\u3051\u3067\u3059\u3002<\/li>\n<li><strong>\u5727\u529b\u3092\u304b\u3051\u308b\uff1a<\/strong> \u3053\u308c\u306f\u56fa\u4f53\u8a66\u6599\u306b\u3068\u3063\u3066\u6700\u3082\u91cd\u8981\u306a\u30b9\u30c6\u30c3\u30d7\u3067\u3059\u3002ATR\u30a2\u30af\u30bb\u30b5\u30ea\u30fc\u306b\u306f\u3001\u5727\u529b\u30a2\u30f3\u30d3\u30eb\u307e\u305f\u306f\u30af\u30e9\u30f3\u30d7\u304c\u3042\u308a\u307e\u3059\u3002\u30a2\u30f3\u30d3\u30eb\u3092\u30b5\u30f3\u30d7\u30eb\u306b\u4e0b\u308d\u3057\u3001\u30ce\u30d6\u3092\u56de\u3057\u3066\u5727\u529b\u3092\u304b\u3051\u307e\u3059\u3002\u3053\u308c\u306b\u3088\u308a\u3001\u56fa\u4f53\u304c\u7d50\u6676\u8868\u9762\u306b\u5bc6\u7740\u3057\u307e\u3059\u3002\u63a5\u89e6\u304c\u826f\u597d\u3067\u306a\u3044\u3068\u3001\u30a8\u30d0\u30cd\u30c3\u30bb\u30f3\u30c8\u6ce2\u304c\u8a66\u6599\u3068\u52b9\u679c\u7684\u306b\u76f8\u4e92\u4f5c\u7528\u3067\u304d\u305a\u3001\u30b9\u30da\u30af\u30c8\u30eb\u304c\u5f31\u304f\u306a\u3063\u305f\u308a\u3001\u30ce\u30a4\u30ba\u304c\u5165\u3063\u305f\u308a\u3001\u5b58\u5728\u3057\u306a\u304b\u3063\u305f\u308a\u3057\u307e\u3059\u3002\u5727\u529b\u306f\u8a66\u6599\u3092\u30df\u30af\u30ed\u306e\u30ec\u30d9\u30eb\u3067\u308f\u305a\u304b\u306b\u5909\u5f62\u3055\u305b\u3001\u63a5\u89e6\u9762\u7a4d\u3092\u6700\u5927\u306b\u3057\u307e\u3059\u3002<\/li>\n<\/ol>\n<h3 id=\"advantages-and-limitations-of-the-atr-technique\">ATR\u6280\u8853\u306e\u5229\u70b9\u3068\u9650\u754c<\/h3>\n<p>ATR\u306f\u3042\u307e\u308a\u306b\u826f\u3059\u304e\u308b\u3088\u3046\u306b\u601d\u3048\u308b\u304c\u3001\u305d\u306e\u5177\u4f53\u7684\u306a\u7279\u5fb4\u3092\u7406\u89e3\u3059\u308b\u3053\u3068\u304c\u91cd\u8981\u3067\u3042\u308b\u3002<\/p>\n<h4 id=\"speed-and-simplicity\">\u30b9\u30d4\u30fc\u30c9\u3068\u30b7\u30f3\u30d7\u30eb\u3055<\/h4>\n<p>\u6700\u5927\u306e\u5229\u70b9\u306f\u3001\u30b5\u30f3\u30d7\u30eb\u306e\u524d\u51e6\u7406\u3092\u307b\u307c\u5b8c\u5168\u306b\u7701\u3051\u308b\u3053\u3068\u3060\u3002\u7c89\u7815\u3082\u6df7\u5408\u3082\u30d7\u30ec\u30b9\u3082\u306a\u3044\u3002\u30b9\u30da\u30af\u30c8\u30eb\u306f1\u5206\u4ee5\u5185\u306b\u5f97\u3089\u308c\u308b\u3002\u3053\u306e\u305f\u3081\u3001\u30cf\u30a4\u30b9\u30eb\u30fc\u30d7\u30c3\u30c8\u30b9\u30af\u30ea\u30fc\u30cb\u30f3\u30b0\u3001\u54c1\u8cea\u7ba1\u7406\u3001\u30b9\u30d4\u30fc\u30c9\u304c\u6700\u512a\u5148\u3055\u308c\u308b\u3042\u3089\u3086\u308b\u30a2\u30d7\u30ea\u30b1\u30fc\u30b7\u30e7\u30f3\u306b\u7406\u60f3\u7684\u3067\u3042\u308b\u3002\u307e\u305f\u3001\u307b\u3068\u3093\u3069\u975e\u7834\u58ca\u3067\u3001\u5206\u6790\u5f8c\u306b\u30b5\u30f3\u30d7\u30eb\u3092\u56de\u53ce\u3067\u304d\u308b\u3053\u3068\u3082\u591a\u3044\u3002<\/p>\n<h4 id=\"surface-sensitivity\">\u8868\u9762\u611f\u5ea6<\/h4>\n<p>ATR\u306f\u672c\u8cea\u7684\u306b\u30b5\u30fc\u30d5\u30a7\u30b9\u6280\u8853\u3067\u3042\u308b\u3002\u3053\u308c\u306f\u8af8\u5203\u306e\u5263\u3067\u3042\u308b\u3002\u8868\u9762\u30b3\u30fc\u30c6\u30a3\u30f3\u30b0\u3001\u9178\u5316\u5c64\u3001\u307e\u305f\u306f\u6750\u6599\u306e\u8868\u9762\u5316\u5b66\u3092\u5206\u6790\u3057\u305f\u3044\u5834\u5408\u306b\u306f\u6700\u9069\u3067\u3059\u3002\u3057\u304b\u3057\u3001\u8868\u9762\u304c\u30d0\u30eb\u30af\u6750\u6599\u3092\u4ee3\u8868\u3059\u308b\u3082\u306e\u3067\u306a\u3044\u5834\u5408\uff08\u6c5a\u67d3\u3055\u308c\u3066\u3044\u305f\u308a\u3001\u7d44\u6210\u304c\u7570\u306a\u308b\u306a\u3069\uff09\u3001ATR\u30b9\u30da\u30af\u30c8\u30eb\u306f\u8aa4\u89e3\u3092\u62db\u304d\u307e\u3059\u3002\u30d0\u30eb\u30af\u5206\u6790\u306b\u306f\u3001KBr\u30da\u30ec\u30c3\u30c8\u306e\u3088\u3046\u306a\u900f\u904e\u6cd5\u304c\u3088\u308a\u9069\u5207\u304b\u3082\u3057\u308c\u306a\u3044\u3002<\/p>\n<h4 id=\"potential-issues\">\u6f5c\u5728\u7684\u306a\u554f\u984c<\/h4>\n<ul>\n<li><strong>\u30b3\u30f3\u30bf\u30af\u30c8\u304c\u60aa\u3044\uff1a<\/strong> \u524d\u8ff0\u306e\u3088\u3046\u306b\u3001\u3053\u308c\u306f\u56fa\u4f53\u306eATR\u30b9\u30da\u30af\u30c8\u30eb\u3092\u60aa\u304f\u3059\u308b\u6700\u5927\u306e\u539f\u56e0\u3067\u3042\u308b\u3002\u89e3\u6c7a\u7b56\u3068\u3057\u3066\u306f\u3001\u3082\u3063\u3068\u5727\u529b\u3092\u304b\u3051\u308b\u304b\u3001\u8a66\u6599\u304c\u975e\u5e38\u306b\u786c\u304f\u3066\u4e0d\u898f\u5247\u306a\u5834\u5408\u306f\u3001\u6700\u521d\u306b\u7c89\u7815\u3057\u3066\u63a5\u89e6\u3092\u3088\u304f\u3059\u308b\u3053\u3068\u3067\u3042\u308b\u3002<\/li>\n<li><strong>\u30af\u30ea\u30b9\u30bf\u30eb\u306e\u30c0\u30e1\u30fc\u30b8<\/strong> \u975e\u5e38\u306b\u786c\u304f\u92ed\u5229\u306a\u8a66\u6599\u306b\u5727\u529b\u3092\u304b\u3051\u3059\u304e\u308b\u3068\u3001ZnSe\u306e\u3088\u3046\u306a\u67d4\u3089\u304b\u3044\u7d50\u6676\u306b\u50b7\u304c\u3064\u3044\u305f\u308a\u3001\u3072\u3073\u304c\u5165\u3063\u305f\u308a\u3059\u308b\u3053\u3068\u304c\u3042\u308b\u3002\u305d\u306e\u305f\u3081\u3001\u672a\u77e5\u306e\u56fa\u4f53\u3084\u786c\u3044\u56fa\u4f53\u306b\u306f\u30c0\u30a4\u30e4\u30e2\u30f3\u30c9\u304c\u597d\u307e\u308c\u308b\u3053\u3068\u304c\u591a\u3044\u306e\u3067\u3059\u3002<\/li>\n<li><strong>\u6d78\u900f\u6df1\u5ea6\u306e\u5909\u5316\uff1a<\/strong> \u30a8\u30d0\u30cd\u30c3\u30bb\u30f3\u30c8\u6ce2\u306e\u4fb5\u5165\u6df1\u3055\u306f\u3001\u5149\u306e\u6ce2\u9577\u3001\u7d50\u6676\u3068\u8a66\u6599\u306e\u5c48\u6298\u7387\u3001\u5165\u5c04\u89d2\u306b\u4f9d\u5b58\u3059\u308b\u3002\u6df1\u3055\u306f\u6ce2\u9577\u304c\u9577\u3044\u307b\u3069\uff08\u6ce2\u6570\u304c\u4f4e\u3044\u307b\u3069\uff09\u5927\u304d\u304f\u306a\u308a\u307e\u3059\u3002\u3053\u306e\u305f\u3081\u3001\u30b9\u30da\u30af\u30c8\u30eb\u306e\u4f4e\u6ce2\u6570\u5074\u306b\u3042\u308b\u30d4\u30fc\u30af\u306e\u76f8\u5bfe\u5f37\u5ea6\u304c\u3001\u900f\u904e\u30b9\u30da\u30af\u30c8\u30eb\u3068\u6bd4\u8f03\u3057\u3066\u308f\u305a\u304b\u306b\u5f37\u304f\u898b\u3048\u308b\u3053\u3068\u304c\u3042\u308a\u307e\u3059\uff08Griffiths &amp; de Haseth, 2007\uff09\u3002\u9ad8\u5ea6\u306a\u30bd\u30d5\u30c8\u30a6\u30a7\u30a2\u3067\u306f\u3001\u3053\u306e\u5f71\u97ff\u306b\u5bfe\u3059\u308b\u88dc\u6b63\u3092\u9069\u7528\u3067\u304d\u308b\u3053\u3068\u304c\u591a\u3044\u3002<\/li>\n<\/ul>\n<table class=\"mce-item-table\" style=\"width:100%; border-collapse: collapse;\" border=\"1\">\n<thead>\n<tr>\n<th style=\"text-align:left;\">\u7279\u5fb4<\/th>\n<th style=\"text-align:left;\">\u900f\u904e\u6cd5\uff08KBr\/Mull\uff09<\/th>\n<th style=\"text-align:left;\">\u6e1b\u8870\u5168\u53cd\u5c04\u7387\uff08ATR\uff09<\/th>\n<\/tr>\n<\/thead>\n<tbody>\n<tr>\n<td style=\"text-align:left;\"><strong>\u539f\u5247<\/strong><\/td>\n<td style=\"text-align:left;\">IR\u30d3\u30fc\u30e0\u304c\u30b5\u30f3\u30d7\u30eb\u3092\u901a\u904e\u3059\u308b\u3002<\/td>\n<td style=\"text-align:left;\">IR\u30d3\u30fc\u30e0\u306f\u30a8\u30d0\u30cd\u30c3\u30bb\u30f3\u30c8\u6ce2\u3092\u4ecb\u3057\u3066\u8868\u9762\u3068\u76f8\u4e92\u4f5c\u7528\u3059\u308b\u3002<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u30b5\u30f3\u30d7\u30eb\u306e\u6e96\u5099<\/strong><\/td>\n<td style=\"text-align:left;\">\u5e83\u7bc4\u56f2\uff08\u7c89\u7815\u3001\u6df7\u5408\u3001\u5727\u643e\uff0f\u6563\u5e03\uff09\u3002<\/td>\n<td style=\"text-align:left;\">\u6700\u5c0f\u9650\uff08\u30b5\u30f3\u30d7\u30eb\u3092\u7d50\u6676\u306e\u4e0a\u306b\u7f6e\u304d\u3001\u5727\u529b\u3092\u52a0\u3048\u308b\uff09\u3002<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u5206\u6790\u6642\u9593<\/strong><\/td>\n<td style=\"text-align:left;\">\u30b5\u30f3\u30d7\u30eb\u3042\u305f\u308a5\uff5e15\u5206\u3002<\/td>\n<td style=\"text-align:left;\">&lt; \u30b5\u30f3\u30d7\u30eb\u3042\u305f\u308a1\u5206\u672a\u6e80<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u5206\u6790\u306e\u7a2e\u985e<\/strong><\/td>\n<td style=\"text-align:left;\">\u30d0\u30eb\u30af\u5206\u6790\u3002<\/td>\n<td style=\"text-align:left;\">\u8868\u9762\u5206\u6790\uff08\u6df1\u30550.5\uff5e2\u03bcm\uff09\u3002<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u7834\u58ca\u7684\uff1f<\/strong><\/td>\n<td style=\"text-align:left;\">\u306f\u3044\uff08\u30b5\u30f3\u30d7\u30eb\u306f\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u3068\u6df7\u3056\u308a\u3001\u56de\u53ce\u3067\u304d\u306a\u3044\u3053\u3068\u304c\u591a\u3044\uff09\u3002<\/td>\n<td style=\"text-align:left;\">\u307b\u3068\u3093\u3069\u975e\u7834\u58ca\uff08\u30b5\u30f3\u30d7\u30eb\u306f\u56de\u53ce\u53ef\u80fd\uff09\u3002<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u3088\u304f\u3042\u308b\u554f\u984c<\/strong><\/td>\n<td style=\"text-align:left;\">\u5149\u6563\u4e71\u3001\u6c34\u6c5a\u67d3\u3001\u5727\u529b\u52b9\u679c\u3002<\/td>\n<td style=\"text-align:left;\">\u8a66\u6599\u3068\u7d50\u6676\u306e\u63a5\u89e6\u4e0d\u826f\u3001\u8868\u9762\u306e\u6c5a\u67d3\u3001\u7d50\u6676\u306e\u640d\u50b7\u3002<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u6700\u9069<\/strong><\/td>\n<td style=\"text-align:left;\">\u5747\u8cea\u306a\u8a66\u6599\u3001\u5b9a\u91cf\u5206\u6790\u3001\u30d0\u30eb\u30af\u7d44\u6210\u304c\u5fc5\u8981\u306a\u5834\u5408\u3001\u53c2\u7167\u30e9\u30a4\u30d6\u30e9\u30ea\u30fc\u306e\u30b9\u30da\u30af\u30c8\u30eb\u53d6\u5f97\u3002<\/td>\n<td style=\"text-align:left;\">\u8fc5\u901f\u306a\u30b9\u30af\u30ea\u30fc\u30cb\u30f3\u30b0; \u54c1\u8cea\u7ba1\u7406; \u786c\u3044\/\u6697\u3044\/\u539a\u3044\u6750\u6599\u306e\u5206\u6790; \u8868\u9762\u5206\u6790; \u975e\u7834\u58ca\u691c\u67fb\u3002<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<h3 id=\"why-atr-is-often-the-first-choice-in-2025\">2025\u5e74\u3001ATR\u304c\u3057\u3070\u3057\u3070\u30d5\u30a1\u30fc\u30b9\u30c8\u30c1\u30e7\u30a4\u30b9\u3068\u306a\u308b\u7406\u7531<\/h3>\n<p>\u305d\u306e\u901f\u3055\u3001\u4f7f\u3044\u3084\u3059\u3055\u3001\u6c4e\u7528\u6027\u304b\u3089\u3001ATR\u306f\u81a8\u5927\u306a\u6570\u306e\u30a2\u30d7\u30ea\u30b1\u30fc\u30b7\u30e7\u30f3\u306e\u65e2\u5b9a\u306e\u624b\u6cd5\u3068\u306a\u3063\u3066\u3044\u308b\u3002ATR\u306fFTIR\u5206\u6790\u3092\u6c11\u4e3b\u5316\u3057\u3001\u5c02\u9580\u5bb6\u3067\u306a\u304f\u3066\u3082\u8cea\u306e\u9ad8\u3044\u30c7\u30fc\u30bf\u3092\u8fc5\u901f\u306b\u53d6\u5f97\u3067\u304d\u308b\u3088\u3046\u306b\u3057\u305f\u3002\u5de5\u696d\u7528QA\/QC\u3001\u79d1\u5b66\u635c\u67fb\u3001\u8fc5\u901f\u306a\u7269\u8cea\u540c\u5b9a\u306b\u3068\u3063\u3066\u3001\u305d\u306e\u5229\u70b9\u306f\u5426\u5b9a\u3067\u304d\u306a\u3044\u3002\u53e4\u5178\u7684\u306a\u900f\u904e\u6cd5\u306f\u3001\u7279\u5b9a\u306e\u7814\u7a76\u8ab2\u984c\u3084\u5fe0\u5b9f\u5ea6\u306e\u9ad8\u3044\u30e9\u30a4\u30d6\u30e9\u30ea\u30fc\u30fb\u30b9\u30da\u30af\u30c8\u30eb\u306e\u751f\u6210\u306e\u305f\u3081\u306b\u305d\u306e\u5730\u4f4d\u3092\u7dad\u6301\u3057\u3066\u3044\u308b\u304c\u3001ATR\u306e\u5229\u4fbf\u6027\u306f\u3001\u307b\u3068\u3093\u3069\u306e\u5206\u6790\u30e9\u30dc\u306b\u304a\u3051\u308b\u65e5\u3005\u306e\u30ef\u30fc\u30af\u30d5\u30ed\u30fc\u3092\u6839\u672c\u7684\u306b\u5909\u3048\u3066\u3044\u308b\u3002<\/p>\n<h2 id=\"choosing-the-right-path-a-decision-making-framework\">\u6b63\u3057\u3044\u9053\u3092\u9078\u3076\u610f\u601d\u6c7a\u5b9a\u306e\u30d5\u30ec\u30fc\u30e0\u30ef\u30fc\u30af<\/h2>\n<p>\u3053\u308c\u3067\u3042\u306a\u305f\u306e\u5206\u6790\u6b66\u5668\u306f3\u3064\u63c3\u3063\u305f\u3053\u3068\u306b\u306a\u308b\u3002\u554f\u984c\u306f\u3082\u306f\u3084\u3001\"IR\u5206\u6790\u7528\u306e\u56fa\u4f53\u8a66\u6599\u3092\u3069\u306e\u3088\u3046\u306b\u8abf\u88fd\u3059\u308b\u304b \"\u3067\u306f\u306a\u304f\u3001\"\u3053\u306e\u8a66\u6599\u3068\u3053\u306e\u8cea\u554f\u306b\u306f\u3001\u3069\u306e\u8abf\u88fd\u6cd5\u304c\u9069\u5207\u304b \"\u3067\u3042\u308b\u3002\u5341\u5206\u306a\u60c5\u5831\u306b\u57fa\u3065\u3044\u305f\u9078\u629e\u3092\u3059\u308b\u306b\u306f\u3001\u7269\u8cea\u306e\u7269\u7406\u7684\u30fb\u5316\u5b66\u7684\u6027\u8cea\u3068\u5206\u6790\u306e\u6700\u7d42\u76ee\u6a19\u306e\u4e21\u65b9\u3092\u8003\u616e\u3057\u3001\u719f\u8003\u3059\u308b\u5fc5\u8981\u304c\u3042\u308a\u307e\u3059\u3002\u305d\u308c\u306f\u3001\u30c4\u30fc\u30eb\u3092\u30bf\u30b9\u30af\u306b\u9069\u5408\u3055\u305b\u308b\u30d7\u30ed\u30bb\u30b9\u3067\u3042\u308b\u3002<\/p>\n<h3 id=\"considering-the-nature-of-your-sample\">\u30b5\u30f3\u30d7\u30eb\u306e\u6027\u8cea\u3092\u8003\u616e\u3059\u308b<\/h3>\n<p>\u30b5\u30f3\u30d7\u30eb\u305d\u306e\u3082\u306e\u304c\u3001\u3042\u306a\u305f\u306e\u624b\u3092\u5c0e\u304f\u3053\u3068\u304c\u591a\u3044\u3002\u305d\u306e\u7279\u6027\u306b\u3088\u3063\u3066\u3001\u3042\u308b\u65b9\u6cd5\u306f\u7406\u60f3\u7684\u3067\u3001\u5225\u306e\u65b9\u6cd5\u306f\u307e\u3063\u305f\u304f\u9069\u3055\u306a\u3044\u3053\u3068\u3082\u3042\u308b\u3002<\/p>\n<h4 id=\"physical-properties\">\u7269\u7406\u7684\u6027\u8cea<\/h4>\n<ul>\n<li><strong>\u786c\u5ea6\uff1a<\/strong> \u8a66\u6599\u306f\u3001\u77f3\u82f1\u306e\u3088\u3046\u306a\u786c\u3044\u7d50\u6676\u6027\u306e\u56fa\u4f53\u3067\u3059\u304b\u3001\u305d\u308c\u3068\u3082\u8edf\u3089\u304b\u3044\u30ef\u30c3\u30af\u30b9\u72b6\u306e\u7269\u8cea\u3067\u3059\u304b\uff1f\u975e\u5e38\u306b\u786c\u3044\u7269\u8cea\u306e\u5834\u5408\u3001\u826f\u597d\u306a\u63a5\u89e6\u306b\u5fc5\u8981\u306a\u5727\u529b\u306b\u8010\u3048\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u30c0\u30a4\u30e4\u30e2\u30f3\u30c9\u7d50\u6676\u3092\u4f7f\u3063\u305fATR\u304c\u6700\u9069\u3067\u3059\u3002\u3053\u306e\u3088\u3046\u306a\u6750\u6599\u3092KBr\u30da\u30ec\u30c3\u30c8\u7528\u306b\u7814\u78e8\u3059\u308b\u306e\u306f\u975e\u5e38\u306b\u56f0\u96e3\u3067\u3059\u3002\u9006\u306b\u3001\u975e\u5e38\u306b\u8edf\u3089\u304b\u304f\u3001\u53ef\u935b\u6027\u306e\u3042\u308b\u56fa\u4f53\u306e\u5834\u5408\u3001KBr\u30da\u30ec\u30c3\u30c8\u306f\u8a66\u6599\u304c\u7c89\u7815\u3055\u308c\u308b\u3088\u308a\u3082\u3080\u3057\u308d\u6c5a\u308c\u308b\u53ef\u80fd\u6027\u304c\u3042\u308b\u305f\u3081\u3001\u554f\u984c\u304c\u3042\u308b\u304b\u3082\u3057\u308c\u307e\u305b\u3093\u3002<\/li>\n<li><strong>\u30d5\u30a9\u30fc\u30e0<\/strong> \u3042\u306a\u305f\u306f\u5fae\u7c89\u672b\u3001\u56fa\u5f62\u584a\u3001\u30dd\u30ea\u30de\u30fc\u30d5\u30a3\u30eb\u30e0\u306e\u3069\u308c\u3092\u4f7f\u3063\u3066\u3044\u307e\u3059\u304b\uff1f\u7c89\u672b\u306f\u6c4e\u7528\u6027\u304c\u3042\u308a\u3001\u3069\u306e\u3088\u3046\u306a\u65b9\u6cd5\u306b\u3082\u4f7f\u7528\u3067\u304d\u307e\u3059\u3002\u56fa\u5f62\u584a\u306fATR\u306b\u306f\u6700\u9069\u3067\u3059\u304c\u3001Kbr\u30da\u30ec\u30c3\u30c8\u3084\u30de\u30eb\u3067\u306f\u307e\u305a\u5206\u89e3\u30fb\u7c89\u7815\u3057\u306a\u3051\u308c\u3070\u4e0d\u53ef\u80fd\u3067\u3059\u3002\u8584\u3044\u30dd\u30ea\u30de\u30fc\u30d5\u30a3\u30eb\u30e0\u306f\u3001\u539a\u3059\u304e\u306a\u3051\u308c\u3070\u3001\u524d\u51e6\u7406\u306a\u3057\u3067\u900f\u904e\u6cd5\u3067\u76f4\u63a5\u5206\u6790\u3067\u304d\u308b\u3053\u3068\u304c\u591a\u3044\u3002<\/li>\n<\/ul>\n<h4 id=\"chemical-properties\">\u5316\u5b66\u7684\u6027\u8cea<\/h4>\n<ul>\n<li><strong>\u5438\u6e7f\u6027\uff1a<\/strong> \u8a66\u6599\u306f\u5927\u6c17\u4e2d\u306e\u6c34\u5206\u3092\u5438\u53ce\u3057\u3084\u3059\u3044\u3067\u3059\u304b\uff1f\u3082\u3057\u305d\u3046\u306a\u3089\u3001KBr\u30da\u30ec\u30c3\u30c8\u6cd5\u306f\u5371\u967a\u3068\u96a3\u308a\u5408\u308f\u305b\u3067\u3059\u3002KBr\u306f\u305d\u308c\u81ea\u4f53\u304c\u5438\u6e7f\u6027\u3067\u3042\u308a\u3001\u6c34\u5206\u3092\u591a\u304f\u542b\u3080\u74b0\u5883\u3092\u4f5c\u308a\u51fa\u3057\u3001\u8a66\u6599\u3092\u5909\u8cea\u3055\u305b\u308b\u53ef\u80fd\u6027\u304c\u3042\u308b\u3002\u8a66\u6599\u3092\u4fdd\u8b77\u6cb9\u3067\u30b3\u30fc\u30c6\u30a3\u30f3\u30b0\u3059\u308bNujol\u30de\u30eb\u306e\u65b9\u304c\u306f\u308b\u304b\u306b\u5b89\u5168\u306a\u9078\u629e\u3067\u3042\u308b\u3002\u307e\u305f\u3001ATR\u306f\u5206\u6790\u304c\u975e\u5e38\u306b\u901f\u3044\u305f\u3081\u3001\u6c34\u5206\u3092\u5438\u53ce\u3059\u308b\u6642\u9593\u304c\u307b\u3068\u3093\u3069\u306a\u304f\u3001\u512a\u308c\u3066\u3044\u308b\u3002<\/li>\n<li><strong>\u53cd\u5fdc\u6027\uff1a<\/strong> \u8a66\u6599\u306f\u30cf\u30ed\u30b2\u30f3\u5316\u30a2\u30eb\u30ab\u30ea\u3068\u53cd\u5fdc\u3057\u307e\u3059\u304b\uff1f\u932f\u5869\u3084\u914d\u4f4d\u5316\u5408\u7269\u306e\u4e2d\u306b\u306fKBr\u3068\u30a4\u30aa\u30f3\u4ea4\u63db\u3092\u8d77\u3053\u3059\u3082\u306e\u304c\u3042\u308a\u307e\u3059\u3002 \u3053\u306e\u3088\u3046\u306a\u7591\u3044\u304c\u3042\u308b\u5834\u5408\u3001KBr\u30da\u30ec\u30c3\u30c8\u306f\u6709\u52b9\u306a\u9078\u629e\u80a2\u3067\u306f\u3042\u308a\u307e\u305b\u3093\u3002Nujol\u30de\u30eb\u306e\u4e0d\u6d3b\u6027\u30aa\u30a4\u30eb\u307e\u305f\u306fATR\u30b7\u30b9\u30c6\u30e0\u306e\u4e0d\u6d3b\u6027\u7d50\u6676\u304c\u5fc5\u8981\u3067\u3059\u3002<\/li>\n<li><strong>\u611f\u6e29\u6027\u307e\u305f\u306f\u611f\u5727\u6027\uff1a<\/strong> \u3042\u306a\u305f\u306e\u7269\u8cea\u306b\u306f\u65e2\u77e5\u306e\u591a\u5f62\u304c\u3042\u308a\u307e\u3059\u304b\uff1f\u591a\u5f62\u4f53\u306f\u540c\u3058\u7269\u8cea\u306e\u7570\u306a\u308b\u7d50\u6676\u5f62\u3067\u3042\u308a\u3001\u7570\u306a\u308bIR\u30b9\u30da\u30af\u30c8\u30eb\u3092\u6301\u3064\u3053\u3068\u304c\u3042\u308a\u307e\u3059\u3002KBr\u30d7\u30ec\u30b9\u306e\u9ad8\u5727\u529b\u306f\u3001\u3042\u308b\u591a\u5f62\u304b\u3089\u5225\u306e\u591a\u5f62\u3078\u306e\u5909\u5316\u3092\u5f15\u304d\u8d77\u3053\u3059\u53ef\u80fd\u6027\u304c\u3042\u308a\u307e\u3059(Giron, 2002)\u3002\u611f\u5727\u6750\u6599\u306e\u672c\u6765\u306e\u72b6\u614b\u3092\u5206\u6790\u3059\u308b\u5fc5\u8981\u304c\u3042\u308b\u5834\u5408\u306f\u3001\u30b8\u30a7\u30f3\u30c8\u30eb\u30de\u30eb\u6cd5\u304b\u30bc\u30ed\u30d7\u30ec\u30c3\u30b7\u30e3\u30fcATR\u3057\u304b\u3042\u308a\u307e\u305b\u3093\u3002<\/li>\n<\/ul>\n<h3 id=\"thinking-about-your-analytical-goal\">\u5206\u6790\u76ee\u6a19\u3092\u8003\u3048\u308b<\/h3>\n<p>\u3069\u306e\u3088\u3046\u306a\u8cea\u554f\u306b\u7b54\u3048\u3088\u3046\u3068\u3057\u3066\u3044\u307e\u3059\u304b\uff1f\u5206\u6790\u306e\u76ee\u7684\u306f\u3001\u30b5\u30f3\u30d7\u30eb\u306e\u6027\u8cea\u3068\u540c\u3058\u304f\u3089\u3044\u91cd\u8981\u3067\u3059\u3002<\/p>\n<h4 id=\"qualitative-vs-quantitative-analysis\">\u5b9a\u6027\u7684\u5206\u6790\u3068\u5b9a\u91cf\u7684\u5206\u6790<\/h4>\n<ul>\n<li><strong>\u5b9a\u6027\u7684\uff08\u8b58\u5225\uff09\uff1a<\/strong> \u5358\u306b\u6750\u6599\u3092\u7279\u5b9a\u3057\u305f\u308a\u3001\u8eab\u5143\u3092\u78ba\u8a8d\u3057\u305f\u3044\u3060\u3051\u306a\u306e\u3067\u3057\u3087\u3046\u304b\uff1f\u3053\u306e\u3088\u3046\u306a\u76ee\u7684\u306e\u5834\u5408\u3001\u30b9\u30d4\u30fc\u30c9\u3068\u624b\u8efd\u3055\u304c\u6700\u512a\u5148\u3055\u308c\u308b\u3053\u3068\u304c\u591a\u3044\u3002ATR\u306f\u3053\u306e\u5206\u91ce\u3067\u306f\u6587\u53e5\u306a\u3057\u306e\u30c1\u30e3\u30f3\u30d4\u30aa\u30f3\u3067\u3059\u3002\u8fc5\u901f\u306a\u30b9\u30da\u30af\u30c8\u30eb\u306f\u3001\u6570\u79d2\u3067\u30e9\u30a4\u30d6\u30e9\u30ea\u30fc\u3068\u7167\u5408\u3067\u304d\u307e\u3059\u3002Nujol mull\u3082\u307e\u305f\u3001\u8fc5\u901f\u306a\u5b9a\u6027\u30c1\u30a7\u30c3\u30af\u306b\u9069\u3057\u3066\u3044\u308b\u3002<\/li>\n<li><strong>\u5b9a\u91cf\u7684\uff08\u3069\u306e\u304f\u3089\u3044\uff1f\uff09<\/strong> \u6df7\u5408\u7269\u4e2d\u306e\u3042\u308b\u6210\u5206\u306e\u6fc3\u5ea6\u3092\u6e2c\u5b9a\u3057\u3088\u3046\u3068\u3057\u3066\u3044\u308b\u306e\u3067\u3059\u304b\uff1f\u3053\u308c\u306b\u306f\u3082\u3063\u3068\u53b3\u5bc6\u3055\u304c\u5fc5\u8981\u3067\u3059\u3002Beer&#039;s\u306e\u6cd5\u5247\u3067\u306f\u3001\u5438\u5149\u5ea6\u306f\u6fc3\u5ea6\u3068\u5149\u8def\u9577\u306b\u6bd4\u4f8b\u3059\u308b\u3002\u5b9a\u91cf\u7684\u306b\u6e2c\u5b9a\u3059\u308b\u305f\u3081\u306b\u306f\u3001\u5149\u8def\u9577\u304c\u4e00\u5b9a\u3067\u65e2\u77e5\u3067\u306a\u3051\u308c\u3070\u306a\u308a\u307e\u305b\u3093\u3002\u3053\u308c\u306f\u3001\u30de\u30eb\u3084ATR\u3067\u306f\u5b9f\u73fe\u304c\u96e3\u3057\u3044\u3053\u3068\u3067\u6709\u540d\u3067\u3042\u308b\u3002KBr\u30da\u30ec\u30c3\u30c8\u6cd5\u306f\u3001\u53b3\u5bc6\u306a\u4e00\u8cab\u6027\uff08\u540c\u3058\u8a66\u6599\u91cd\u91cf\u3001\u540c\u3058\u30da\u30ec\u30c3\u30c8\u306e\u539a\u3055\uff09\u3067\u884c\u3048\u3070\u3001\u826f\u597d\u306a\u5b9a\u91cf\u7d50\u679c\u3092\u5f97\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002\u6700\u3082\u6b63\u78ba\u306a\u5b9a\u91cf\u3092\u884c\u3046\u306b\u306f\u3001\u30d5\u30a3\u30eb\u30e0\u3084\u6db2\u4f53\u7528\u306e\u7279\u6b8a\u306a\u900f\u904e\u30bb\u30eb\u3092\u4f7f\u7528\u3059\u308b\u306e\u304c\u4e00\u822c\u7684\u3067\u3059\u3002<\/li>\n<\/ul>\n<h4 id=\"bulk-vs-surface-analysis\">\u30d0\u30eb\u30af\u5206\u6790\u3068\u8868\u9762\u5206\u6790<\/h4>\n<p>\u3053\u308c\u304c\u6700\u3082\u660e\u78ba\u306a\u5206\u304b\u308c\u76ee\u3060\u308d\u3046\u3002<\/p>\n<ul>\n<li><strong>\u30d0\u30eb\u30af\u5206\u6790\uff1a<\/strong> \u6750\u6599\u306e\u5168\u4f53\u7684\u306a\u7d44\u6210\u3092\u77e5\u308b\u5fc5\u8981\u304c\u3042\u308b\u5834\u5408\u306f\u3001\u30d0\u30eb\u30af\u3092\u30b5\u30f3\u30d7\u30ea\u30f3\u30b0\u3059\u308b\u6280\u6cd5\u304c\u5fc5\u8981\u3067\u3059\u3002KBr\u30da\u30ec\u30c3\u30c8\u6cd5\u306f\u3001\u6750\u6599\u306e\u4ee3\u8868\u30b5\u30f3\u30d7\u30eb\u3092\u7c89\u7815\u3057\u3066\u5747\u8cea\u5316\u3059\u308b\u305f\u3081\u3001\u3053\u306e\u305f\u3081\u306e\u30b4\u30fc\u30eb\u30c9\u30b9\u30bf\u30f3\u30c0\u30fc\u30c9\u3067\u3059\u3002Nujol mull\u3082\u30d0\u30eb\u30af\u60c5\u5831\u3092\u63d0\u4f9b\u3057\u307e\u3059\u3002<\/li>\n<li><strong>\u8868\u9762\u5206\u6790\uff1a<\/strong> \u30b3\u30fc\u30c6\u30a3\u30f3\u30b0\u3001\u8868\u9762\u51e6\u7406\u3001\u9178\u5316\u5c64\u3001\u3042\u308b\u3044\u306f\u8868\u9762\u306e\u6c5a\u67d3\u7269\u8cea\u306b\u8208\u5473\u304c\u3042\u308b\u306a\u3089\u3001ATR\u306f\u6700\u9069\u306a\u30c4\u30fc\u30eb\u3067\u3059\u3002\u6d78\u900f\u6df1\u5ea6\u304c\u6d45\u3044\u305f\u3081\u3001\u6750\u6599\u306e\u4e0a\u90e8\u6570\u30df\u30af\u30ed\u30f3\u3057\u304b\u898b\u3048\u305a\u3001\u305d\u306e\u4e0b\u306e\u5927\u90e8\u5206\u306f\u7121\u8996\u3055\u308c\u307e\u3059\u3002\u3053\u3053\u3067KBr\u30da\u30ec\u30c3\u30c8\u3092\u4f7f\u7528\u3059\u308b\u306e\u306f\u9593\u9055\u3044\u3067\u3042\u308b\u3002\u8868\u9762\u5c64\u3092\u524a\u308a\u53d6\u308a\u3001\u30d0\u30eb\u30af\u6750\u6599\u3067\u5e0c\u91c8\u3057\u3066\u3057\u307e\u3046\u305f\u3081\u3001\u6c42\u3081\u308b\u60c5\u5831\u305d\u306e\u3082\u306e\u304c\u5931\u308f\u308c\u3066\u3057\u307e\u3046\u3002<\/li>\n<\/ul>\n<h3 id=\"the-role-of-advanced-ftir-pre-processing-sample-preparation-tools\">\u9ad8\u5ea6\u306aFTIR\u524d\u51e6\u7406\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u30c4\u30fc\u30eb\u306e\u5f79\u5272<\/h3>\n<p>\u7279\u306b\u53e4\u5178\u7684\u306a\u900f\u904e\u6cd5\u3067\u306f\u3001\u9069\u5207\u306a\u5668\u5177\u3092\u4f7f\u7528\u3059\u308b\u3053\u3068\u3067\u8abf\u88fd\u306e\u8cea\u304c\u5927\u5e45\u306b\u5411\u4e0a\u3059\u308b\u3002\u30b7\u30f3\u30d7\u30eb\u306a\u30e1\u30ce\u30a6\u88fd\u306e\u4e73\u9262\u3068\u4e73\u68d2\u306f\u6642\u4ee3\u3092\u8d85\u8d8a\u3057\u305f\u3082\u306e\u3060\u304c\u3001\u73fe\u4ee3\u306e\u7814\u7a76\u5ba4\u3067\u306f\u3001\u4e00\u8cab\u6027\u3068\u52b9\u7387\u6027\u3092\u8ffd\u6c42\u3057\u305f\u9053\u5177\u306e\u6069\u6075\u3092\u53d7\u3051\u3066\u3044\u308b\u3002\u5727\u529b\u8a08\u3092\u5099\u3048\u305f\u9ad8\u54c1\u8cea\u306e\u6cb9\u5727\u30d7\u30ec\u30b9\u306f\u3001\u518d\u73fe\u6027\u306e\u3042\u308b\u30da\u30ec\u30c3\u30c8\u5316\u3092\u53ef\u80fd\u306b\u3059\u308b\u3002\u30e2\u30fc\u30bf\u30fc\u99c6\u52d5\u306e\u7c89\u7815\u6a5f\u3084\u30a6\u30a3\u30c3\u30b0\u30fb\u30eb\u30d0\u30b0\u5f0f\u52a0\u632f\u5668\u306f\u3001\u7c89\u7815\u30d7\u30ed\u30bb\u30b9\u3092\u81ea\u52d5\u5316\u3057\u3001\u4e00\u8cab\u3057\u305f\u5fae\u7c92\u5b50\u30b5\u30a4\u30ba\u3068\u512a\u308c\u305f\u5747\u8cea\u6027\u3092\u4fdd\u8a3c\u3057\u307e\u3059\u3002ATR\u3067\u306f\u3001\u6821\u6b63\u3055\u308c\u305f\u5727\u529b\u30af\u30e9\u30f3\u30d7\u3092\u5099\u3048\u305f\u30a2\u30af\u30bb\u30b5\u30ea\u30fc\u304c\u3001\u5341\u5206\u306a\u63a5\u89e6\u3068\u518d\u73fe\u6027\u3092\u4fdd\u8a3c\u3057\u307e\u3059\u3002\u3053\u308c\u3089\u3078\u306e\u6295\u8cc7 <a href=\"https:\/\/www.hcftir.com\/ir-sample-preparation-category\/\" rel=\"nofollow\">\u9ad8\u5ea6\u306aFTIR\u524d\u51e6\u7406\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u30c4\u30fc\u30eb<\/a> \u79d1\u5b66\u306f\u5de5\u82b8\u54c1\u304b\u3089\u518d\u73fe\u53ef\u80fd\u306a\u6280\u8853\u7684\u624b\u9806\u3078\u3068\u6607\u83ef\u3057\u3001\u3070\u3089\u3064\u304d\u3092\u6700\u5c0f\u9650\u306b\u6291\u3048\u3001\u7570\u306a\u308b\u30e6\u30fc\u30b6\u30fc\u3084\u7570\u306a\u308b\u65e5\u306b\u308f\u305f\u3063\u3066\u3088\u308a\u4fe1\u983c\u6027\u306e\u9ad8\u3044\u30c7\u30fc\u30bf\u3092\u5f97\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002<\/p>\n<h2 id=\"frequently-asked-questions-faq\">\u3088\u304f\u3042\u308b\u8cea\u554f\uff08FAQ\uff09<\/h2>\n<p><strong>KBr\u30da\u30ec\u30c3\u30c8\u306e\u30b9\u30da\u30af\u30c8\u30eb\u3067\u30013400cm-\u00b9\u4ed8\u8fd1\u306b\u30d6\u30ed\u30fc\u30c9\u3067\u919c\u3044\u30d4\u30fc\u30af\u304c\u3042\u308b\u306e\u306f\u306a\u305c\u3067\u3059\u304b\uff1f<\/strong> \u3053\u308c\u306f\u6c34\u306e\u6df7\u5165\u306e\u5178\u578b\u7684\u306a\u30b5\u30a4\u30f3\u3067\u3042\u308b\u3002\u30d6\u30ed\u30fc\u30c9\u306a\u30d4\u30fc\u30af\u306f\u3001H\u2082O\u5206\u5b50\u306eO-H\u4f38\u7e2e\u632f\u52d5\u3067\u3042\u308b\u3002\u5438\u6e7f\u6027\u306e\u3042\u308bKBr\u7c89\u672b\u307e\u305f\u306f\u8a66\u6599\u81ea\u4f53\u306b\u5438\u53ce\u3055\u308c\u305f\u6c34\u5206\u306b\u7531\u6765\u3059\u308b\u3002\u3053\u308c\u3092\u907f\u3051\u308b\u306b\u306f\u3001\u4f7f\u7528\u524d\u306bKBr\u3092\u30aa\u30fc\u30d6\u30f3\u3067\u5341\u5206\u306b\u4e7e\u71e5\u3055\u305b\u3001\u30c7\u30b7\u30b1\u30fc\u30bf\u30fc\u3067\u4fdd\u7ba1\u3057\u3001\u3067\u304d\u308b\u3060\u3051\u65e9\u304f\u30da\u30ec\u30c3\u30c8\u3092\u6e96\u5099\u3059\u308b\u3002<\/p>\n<p><strong>\u79c1\u306eATR\u30b9\u30da\u30af\u30c8\u30eb\u306f\u975e\u5e38\u306b\u5f31\u304f\u3001\u30ce\u30a4\u30ba\u304c\u591a\u3044\u3002\u4f55\u304c\u4e00\u756a\u554f\u984c\u306a\u306e\u3067\u3057\u3087\u3046\u304b\uff1f<\/strong> \u56fa\u4f53\u8a66\u6599\u3067ATR\u4fe1\u53f7\u304c\u5f31\u304f\u306a\u308b\u6700\u3082\u4e00\u822c\u7684\u306a\u539f\u56e0\u306f\u3001\u8a66\u6599\u3068ATR\u7d50\u6676\u306e\u63a5\u89e6\u4e0d\u826f\u3067\u3042\u308b\u3002\u30a8\u30d0\u30cd\u30c3\u30bb\u30f3\u30c8\u6ce2\u306f\u6570\u30df\u30af\u30ed\u30f3\u7a0b\u5ea6\u3057\u304b\u900f\u904e\u3057\u306a\u3044\u305f\u3081\u3001\u5bc6\u7740\u306f\u8b72\u308c\u307e\u305b\u3093\u3002\u30a2\u30f3\u30d3\u30eb\u3067\u3055\u3089\u306b\u5727\u529b\u3092\u304b\u3051\u3066\u307f\u3066\u304f\u3060\u3055\u3044\u3002\u8a66\u6599\u304c\u975e\u5e38\u306b\u786c\u304b\u3063\u305f\u308a\u3001\u8868\u9762\u304c\u4e0d\u898f\u5247\u306a\u5834\u5408\u306f\u3001\u7d50\u6676\u306e\u4e0a\u306b\u7f6e\u304f\u524d\u306b\u8a66\u6599\u3092\u7d30\u304b\u304f\u7c89\u7815\u3059\u308b\u3068\u3001\u63a5\u89e6\u9762\u7a4d\u3068\u4fe1\u53f7\u5f37\u5ea6\u304c\u5287\u7684\u306b\u6539\u5584\u3055\u308c\u307e\u3059\u3002<\/p>\n<p><strong>\u30e0\u30ea\u30f3\u30b0\u5264\u306f\u30cc\u30b8\u30e7\u30fc\u30eb\u3060\u3051\u3067\u3059\u304b\uff1fC-H\u9818\u57df\u3092\u898b\u308b\u5fc5\u8981\u304c\u3042\u308b\u5834\u5408\u306f\uff1f<\/strong> \u30cc\u30b8\u30e7\u30fc\u30eb\u306f\u6700\u3082\u4e00\u822c\u7684\u306a\u30de\u30ea\u30f3\u30b0\u5264\u3067\u3059\u304c\u3001\u30cc\u30b8\u30e7\u30fc\u30eb\u306eC-H\u30d4\u30fc\u30af\u306f3000-2850 cm-\u00b9\u304a\u3088\u30731460-1375 cm-\u00b9\u9818\u57df\u3092\u4e0d\u660e\u77ad\u306b\u3057\u307e\u3059\u3002\u3053\u306e\u9818\u57df\u304c\u5206\u6790\u306b\u91cd\u8981\u306a\u5834\u5408\u306f\u3001Fluorolube\uff08\u30d1\u30fc\u30d5\u30eb\u30aa\u30ed\u70ad\u5316\u6c34\u7d20\uff09\u306e\u3088\u3046\u306a\u88dc\u5b8c\u7684\u306a\u30de\u30ea\u30f3\u30b0\u5264\u3092\u4f7f\u7528\u3059\u308b\u5fc5\u8981\u304c\u3042\u308a\u307e\u3059\u3002Fluorolube\u306fC-H\u9818\u57df\u3067\u306f\u900f\u660e\u3067\u3059\u304c\u30011300 cm-\u00b9\u4ee5\u4e0b\u3067\u306f\u5f37\u3044\u5438\u53ce\u304c\u3042\u308a\u307e\u3059\u3002\u8a66\u6599\u306e\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5b8c\u5168\u306b\u628a\u63e1\u3059\u308b\u305f\u3081\u306b\u306f\u3001Nujol\u3068Fluorolube\u306e2\u7a2e\u985e\u306e\u30b9\u30da\u30af\u30c8\u30eb\u3092\u6e2c\u5b9a\u3059\u308b\u306e\u304c\u30d9\u30b9\u30c8\u3067\u3059\u3002<\/p>\n<p><strong>\u30e1\u30ce\u30a6\u306e\u4e73\u9262\u3068\u4e73\u68d2\u3092\u30b5\u30f3\u30d7\u30eb\u3068\u30b5\u30f3\u30d7\u30eb\u306e\u9593\u306b\u9069\u5207\u306b\u6d17\u6d44\u3059\u308b\u306b\u306f\uff1f<\/strong> \u4e8c\u6b21\u6c5a\u67d3\u3092\u9632\u3050\u306b\u306f\u3001\u5165\u5ff5\u306a\u6e05\u6383\u304c\u6b20\u304b\u305b\u306a\u3044\u3002\u307e\u305a\u3001\u4e7e\u3044\u305f\u5e03\u304b\u30da\u30fc\u30d1\u30fc\u30bf\u30aa\u30eb\u3067\u3067\u304d\u308b\u3060\u3051\u6b8b\u7559\u7269\u3092\u62ed\u304d\u53d6\u308b\u3002\u6b21\u306b\u3001\u5c11\u91cf\u306e\u6e05\u6f54\u306a\u7814\u78e8\u5264\uff08\u5206\u5149\u5b66\u30b0\u30ec\u30fc\u30c9\u306eKBr\u307e\u305f\u306fNaCl\u304c\u52b9\u679c\u7684\uff09\u3092\u4e73\u9262\u306b\u5165\u308c\u30011\u5206\u9593\u3059\u308a\u6f70\u3059\u3002\u3053\u308c\u3067\u8868\u9762\u3092\u300c\u3053\u3059\u308b\u300d\u3002\u3053\u306e\u30af\u30ea\u30fc\u30cb\u30f3\u30b0\u30d1\u30a6\u30c0\u30fc\u306f\u6368\u3066\u308b\u3002\u5fc5\u8981\u306b\u5fdc\u3058\u3066\u7e70\u308a\u8fd4\u3057\u884c\u3046\u3002\u9811\u56fa\u306a\u6b8b\u7559\u7269\u306e\u5834\u5408\u306f\u3001\u6eb6\u5264\u6d17\u6d44\uff08\u30a2\u30bb\u30c8\u30f3\u307e\u305f\u306f\u30a4\u30bd\u30d7\u30ed\u30d1\u30ce\u30fc\u30eb\uff09\u3092\u884c\u3044\u3001\u305d\u306e\u5f8c\u5341\u5206\u306b\u4e7e\u71e5\u3055\u305b\u308b\u5fc5\u8981\u304c\u3042\u308b\u3002\u6c5a\u67d3\u3055\u308c\u305f\u4e73\u9262\u306f\u7d76\u5bfe\u306b\u4f7f\u7528\u3057\u306a\u3044\u3067\u304f\u3060\u3055\u3044\u3002<\/p>\n<p><strong>KBr\u30da\u30ec\u30c3\u30c8\u306f\u518d\u5229\u7528\u3067\u304d\u307e\u3059\u304b\uff1f<\/strong> \u6280\u8853\u7684\u306b\u306f\u305d\u3046\u3067\u3059\u304c\u3001\u4e00\u822c\u7684\u306b\u306f\u826f\u3044\u3084\u308a\u65b9\u3067\u306f\u3042\u308a\u307e\u305b\u3093\u3002\u4e00\u5ea6\u5927\u6c17\u306b\u3055\u3089\u3055\u308c\u308b\u3068\u3001\u30da\u30ec\u30c3\u30c8\u306f\u6e7f\u6c17\u3092\u5438\u53ce\u3057\u59cb\u3081\u3001\u6642\u9593\u306e\u7d4c\u904e\u3068\u3068\u3082\u306b\u30b9\u30da\u30af\u30c8\u30eb\u3092\u52a3\u5316\u3055\u305b\u307e\u3059\u3002\u3069\u3046\u3057\u3066\u3082\u4fdd\u7ba1\u3057\u305f\u3044\u5834\u5408\u306f\u3001\u30c7\u30b7\u30b1\u30fc\u30bf\u30fc\u306b\u5165\u308c\u3066\u304f\u3060\u3055\u3044\u3002\u53b3\u5bc6\u306a\u4f5c\u696d\u3084\u5b9a\u91cf\u4f5c\u696d\u3067\u306f\u3001\u518d\u73fe\u6027\u3092\u78ba\u4fdd\u3059\u308b\u305f\u3081\u3001\u5206\u6790\u3054\u3068\u306b\u65b0\u9bae\u306a\u30da\u30ec\u30c3\u30c8\u3092\u6e96\u5099\u3059\u308b\u5fc5\u8981\u304c\u3042\u308a\u307e\u3059\u3002<\/p>\n<p><strong>\u30af\u30ea\u30b9\u30c1\u30e3\u30f3\u30bb\u30f3\u52b9\u679c\u3068\u306f\u4f55\u3067\u3059\u304b\uff1f<\/strong> Christiansen\u52b9\u679c\u3068\u306f\u3001\u5a92\u4f53\u4e2d\u306b\u6d6e\u904a\u3059\u308b\u7c92\u5b50\uff08Nujol mull\u306a\u3069\uff09\u306e\u900f\u904e\u30b9\u30da\u30af\u30c8\u30eb\u306b\u73fe\u308c\u308b\u30b9\u30da\u30af\u30c8\u30eb\u30a2\u30fc\u30c1\u30d5\u30a1\u30af\u30c8\u3002\u6b6a\u3093\u3060\u975e\u5bfe\u79f0\u306e\u30d4\u30fc\u30af\u5f62\u72b6\u3068\u50be\u659c\u3057\u305f\u30d9\u30fc\u30b9\u30e9\u30a4\u30f3\u3092\u5f15\u304d\u8d77\u3053\u3057\u307e\u3059\u3002\u3053\u308c\u306f\u3001\u7c92\u5b50\u3068\u5a92\u8cea\u306e\u5c48\u6298\u7387\u304c\u3042\u308b\u6ce2\u9577\u3067\u306f\u4e00\u81f4\u3059\u308b\u304c\u3001\u4ed6\u306e\u6ce2\u9577\u3067\u306f\u4e00\u81f4\u3057\u306a\u3044\u305f\u3081\u3001\u5909\u52d5\u6563\u4e71\u3092\u5f15\u304d\u8d77\u3053\u3059\u305f\u3081\u306b\u767a\u751f\u3057\u307e\u3059\u3002\u3053\u308c\u3092\u6700\u5c0f\u9650\u306b\u6291\u3048\u308b\u6700\u5584\u306e\u65b9\u6cd5\u306f\u3001\u30b5\u30f3\u30d7\u30eb\u3092\u53ef\u80fd\u306a\u9650\u308a\u5c0f\u3055\u306a\u7c92\u5b50\u5f84\uff08\u7406\u60f3\u7684\u306b\u306f2 \u00b5m\u672a\u6e80\uff09\u306b\u7c89\u7815\u3059\u308b\u3053\u3068\u3067\u3059\u3002<\/p>\n<p><strong>ATR\u3092\u4f7f\u3063\u3066\u5b9a\u91cf\u5206\u6790\u306f\u3067\u304d\u307e\u3059\u304b\uff1f<\/strong> ATR\u306b\u3088\u308b\u5b9a\u91cf\u5206\u6790\u306f\u53ef\u80fd\u3067\u3042\u308b\u304c\u3001\u900f\u904e\u6cd5\u3088\u308a\u3082\u8907\u96d1\u3067\u3042\u308b\u3002\u6709\u52b9\u5149\u8def\u9577\u306f\u3001\u6ce2\u9577\u3084\u7d50\u6676\u3068\u8a66\u6599\u306e\u5c48\u6298\u7387\u306a\u3069\u3001\u3044\u304f\u3064\u304b\u306e\u5909\u6570\u306b\u4f9d\u5b58\u3059\u308b\u3002\u3057\u304b\u3057\u3001\u4e0e\u3048\u3089\u308c\u305f\u30b5\u30f3\u30d7\u30eb\u30bf\u30a4\u30d7\u306b\u3064\u3044\u3066\u3001\u5727\u529b\u304c\u4e00\u5b9a\u306b\u52a0\u3048\u3089\u308c\u3001\u8868\u9762\u304c\u5747\u4e00\u3067\u3042\u308c\u3070\u3001ATR\u30b7\u30b0\u30ca\u30eb\u306f\u6fc3\u5ea6\u306b\u6bd4\u4f8b\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002\u6fc3\u5ea6\u65e2\u77e5\u306e\u6a19\u6e96\u8a66\u6599\u3092\u7528\u3044\u305f\u614e\u91cd\u306a\u6821\u6b63\u304c\u5fc5\u8981\u3067\u3042\u308a\u3001\u5fae\u91cf\u6210\u5206\u306e\u6e2c\u5b9a\u3084\u4e00\u8cab\u6027\u306e\u3042\u308b\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u306e\u5909\u5316\u306b\u6700\u3082\u4fe1\u983c\u6027\u304c\u9ad8\u3044\u3002<\/p>\n<h2 id=\"conclusion\">\u7d50\u8ad6<\/h2>\n<p>\u56fa\u4f53\u7269\u8cea\u304b\u3089\u610f\u5473\u306e\u3042\u308b\u8d64\u5916\u30b9\u30da\u30af\u30c8\u30eb\u307e\u3067\u306e\u9053\u306e\u308a\u306f\u3001\u5316\u5b66\u8005\u306e\u82b8\u8853\u3068\u79d1\u5b66\u306e\u8a3c\u3067\u3042\u308b\u3002\u305d\u308c\u306f\u3001\u7c89\u7815\u3001\u6df7\u5408\u3001\u52a0\u5727\u3068\u3044\u3063\u305f\u5de8\u8996\u7684\u306a\u4f5c\u7528\u304c\u3001\u5fae\u8996\u7684\u3001\u5206\u5149\u5b66\u7684\u306a\u30ec\u30d9\u30eb\u3067\u91cd\u5927\u306a\u7d50\u679c\u3092\u3082\u305f\u3089\u3059\u30d7\u30ed\u30bb\u30b9\u3067\u3042\u308b\u3002IR\u5206\u6790\u7528\u306e\u56fa\u4f53\u8a66\u6599\u3092\u3069\u306e\u3088\u3046\u306b\u8abf\u88fd\u3059\u308b\u304b\u306b\u3064\u3044\u3066\u306f\u3001\u5358\u4e00\u306e\u300c\u30d9\u30b9\u30c8\u300d\u306a\u65b9\u6cd5\u306f\u5b58\u5728\u305b\u305a\u3001\u3080\u3057\u308d\u3001\u305d\u308c\u305e\u308c\u306e\u8ad6\u7406\u3068\u76ee\u7684\u3092\u3082\u3063\u305f\u3001\u3055\u307e\u3056\u307e\u306a\u9078\u629e\u80a2\u304c\u3042\u308b\u3053\u3068\u3092\u898b\u3066\u304d\u305f\u3002KBr\u30da\u30ec\u30c3\u30c8\u6cd5\u306f\u3001\u8981\u6c42\u304c\u9ad8\u304f\u6b63\u78ba\u3067\u3001\u9ad8\u5206\u89e3\u80fd\u306e\u30d0\u30eb\u30af\u5206\u6790\u3078\u306e\u9053\u3092\u63d0\u4f9b\u3059\u308b\u3002Nujol mull\u6cd5\u306f\u3001\u654f\u611f\u306a\u6750\u6599\u306b\u512a\u3057\u3044\u4ee3\u66ff\u6cd5\u3092\u63d0\u4f9b\u3057\u3001\u624b\u9806\u304c\u7c21\u5358\u306a\u4ee3\u308f\u308a\u306b\u30d5\u30eb\u30b9\u30da\u30af\u30c8\u30eb\u7a93\u3092\u63d0\u4f9b\u3059\u308b\u3002\u305d\u3057\u3066\u3001\u73fe\u4ee3\u306e\u30d1\u30ef\u30fc\u30cf\u30a6\u30b9\u3067\u3042\u308b\u6e1b\u8870\u5168\u53cd\u5c04\u6cd5\u306f\u3001\u8868\u9762\u5206\u6790\u306b\u6bd4\u985e\u306e\u306a\u3044\u30b9\u30d4\u30fc\u30c9\u3068\u5bb9\u6613\u3055\u3092\u63d0\u4f9b\u3057\u3001\u7121\u6570\u306e\u30e9\u30dc\u306e\u30ef\u30fc\u30af\u30d5\u30ed\u30fc\u3092\u518d\u5b9a\u7fa9\u3059\u308b\u3002<\/p>\n<p>\u3053\u308c\u3089\u306e\u624b\u6cd5\u306e\u4e2d\u304b\u3089\u8ce2\u304f\u9078\u629e\u3059\u308b\u3053\u3068\u306f\u3001\u7269\u8cea\u305d\u306e\u3082\u306e\u3068\u5bfe\u8a71\u3057\u3001\u305d\u306e\u7269\u7406\u7684\u30fb\u5316\u5b66\u7684\u6027\u8cea\u3092\u7406\u89e3\u3057\u3001\u5206\u6790\u610f\u56f3\u3068\u624b\u6cd5\u3092\u4e00\u81f4\u3055\u305b\u308b\u3053\u3068\u3067\u3042\u308b\u3002\u5341\u5206\u306b\u6e96\u5099\u3055\u308c\u305f\u8a66\u6599\u306f\u3001\u5206\u5149\u5b66\u7684\u767a\u898b\u306e\u7121\u8a00\u306e\u30d1\u30fc\u30c8\u30ca\u30fc\u3067\u3042\u308b\u3002\u305d\u308c\u306f\u3001\u4fe1\u983c\u3067\u304d\u308b\u30c7\u30fc\u30bf\u3092\u69cb\u7bc9\u3057\u3001\u305d\u3053\u304b\u3089\u660e\u78ba\u3067\u660e\u767d\u306a\u7d50\u8ad6\u3092\u5c0e\u304d\u51fa\u3059\u305f\u3081\u306e\u57fa\u790e\u3068\u306a\u308b\u3082\u306e\u3067\u3042\u308b\u3002\u3053\u306e\u3088\u3046\u306a\u8a66\u6599\u8abf\u88fd\u6280\u8853\u3092\u30de\u30b9\u30bf\u30fc\u3059\u308b\u3053\u3068\u306f\u3001\u524d\u6bb5\u968e\u306e\u96d1\u7528\u3067\u306f\u306a\u304f\u3001\u4e0d\u900f\u660e\u306a\u56fa\u4f53\u3092\u5206\u5b50\u6307\u7d0b\u3068\u3057\u3066\u660e\u3089\u304b\u306b\u3059\u308b\u305f\u3081\u306e\u5206\u6790\u30d7\u30ed\u30bb\u30b9\u306e\u4e0d\u53ef\u6b20\u306a\u90e8\u5206\u306a\u306e\u3067\u3042\u308b\u3002<\/p>\n<h2 id=\"references\">\u53c2\u8003\u6587\u732e<\/h2>\n<p>Christiansen, C. (1884).Untersuchungen \u00fcber die optischen Eigenschaften von fein vertheilten K\u00f6rpern.Annalen der Physik und Chemie, 259(10), 298-306. <a href=\"https:\/\/doi.org\/10.1002\/andp.18842591008\" rel=\"nofollow\">https:\/\/doi.org\/10.1002\/andp.18842591008<\/a><\/p>\n<p>Giron, D. (2002).\u71b1\u5206\u6790\u3092\u7528\u3044\u305f\u88fd\u85ac\u696d\u754c\u306b\u304a\u3051\u308b\u591a\u5f62\u304a\u3088\u3073\u64ec\u4f3c\u591a\u5f62\u306e\u8abf\u67fb\u3002\u71b1\u5206\u6790\u3068\u71b1\u91cf\u6e2c\u5b9a, 68(2), 359-382.<\/p>\n<p>Griffiths, P. R., &amp; de Haseth, J. A. (2007).Fourier transform infrared spectrometry (2nd ed.).Wiley-Interscience. <a href=\"https:\/\/doi.org\/10.1002\/0470106338\" rel=\"nofollow\">https:\/\/doi.org\/10.1002\/0470106338<\/a><\/p>\n<p>Pavia, D. L., Lampman, G. M., Kriz, G. S., &amp; Vyvyan, J. R. (2015).Introduction to spectroscopy (5th ed.).Cengage Learning.<\/p>\n<p>Thermo Fisher Scientific.(n.d.).ATR a-go-go: \u6e1b\u8870\u5168\u53cd\u5c04\u7387\u5165\u9580. <a href=\"https:\/\/assets.thermofisher.com\/TFS-Assets\/MSD\/Application-Notes\/AN50731-ATR-a-go-go-introduction-attenuated-total-reflectance.pdf\" rel=\"nofollow\">https:\/\/assets.thermofisher.com\/TFS-Assets\/MSD\/Application-Notes\/AN50731-ATR-a-go-go-introduction-attenuated-total-reflectance.pdf<\/a><\/p>","protected":false},"excerpt":{"rendered":"<p>\u8981\u65e8 \u56fa\u4f53\u8a66\u6599\u304b\u3089\u9ad8\u54c1\u8cea\u306e\u30d5\u30fc\u30ea\u30a8\u5909\u63db\u8d64\u5916\u5206\u5149\uff08FTIR\uff09\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5f97\u308b\u306b\u306f\u3001\u305d\u306e\u8a66\u6599\u8abf\u88fd\u306b\u3069\u306e\u3088\u3046\u306a\u65b9\u6cd5\u3092\u9078\u629e\u3059\u308b\u304b\u306b\u57fa\u672c\u7684\u306b\u4f9d\u5b58\u3059\u308b\u3002\u56fa\u4f53\u8a66\u6599\u306e\u7269\u7406\u7684\u72b6\u614b\u306b\u306f\u3001\u5149\u6563\u4e71\u3084\u4e0d\u5747\u4e00\u6027\u3068\u3044\u3063\u305f\u56fa\u6709\u306e\u8ab2\u984c\u304c\u3042\u308a\u3001\u3053\u308c\u304c\u6c42\u3081\u308b\u632f\u52d5\u60c5\u5831\u3092\u4e0d\u660e\u77ad\u306b\u3057\u305f\u308a\u6b6a\u3081\u305f\u308a\u3059\u308b\u3053\u3068\u304c\u3042\u308a\u307e\u3059\u3002\u3053\u306e\u8a18\u4e8b\u3067\u306f\u3001IR\u5206\u6790\u306e\u305f\u3081\u306b\u56fa\u4f53\u8a66\u6599\u3092\u8abf\u88fd\u3059\u308b\u65b9\u6cd5\u306b\u3064\u3044\u3066\u3001\u81ed\u5316\u30ab\u30ea\u30a6\u30e0\uff08KBr\uff09\u30da\u30ec\u30c3\u30c8\u6cd5\u3001Nujol mull\u6cd5\u3001\u304a\u3088\u3073\u6e1b\u8870\u5168\u53cd\u5c04\uff08ATR\uff09\u5206\u5149\u6cd5\u306e3\u3064\u306e\u4e3b\u8981\u306a\u624b\u6cd5\u3092\u5305\u62ec\u7684\u306b\u691c\u8a0e\u3057\u307e\u3059\u3002\u5404\u624b\u6cd5\u306f\u3001\u305d\u306e\u57fa\u672c\u7684\u306a\u7269\u7406\u539f\u7406\u3001\u624b\u9806\u306e\u8907\u96d1\u3055\u3001\u3055\u307e\u3056\u307e\u306a\u30b5\u30f3\u30d7\u30eb\u30bf\u30a4\u30d7\u3078\u306e\u9069\u5408\u6027\u306b\u57fa\u3065\u3044\u3066\u8a55\u4fa1\u3055\u308c\u3066\u3044\u307e\u3059\u3002\u8003\u5bdf\u3067\u306f\u3001\u4e00\u822c\u7684\u306a\u624b\u9806 [...]...<\/p>","protected":false},"author":1,"featured_media":5992,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[238],"tags":[],"class_list":["post-5991","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-news"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v24.4 - https:\/\/yoast.com\/wordpress\/plugins\/seo\/ -->\n<title>Expert Guide: 3 Proven Methods for How to Prepare a Solid Sample for IR Analysis - Hench Technology<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/www.hcftir.com\/ja\/expert-guide-3-proven-methods-for-how-to-prepare-a-solid-sample-for-ir-analysis-article\/\" \/>\n<meta property=\"og:locale\" content=\"ja_JP\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Expert Guide: 3 Proven Methods for How to Prepare a Solid Sample for IR Analysis - Hench Technology\" \/>\n<meta property=\"og:description\" content=\"Abstract The acquisition of a high-quality Fourier Transform Infrared (FTIR) spectrum from a solid material is fundamentally dependent on the method chosen for its preparation. 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