{"id":5988,"date":"2025-10-21T10:50:20","date_gmt":"2025-10-21T10:50:20","guid":{"rendered":"https:\/\/www.hcftir.com\/7-proven-methods-a-guide-on-how-to-prepare-sample-for-ir-spectroscopy-article\/"},"modified":"2025-10-21T10:50:21","modified_gmt":"2025-10-21T10:50:21","slug":"7-proven-methods-a-guide-on-how-to-prepare-sample-for-ir-spectroscopy","status":"publish","type":"post","link":"https:\/\/www.hcftir.com\/ja\/7-proven-methods-a-guide-on-how-to-prepare-sample-for-ir-spectroscopy-article\/","title":{"rendered":"7\u3064\u306e\u5b9f\u8a3c\u6e08\u307f\u306e\u65b9\u6cd5IR\u30b9\u30da\u30af\u30c8\u30ed\u30b9\u30b3\u30d4\u30fc\u7528\u30b5\u30f3\u30d7\u30eb\u306e\u8abf\u88fd\u65b9\u6cd5\u30ac\u30a4\u30c9"},"content":{"rendered":"<p><img loading=\"lazy\" decoding=\"async\" style=\"display: block; margin-left: auto; margin-right: auto;\" data-src=\"https:\/\/www.hcftir.com\/wp-content\/uploads\/2025\/09\/FTIR-Film-sample-holder-1.webp\" alt=\"\" width=\"600\" height=\"600\" src=\"https:\/\/www.hcftir.com\/wp-content\/uploads\/2025\/09\/FTIR-Film-sample-holder-1.webp\" data-ll-status=\"loaded\" class=\"entered loaded\"><\/p>\n<h2 id=\"abstract\">\u8981\u65e8<\/h2>\n<p>\u8d64\u5916\uff08IR\uff09\u5206\u5149\u6cd5\u306f\u3001\u8d64\u5916\u7dda\u306e\u5438\u53ce\u3092\u6e2c\u5b9a\u3059\u308b\u3053\u3068\u306b\u3088\u3063\u3066\u5316\u5b66\u7269\u8cea\u3092\u540c\u5b9a\u3059\u308b\u305f\u3081\u306e\u5f37\u529b\u306a\u5206\u6790\u6280\u8853\u3067\u3042\u308b\u3002\u3057\u304b\u3057\u3001\u8d64\u5916\u30b9\u30da\u30af\u30c8\u30eb\u306e\u54c1\u8cea\u3068\u89e3\u91c8\u306e\u3057\u3084\u3059\u3055\u306f\u3001\u57fa\u672c\u7684\u306b\u30b5\u30f3\u30d7\u30eb\u306e\u5165\u5ff5\u306a\u524d\u51e6\u7406\u306b\u4f9d\u5b58\u3057\u307e\u3059\u3002\u672c\u66f8\u3067\u306f\u3001\u30d5\u30fc\u30ea\u30a8\u5909\u63db\u8d64\u5916\u5206\u5149\uff08FTIR\uff09\u5206\u6790\u7528\u306e\u8a66\u6599\u8abf\u88fd\u306b\u95a2\u308f\u308b\u65b9\u6cd5\u8ad6\u3092\u5305\u62ec\u7684\u306b\u691c\u8a0e\u3057\u307e\u3059\u3002\u56fa\u4f53\u3001\u6db2\u4f53\u3001\u6c17\u4f53\u306b\u9069\u7528\u53ef\u80fd\u306a7\u3064\u306e\u7570\u306a\u308b\u5b9f\u7e3e\u306e\u3042\u308b\u624b\u6cd5\u3092\u4f53\u7cfb\u7684\u306b\u691c\u8a0e\u3057\u3001\u305d\u308c\u305e\u308c\u306e\u7406\u8ad6\u7684\u80cc\u666f\u3068\u5b9f\u969b\u7684\u306a\u5b9f\u65bd\u65b9\u6cd5\u3092\u660e\u3089\u304b\u306b\u3057\u3066\u3044\u307e\u3059\u3002\u81ed\u5316\u30ab\u30ea\u30a6\u30e0(KBr)\u30da\u30ec\u30c3\u30c8\u3084\u30cc\u30b8\u30e7\u30fc\u30eb\u30de\u30eb\u306e\u4f5c\u6210\u3068\u3044\u3063\u305f\u4f1d\u7d71\u7684\u306a\u624b\u6cd5\u304b\u3089\u3001\u6e1b\u8870\u5168\u53cd\u5c04(ATR)\u306e\u3088\u3046\u306a\u73fe\u4ee3\u7684\u3067\u5408\u7406\u7684\u306a\u30a2\u30d7\u30ed\u30fc\u30c1\u307e\u3067\u7db2\u7f85\u3057\u3066\u3044\u307e\u3059\u3002\u3055\u3089\u306b\u3001\u8584\u819c\u5206\u6790\u3001\u6db2\u76f8\u30fb\u6c17\u76f8\u6e2c\u5b9a\u3001\u62e1\u6563\u53cd\u5c04\u7387\uff08DRIFTS\uff09\u306a\u3069\u306e\u7279\u6b8a\u306a\u624b\u6cd5\u306e\u30c6\u30af\u30cb\u30c3\u30af\u306b\u3064\u3044\u3066\u3082\u8a73\u3057\u304f\u89e3\u8aac\u3059\u308b\u3002\u305d\u306e\u76ee\u7684\u306f\u3001\u7814\u7a76\u8005\u3001\u6280\u8853\u8005\u3001\u5b66\u751f\u306b\u3001\u9069\u5207\u306a\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u6280\u8853\u3092\u9078\u629e\u3057\u3001\u9069\u5207\u306b\u5b9f\u884c\u3059\u308b\u305f\u3081\u306e\u77e5\u8b58\u3092\u8eab\u306b\u3064\u3051\u3055\u305b\u308b\u3053\u3068\u3067\u3042\u308a\u3001\u305d\u308c\u306b\u3088\u308a\u3001\u5149\u6563\u4e71\u3084\u6c34\u5206\u6c5a\u67d3\u306a\u3069\u306e\u4e00\u822c\u7684\u306a\u30a8\u30e9\u30fc\u3092\u6700\u5c0f\u9650\u306b\u6291\u3048\u3001\u6b63\u78ba\u3067\u518d\u73fe\u6027\u306e\u3042\u308b\u610f\u5473\u306e\u3042\u308b\u30b9\u30da\u30af\u30c8\u30eb\u30c7\u30fc\u30bf\u3092\u9054\u6210\u3059\u308b\u3053\u3068\u3067\u3059\u3002<\/p>\n<h2 id=\"key-takeaways\">\u8981\u70b9<\/h2>\n<ul>\n<li>\u8a66\u6599\u306e\u7269\u7406\u7684\u72b6\u614b\u3068\u6027\u8cea\u306b\u6700\u3082\u9069\u3057\u305f\u8abf\u88fd\u6cd5\u3092\u9078\u629e\u3059\u308b\u3002<\/li>\n<li>\u30d6\u30ed\u30fc\u30c9\u306a\u6c34\u5206\u30d4\u30fc\u30af\u304c\u30c7\u30fc\u30bf\u3092\u4e0d\u660e\u77ad\u306b\u3059\u308b\u306e\u3092\u9632\u3050\u305f\u3081\u3001\u30b5\u30f3\u30d7\u30eb\u3068\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u3092\u5341\u5206\u306b\u4e7e\u71e5\u3055\u305b\u308b\u3002<\/li>\n<li>\u5149\u306e\u6563\u4e71\u3092\u6e1b\u3089\u3059\u305f\u3081\u3001\u56fa\u4f53\u8a66\u6599\u3092IR\u6ce2\u9577\u3088\u308a\u5c0f\u3055\u3044\u7c92\u5f84\u306b\u7c89\u7815\u3059\u308b\u3002<\/li>\n<li>IR\u30b9\u30da\u30af\u30c8\u30ed\u30b9\u30b3\u30d4\u30fc\u306e\u305f\u3081\u306e\u30b5\u30f3\u30d7\u30eb\u306e\u6e96\u5099\u65b9\u6cd5\u3092\u30de\u30b9\u30bf\u30fc\u3059\u308b\u3053\u3068\u306f\u3001\u4fe1\u983c\u3067\u304d\u308b\u30c7\u30fc\u30bf\u3092\u53d6\u5f97\u3059\u308b\u305f\u3081\u306e\u76f4\u63a5\u7684\u306a\u9053\u3067\u3042\u308b\u3002<\/li>\n<li>\u30af\u30ed\u30b9\u30b3\u30f3\u30bf\u30df\u30cd\u30fc\u30b7\u30e7\u30f3\u3092\u907f\u3051\u308b\u305f\u3081\u3001\u30b5\u30f3\u30d7\u30eb\u3068\u30b5\u30f3\u30d7\u30eb\u306e\u9593\u306b\u3059\u3079\u3066\u306e\u30c4\u30fc\u30eb\u304a\u3088\u3073\u5149\u5b66\u7cfb\u3092\u5165\u5ff5\u306b\u6d17\u6d44\u3059\u308b\u3002<\/li>\n<li>\u7a93\u3001\u30da\u30ec\u30c3\u30c8\u3001\u30bb\u30eb\u69cb\u9020\u306b\u306f\u3001NaCl\u3001KBr\u3001ZnSe\u306a\u3069\u306e\u8d64\u5916\u900f\u904e\u6027\u6750\u6599\u3092\u4f7f\u7528\u3059\u308b\u3002<\/li>\n<li>\u9ad8\u54c1\u8cea\u306eATR\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5f97\u308b\u305f\u3081\u306b\u306f\u3001\u8a66\u6599\u3068\u7d50\u6676\u306e\u7269\u7406\u7684\u63a5\u89e6\u304c\u826f\u597d\u3067\u3042\u308b\u3053\u3068\u304c\u5fc5\u8981\u3067\u3059\u3002<\/li>\n<\/ul>\n<h2 id=\"table-of-contents\">\u76ee\u6b21<\/h2>\n<ul>\n<li><a href=\"#a-philosophical-prelude-to-sample-preparation\">\u8a66\u6599\u8abf\u88fd\u3078\u306e\u54f2\u5b66\u7684\u524d\u594f\u66f2<\/a><\/li>\n<li><a href=\"#foundational-principles-of-ir-sample-integrity\">IR\u30b5\u30f3\u30d7\u30eb\u306e\u5b8c\u5168\u6027\u306e\u57fa\u672c\u539f\u5247<\/a><\/li>\n<li><a href=\"#method-1-the-enduring-craft-of-the-kbr-pellet-for-solids\">\u65b9\u6cd51\uff1a\u56fa\u4f53\u7528KBr\u30da\u30ec\u30c3\u30c8\u306e\u4e0d\u673d\u306e\u540d\u4f5c<\/a><\/li>\n<li><a href=\"#method-2-the-mull-technique-a-suspension-based-artform\">\u65b9\u6cd52\uff1a\u30df\u30e5\u30eb\u30fb\u30c6\u30af\u30cb\u30c3\u30af-\u30b5\u30b9\u30da\u30f3\u30c7\u30c3\u30c9\u30fb\u30a2\u30fc\u30c8\u30d5\u30a9\u30fc\u30e0<\/a><\/li>\n<li><a href=\"#method-3-attenuated-total-reflectance-atr-the-modern-paradigm\">\u65b9\u6cd53\uff1a\u6e1b\u8870\u5168\u53cd\u5c04\uff08ATR\uff09-\u73fe\u4ee3\u306e\u30d1\u30e9\u30c0\u30a4\u30e0<\/a><\/li>\n<li><a href=\"#method-4-thin-film-analysis-for-polymers-and-soluble-materials\">\u65b9\u6cd54\uff1a\u30dd\u30ea\u30de\u30fc\u3068\u53ef\u6eb6\u6027\u7269\u8cea\u306e\u8584\u819c\u5206\u6790<\/a><\/li>\n<li><a href=\"#method-5-the-direct-examination-of-liquids-and-solutions\">\u65b9\u6cd55\uff1a\u6db2\u4f53\u3068\u6eb6\u6db2\u306e\u76f4\u63a5\u691c\u67fb<\/a><\/li>\n<li><a href=\"#method-6-capturing-the-freedom-of-gas-phase-molecules\">\u65b9\u6cd56\uff1a\u6c17\u76f8\u5206\u5b50\u306e\u81ea\u7531\u5ea6\u3092\u6349\u3048\u308b<\/a><\/li>\n<li><a href=\"#method-7-advanced-and-specialized-reflectance-techniques\">\u65b9\u6cd57\uff1a\u9ad8\u5ea6\u3067\u7279\u6b8a\u306a\u53cd\u5c04\u7387\u6280\u8853<\/a><\/li>\n<li><a href=\"#frequently-asked-questions-faq\">\u3088\u304f\u3042\u308b\u8cea\u554f\uff08FAQ\uff09<\/a><\/li>\n<li><a href=\"#a-final-reflection-on-practice-and-precision\">\u7df4\u7fd2\u3068\u7cbe\u5ea6\u306b\u95a2\u3059\u308b\u6700\u5f8c\u306e\u8003\u5bdf<\/a><\/li>\n<li><a href=\"#references\">\u53c2\u8003\u6587\u732e<\/a><\/li>\n<\/ul>\n<h2 id=\"a-philosophical-prelude-to-sample-preparation\">\u8a66\u6599\u8abf\u88fd\u3078\u306e\u54f2\u5b66\u7684\u524d\u594f\u66f2<\/h2>\n<p>\u8d64\u5916\u5206\u5149\u306e\u305f\u3081\u306e\u8a66\u6599\u4f5c\u88fd\u3068\u3044\u3046\u8ab2\u984c\u306b\u53d6\u308a\u7d44\u3080\u3053\u3068\u306f\u3001\u7269\u8cea\u4e16\u754c\u3068\u305d\u308c\u306b\u5bfe\u3059\u308b\u62bd\u8c61\u7684\u306a\u7406\u89e3\u3068\u306e\u5bfe\u8a71\u306b\u53d6\u308a\u7d44\u3080\u3053\u3068\u3067\u3042\u308b\u3002\u5149\u5b66\u3068\u8a08\u7b97\u5de5\u5b66\u306e\u9a5a\u7570\u3067\u3042\u308b\u5206\u5149\u8a08\u306f\u3001\u5206\u5b50\u632f\u52d5\u306e\u9759\u304b\u306a\u30c0\u30f3\u30b9\u3092\u8c4a\u304b\u306a\u30b0\u30e9\u30d5\u30a3\u30c3\u30af\u8a00\u8a9e\u306b\u7ffb\u8a33\u3059\u308b\u7528\u610f\u304c\u3067\u304d\u3066\u3044\u308b\u3002\u3057\u304b\u3057\u3001\u3053\u306e\u6d17\u7df4\u3055\u308c\u305f\u88c5\u7f6e\u306f\u3001\u79c1\u305f\u3061\u304c\u63d0\u793a\u3059\u308b\u8a66\u6599\u306b\u5b8c\u5168\u306b\u7ffb\u5f04\u3055\u308c\u3066\u3044\u308b\u3002\u3053\u306e\u88c5\u7f6e\u304c\u751f\u6210\u3059\u308b\u30b9\u30da\u30af\u30c8\u30eb\u306f\u3001\u7269\u8cea\u306e\u9b42\u306e\u7121\u5a92\u4ecb\u306a\u5553\u793a\u3067\u306f\u306a\u304f\u3001\u6211\u3005\u306e\u6e96\u5099\u884c\u70ba\u306e\u30d5\u30a3\u30eb\u30bf\u30fc\u3092\u901a\u3057\u3066\u8a9e\u3089\u308c\u308b\u7269\u8a9e\u3067\u3042\u308b\u3002\u6e96\u5099\u306e\u4e0d\u5341\u5206\u306a\u30b5\u30f3\u30d7\u30eb\u306f\u3001\u6587\u5b57\u5316\u3051\u3057\u305f\u3055\u3055\u3084\u304d\u58f0\u306e\u30e1\u30c3\u30bb\u30fc\u30b8\u306b\u4f3c\u3066\u3044\u308b\u3002\u9006\u306b\u3001\u5165\u5ff5\u306b\u6e96\u5099\u3055\u308c\u305f\u30b5\u30f3\u30d7\u30eb\u306f\u3001\u5206\u5b50\u3092\u306f\u3063\u304d\u308a\u3068\u8a9e\u3089\u305b\u3001\u305d\u306e\u69cb\u9020\u7684\u540c\u4e00\u6027\u3001\u5b98\u80fd\u57fa\u3001\u672c\u8cea\u3092\u6df1\u304f\u660e\u77ad\u306b\u3059\u308b\u3002<\/p>\n<p>\u79c1\u305f\u3061\u306e\u4ed5\u4e8b\u306f\u3001\u5358\u306a\u308b\u6a5f\u68b0\u7684\u306a\u624b\u9806\u3067\u306f\u306a\u3044\u3002\u305d\u308c\u306f\u77e5\u7684\u3067\u5b9f\u7528\u7684\u306a\u53b3\u5bc6\u3055\u306e\u884c\u70ba\u3067\u3042\u308a\u3001\u30b5\u30f3\u30d7\u30eb\u306e\u6027\u8cea\u3092\u5171\u611f\u7684\u306b\u7406\u89e3\u3059\u308b\u3053\u3068\u3092\u8981\u6c42\u3059\u308b\u3002\u305d\u308c\u306f\u7d50\u6676\u6027\u306e\u56fa\u4f53\u3067\u3042\u308a\u3001\u305d\u306e\u5805\u3044\u683c\u5b50\u306f\u624b\u306a\u305a\u3051\u3089\u308c\u306a\u3051\u308c\u3070\u5149\u3092\u6563\u4e71\u3055\u305b\u308b\u304b\u3082\u3057\u308c\u306a\u3044\u306e\u304b\uff1f\u7d4c\u8def\u306e\u9577\u3055\u3092\u6b63\u78ba\u306b\u5236\u5fa1\u3057\u306a\u3051\u308c\u3070\u306a\u3089\u306a\u3044\u7c98\u6027\u306e\u3042\u308b\u6db2\u4f53\u306a\u306e\u304b\uff1f\u305d\u308c\u3068\u3082\u30a2\u30e2\u30eb\u30d5\u30a1\u30b9\u30dd\u30ea\u30de\u30fc\u306a\u306e\u304b\u3002\u624b\u6cd5\u306e\u9078\u629e\u306f\u54f2\u5b66\u7684\u306a\u30b3\u30df\u30c3\u30c8\u30e1\u30f3\u30c8\u3067\u3042\u308a\u3001\u79c1\u305f\u3061\u81ea\u8eab\u306e\u6210\u679c\u7269\u3092\u62bc\u3057\u4ed8\u3051\u308b\u3053\u3068\u306a\u304f\u3001\u7269\u8cea\u306e\u771f\u5b9f\u3092\u660e\u3089\u304b\u306b\u3059\u308b\u6700\u5584\u306e\u65b9\u6cd5\u306b\u3064\u3044\u3066\u306e\u6c7a\u65ad\u3067\u3042\u308b\u3002\u53e4\u5178\u7684\u306aKBr\u30da\u30ec\u30c3\u30c8\u304b\u3089\u6700\u65b0\u306eATR\u30a2\u30af\u30bb\u30b5\u30ea\u30fc\u306b\u81f3\u308b\u307e\u3067\u3001\u5404\u624b\u6cd5\u306b\u306f\u72ec\u81ea\u306e\u4eee\u5b9a\u3068\u6f5c\u5728\u7684\u306a\u843d\u3068\u3057\u7a74\u304c\u3042\u308b\u3002\u8d64\u5916\u5206\u5149\u6cd5\u306e\u305f\u3081\u306e\u8a66\u6599\u8abf\u88fd\u6cd5\u3092\u5b66\u3076\u3053\u3068\u306f\u3001\u7269\u8cea\u306b\u6b63\u3057\u3044\u8cea\u554f\u3092\u6295\u3052\u304b\u3051\u3001\u5f97\u3089\u308c\u308b\u7b54\u3048\u304c\u672c\u7269\u3067\u3042\u308a\u3001\u304b\u3064\u8aad\u307f\u3084\u3059\u3044\u3082\u306e\u3067\u3042\u308b\u3053\u3068\u3092\u4fdd\u8a3c\u3059\u308b\u6280\u8853\u3092\u5b66\u3076\u3053\u3068\u3067\u3042\u308b\u3002<\/p>\n<h2 id=\"foundational-principles-of-ir-sample-integrity\">IR\u30b5\u30f3\u30d7\u30eb\u306e\u5b8c\u5168\u6027\u306e\u57fa\u672c\u539f\u5247<\/h2>\n<p>\u5177\u4f53\u7684\u306a\u30c6\u30af\u30cb\u30c3\u30af\u3092\u63a2\u6c42\u3059\u308b\u524d\u306b\u3001\u307e\u305aIR\u5206\u6790\u3092\u6210\u529f\u306b\u5c0e\u304f\u666e\u904d\u7684\u306a\u539f\u5247\u3092\u78ba\u7acb\u3057\u306a\u3051\u308c\u3070\u306a\u3089\u306a\u3044\u3002\u30b9\u30da\u30af\u30c8\u30eb\u306e\u8cea\u306f\u3001\u5206\u5149\u8a08\u306e\u4e2d\u3067\u751f\u307e\u308c\u308b\u306e\u3067\u306f\u306a\u304f\u3001\u6e2c\u5b9a\u306b\u5148\u7acb\u3064\u5b9f\u9a13\u5ba4\u3067\u306e\u884c\u52d5\u306b\u3042\u308b\u3002\u3053\u308c\u3089\u306e\u539f\u5247\u306f\u3001\u512a\u308c\u305f\u5206\u5149\u5b66\u7684\u5b9f\u8df5\u306e\u61b2\u6cd5\u3068\u8003\u3048\u3066\u304f\u3060\u3055\u3044\u3002<\/p>\n<h3 id=\"the-tyranny-of-water\">\u6c34\u306e\u66b4\u8650<\/h3>\n<p>\u6c34\u306f\u3001\u4e2d\u8d64\u5916\u5206\u5149\u6cd5\u306b\u304a\u3051\u308b\u30e6\u30d3\u30ad\u30bf\u30b9\u306a\u6575\u3067\u3042\u308b\u3002\u6c34\u5206\u5b50\uff08H\u2082O\uff09\u306f\u3001\u4e00\u822c\u7684\u306b3200-3600cm\u00b9\u306e\u9818\u57df\u306b\u73fe\u308c\u308b\u5f37\u304f\u5e83\u3044O-H\u4f38\u7e2e\u632f\u52d5\u3092\u6301\u3063\u3066\u3044\u308b\u3002\u307e\u305f\u30011640cm-\u00b9\u4ed8\u8fd1\u306bH-O-H\u5c48\u66f2\u632f\u52d5\u304c\u3042\u308b\u3002\u3053\u308c\u3089\u306e\u5438\u53ce\u30d0\u30f3\u30c9\u306f\u975e\u5e38\u306b\u5f37\u3044\u305f\u3081\u3001\u30b5\u30f3\u30d7\u30eb\u3084\u5468\u56f2\u306e\u5927\u6c17\u4e2d\u306e\u5fae\u91cf\u306e\u6c34\u5206\u3067\u3055\u3048\u30b9\u30da\u30af\u30c8\u30eb\u3092\u652f\u914d\u3057\u3066\u3057\u307e\u3044\u3001\u5206\u6790\u5bfe\u8c61\u7269\u306e\u3088\u308a\u7e4a\u7d30\u3067\u6709\u76ca\u306a\u30d4\u30fc\u30af\u3092\u4e0d\u660e\u77ad\u306b\u3057\u3066\u3057\u307e\u3046\u3002\u81ed\u5316\u30ab\u30ea\u30a6\u30e0\uff08KBr\uff09\u306e\u3088\u3046\u306a\u4e00\u822c\u7684\u306a\u7269\u8cea\u306b\u306f\u5438\u6e7f\u6027\u304c\u3042\u308b\u305f\u3081\u3001\u3053\u308c\u306f\u6c38\u9060\u306e\u8ab2\u984c\u3067\u3042\u308b\u3002\u3057\u305f\u304c\u3063\u3066\u3001IR\u8a66\u6599\u8abf\u88fd\u306e\u7b2c\u4e00\u306e\u6212\u3081\u306f\u3001\u8a66\u6599\u3001\u6750\u6599\u3001\u88c5\u7f6e\u3092\u3067\u304d\u308b\u3060\u3051\u4e7e\u71e5\u3055\u305b\u3066\u304a\u304f\u3053\u3068\u3067\u3042\u308b\u3002\u305d\u306e\u305f\u3081\u306b\u306f\u3001\u30cf\u30ed\u30b2\u30f3\u5316\u30a2\u30eb\u30ab\u30ea\u5869\u3092\u30c7\u30b7\u30b1\u30fc\u30bf\u30fc\u3067\u4fdd\u7ba1\u3057\u305f\u308a\u3001\u4f7f\u7528\u524d\u306b\u30aa\u30fc\u30d6\u30f3\u3067\u4e7e\u71e5\u3055\u305b\u305f\u308a\u3059\u308b\u5fc5\u8981\u304c\u3042\u308b\u3002<\/p>\n<h3 id=\"the-problem-of-light-scattering\">\u5149\u6563\u4e71\u306e\u554f\u984c<\/h3>\n<p>\u56fa\u4f53\u8a66\u6599\u3001\u7279\u306b\u900f\u904e\u6cd5\u3067\u306f\u3001\u7269\u7406\u7684\u5f62\u72b6\u306f\u5316\u5b66\u7d44\u6210\u3068\u540c\u3058\u304f\u3089\u3044\u91cd\u8981\u3067\u3042\u308b\u3002\u56fa\u4f53\u306e\u7c92\u5b50\u5f84\u304c\u8d64\u5916\u5149\u306e\u6ce2\u9577\uff08\u304a\u3088\u305d2.5\uff5e25\u30de\u30a4\u30af\u30ed\u30e1\u30fc\u30c8\u30eb\uff09\u306b\u5339\u6575\u3059\u308b\u304b\u305d\u308c\u3088\u308a\u3082\u5927\u304d\u3044\u5834\u5408\u3001\u5149\u306f\u900f\u904e\u3067\u306f\u306a\u304f\u6563\u4e71\u3055\u308c\u308b\u3002\u30af\u30ea\u30b9\u30c1\u30e3\u30f3\u30bb\u30f3\u52b9\u679c\u3068\u3057\u3066\u77e5\u3089\u308c\u308b\u3053\u306e\u73fe\u8c61\u306f\u3001\u6b6a\u3093\u3060\u30d4\u30fc\u30af\u5f62\u72b6\u3068\u50be\u659c\u3057\u305f\u4e0d\u898f\u5247\u306a\u30d9\u30fc\u30b9\u30e9\u30a4\u30f3\u3092\u3082\u305f\u3089\u3057\u3001\u30b9\u30da\u30af\u30c8\u30eb\u306e\u89e3\u91c8\u3092\u96e3\u3057\u304f\u3059\u308b\u3002\u89e3\u6c7a\u7b56\u306f\u3001\u8a66\u6599\u306e\u7c92\u5f84\u3092\u7d30\u304b\u304f\u5747\u4e00\u306a\u7c89\u672b\u306b\u3059\u308b\u3053\u3068\u3067\u3042\u308a\u3001\u7406\u60f3\u7684\u306b\u306f2\u30de\u30a4\u30af\u30ed\u30e1\u30fc\u30c8\u30eb\u4ee5\u4e0b\u306e\u7c92\u5b50\u306b\u3059\u308b\u3053\u3068\u3067\u3042\u308b\u3002\u3053\u306e\u305f\u3081\u3001\u56fa\u4f53\u8a66\u6599\u306e\u524d\u51e6\u7406\u306e\u5927\u90e8\u5206\u306b\u306f\u3001\u5f37\u529b\u304b\u3064\u5fb9\u5e95\u7684\u306a\u7c89\u7815\u304c\u542b\u307e\u308c\u308b\u3002<\/p>\n<h3 id=\"concentration-and-the-beer-lambert-law\">\u6fc3\u5ea6\u3068\u30d3\u30fc\u30eb\uff1d\u30e9\u30f3\u30d0\u30fc\u30c8\u306e\u6cd5\u5247<\/h3>\n<p>\u8d64\u5916\u5206\u5149\u6cd5\u306f\u5b9a\u6027\uff08\u4f55\u304c\u3042\u308b\u304b\uff09\u3068\u5b9a\u91cf\uff08\u3069\u306e\u304f\u3089\u3044\u3042\u308b\u304b\uff09\u306e\u4e21\u65b9\u304c\u53ef\u80fd\u3067\u3059\u3002\u3069\u3061\u3089\u306e\u76ee\u7684\u306b\u304a\u3044\u3066\u3082\u3001\u8d64\u5916\u30d3\u30fc\u30e0\u4e2d\u306e\u8a66\u6599\u306e\u6fc3\u5ea6\u304c\u6700\u3082\u91cd\u8981\u3067\u3059\u3002Beer-Lambert\u306e\u6cd5\u5247\u3067\u306f\u3001\u5438\u5149\u5ea6\u306f\u5206\u6790\u7269\u306e\u6fc3\u5ea6\u3068\u8a66\u6599\u3092\u901a\u308b\u30d3\u30fc\u30e0\u306e\u7d4c\u8def\u9577\u306b\u6b63\u6bd4\u4f8b\u3057\u307e\u3059\uff08A = \u03b5bc\uff09\u3002<\/p>\n<ul>\n<li><strong>\u30b5\u30f3\u30d7\u30eb\u91cf\u304c\u591a\u3059\u304e\u308b\uff08\u307e\u305f\u306f\u30d1\u30b9\u9577\u304c\u9577\u3059\u304e\u308b\uff09\uff1a<\/strong> \u8a66\u6599\u306e\u6fc3\u5ea6\u304c\u9ad8\u3059\u304e\u308b\u3068\u3001\u8d64\u5916\u653e\u5c04\u3092\u305d\u306e\u7279\u5fb4\u7684\u306a\u5468\u6ce2\u6570\u3067\u3059\u3079\u3066\u5438\u53ce\u3057\u3066\u3057\u307e\u3044\u307e\u3059\u3002\u305d\u306e\u7d50\u679c\u3001\u5438\u5149\u5ea6100%\uff08\u307e\u305f\u306f\u900f\u904e\u73870%\uff09\u306e \"\u30d5\u30e9\u30c3\u30c8\u30c8\u30c3\u30d7 \"\u30d4\u30fc\u30af\u304c\u751f\u3058\u307e\u3059\u3002\u30d4\u30fc\u30af\u306e\u771f\u306e\u5f37\u5ea6\u3068\u5f62\u72b6\u306b\u95a2\u3059\u308b\u60c5\u5831\u304c\u5931\u308f\u308c\u3001\u5b9a\u91cf\u5206\u6790\u304c\u4e0d\u53ef\u80fd\u306b\u306a\u308a\u3001\u5b9a\u6027\u540c\u5b9a\u304c\u56f0\u96e3\u306b\u306a\u308a\u307e\u3059\u3002<\/li>\n<li><strong>\u30b5\u30f3\u30d7\u30eb\u304c\u5c11\u306a\u3059\u304e\u308b\uff08\u307e\u305f\u306f\u30d1\u30b9\u9577\u304c\u77ed\u3059\u304e\u308b\uff09\uff1a<\/strong> \u30b5\u30f3\u30d7\u30eb\u304c\u5e0c\u8584\u3059\u304e\u308b\u3068\u3001\u5f97\u3089\u308c\u308b\u5438\u53ce\u30d4\u30fc\u30af\u306f\u5f31\u304f\u3001\u30d0\u30c3\u30af\u30b0\u30e9\u30a6\u30f3\u30c9\u30ce\u30a4\u30ba\u3068\u307b\u3068\u3093\u3069\u533a\u5225\u304c\u3064\u304b\u306a\u304f\u306a\u308b\u3002S\/N\u6bd4\u304c\u60aa\u304f\u306a\u308a\u3001\u5f31\u3044\u304c\u91cd\u8981\u306a\u5b98\u80fd\u57fa\u3092\u5b8c\u5168\u306b\u898b\u9003\u3057\u3066\u3057\u307e\u3046\u53ef\u80fd\u6027\u304c\u3042\u308b\u3002<\/li>\n<\/ul>\n<p>\u76ee\u6a19\u306f\u3001\u6700\u3082\u5f37\u3044\u5438\u53ce\u5e2f\u306e\u900f\u904e\u7387\u304c\u7d0410%\uff5e70%\uff08\u307e\u305f\u306f\u5438\u5149\u5ea6\u304c\u7d040.15\uff5e1.0\uff09\u306e\u8a66\u6599\u3092\u8abf\u88fd\u3059\u308b\u3053\u3068\u3067\u3042\u308b\u3002\u305d\u306e\u305f\u3081\u306b\u306f\u3001\u30b5\u30f3\u30d7\u30eb\u306e\u4f7f\u7528\u91cf\u3092\u6ce8\u610f\u6df1\u304f\u30b3\u30f3\u30c8\u30ed\u30fc\u30eb\u3059\u308b\u5fc5\u8981\u304c\u3042\u308b\u3002<\/p>\n<p><strong>\u88681\uff1a\u4e00\u822c\u7684\u306a\u56fa\u4f53\u8a66\u6599\u8abf\u88fd\u6cd5\u306e\u6bd4\u8f03<\/strong><\/p>\n<table class=\"mce-item-table\" style=\"width:100%; border-collapse: collapse;\" border=\"1\">\n<thead>\n<tr>\n<th style=\"text-align:left;\">\u7279\u5fb4<\/th>\n<th style=\"text-align:left;\">KBr\u30da\u30ec\u30c3\u30c8\u6cd5<\/th>\n<th style=\"text-align:left;\">\u30de\u30eb\u30fb\u30c6\u30af\u30cb\u30c3\u30af<\/th>\n<th style=\"text-align:left;\">\u6e1b\u8870\u5168\u53cd\u5c04\u7387\uff08ATR\uff09<\/th>\n<\/tr>\n<\/thead>\n<tbody>\n<tr>\n<td style=\"text-align:left;\"><strong>\u539f\u5247<\/strong><\/td>\n<td style=\"text-align:left;\">\u900f\u660e\u306a\u56fa\u4f53\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u306b\u5206\u6563\u3057\u305f\u8a66\u6599<\/td>\n<td style=\"text-align:left;\">\u7c98\u6027\u6db2\u4f53\u306b\u61f8\u6fc1\u3055\u308c\u305f\u8a66\u6599<\/td>\n<td style=\"text-align:left;\">\u30a8\u30d0\u30cd\u30c3\u30bb\u30f3\u30c8\u6ce2\u30d7\u30ed\u30fc\u30d6<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u30b5\u30f3\u30d7\u30eb\u91cf<\/strong><\/td>\n<td style=\"text-align:left;\">1-2 mg<\/td>\n<td style=\"text-align:left;\">2-5 mg<\/td>\n<td style=\"text-align:left;\">&lt;1mg\u672a\u6e80\uff5e\u6570mg<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u6e96\u5099\u671f\u9593<\/strong><\/td>\n<td style=\"text-align:left;\">10\uff5e20\u5206<\/td>\n<td style=\"text-align:left;\">5\uff5e10\u5206<\/td>\n<td style=\"text-align:left;\">&lt;1\u5206<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u30b9\u30ad\u30eb\u30ec\u30d9\u30eb<\/strong><\/td>\n<td style=\"text-align:left;\">\u9ad8\u3044\uff08\u7df4\u7fd2\u304c\u5fc5\u8981\uff09<\/td>\n<td style=\"text-align:left;\">\u30df\u30c7\u30a3\u30a2\u30e0<\/td>\n<td style=\"text-align:left;\">\u4f4e\u3044<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u8a08\u91cf\u80fd\u529b<\/strong><\/td>\n<td style=\"text-align:left;\">\u53ef\u80fd\u3060\u304c\u3001\u96e3\u3057\u3044<\/td>\n<td style=\"text-align:left;\">\u60aa\u3044\uff08\u30d1\u30b9\u306e\u9577\u3055\u3092\u30b3\u30f3\u30c8\u30ed\u30fc\u30eb\u3059\u308b\u306e\u304c\u96e3\u3057\u3044\uff09<\/td>\n<td style=\"text-align:left;\">\u30b0\u30c3\u30c9\uff5e\u30a8\u30af\u30bb\u30ec\u30f3\u30c8\uff08\u518d\u73fe\u53ef\u80fd\uff09<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u4e00\u822c\u7684\u306a\u4eba\u5de5\u7269<\/strong><\/td>\n<td style=\"text-align:left;\">\u6c34\u306e\u30d4\u30fc\u30af\u3001\u6563\u4e71\u3001\u30af\u30ea\u30b9\u30c1\u30e3\u30f3\u30bb\u30f3\u52b9\u679c<\/td>\n<td style=\"text-align:left;\">\u30de\u30ea\u30f3\u30b0\u5264\u306e\u30d4\u30fc\u30af\u3001\u6563\u4e71<\/td>\n<td style=\"text-align:left;\">\u30d0\u30f3\u30c9\u30b7\u30d5\u30c8\u3001\u63a5\u89e6\u4e0d\u826f\u306e\u554f\u984c<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u30d9\u30b9\u30c8\u30fb\u30d5\u30a9\u30fc...<\/strong><\/td>\n<td style=\"text-align:left;\">\u9ad8\u5206\u89e3\u80fd\u900f\u904e\u30b9\u30da\u30af\u30c8\u30eb\u3001\u30e9\u30a4\u30d6\u30e9\u30ea<\/td>\n<td style=\"text-align:left;\">\u6c34\u306b\u654f\u611f\u307e\u305f\u306f\u53cd\u5fdc\u6027\u306e\u30b5\u30f3\u30d7\u30eb\u3001\u8fc5\u901f\u306a\u5b9a\u6027\u30b9\u30ad\u30e3\u30f3<\/td>\n<td style=\"text-align:left;\">\u7c89\u672b\u3001\u6db2\u4f53\u3001\u30dd\u30ea\u30de\u30fc\u3001\u4e0d\u900f\u660e\u8a66\u6599\uff1b\u30eb\u30fc\u30c1\u30f3\u5206\u6790<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<h2 id=\"method-1-the-enduring-craft-of-the-kbr-pellet-for-solids\">\u65b9\u6cd51\uff1a\u56fa\u4f53\u7528KBr\u30da\u30ec\u30c3\u30c8\u306e\u4e0d\u673d\u306e\u540d\u4f5c<\/h2>\n<p>\u81ed\u5316\u30ab\u30ea\u30a6\u30e0(KBr)\u30da\u30ec\u30c3\u30c8\u6cd5\u306f\u3001\u56fa\u4f53\u8a66\u6599\u3092\u900f\u904e\u30e2\u30fc\u30c9\u3067\u5206\u6790\u3059\u308b\u305f\u3081\u306e\u6700\u3082\u53e4\u304f\u3001\u6700\u3082\u5c0a\u656c\u3055\u308c\u3066\u3044\u308b\u30c6\u30af\u30cb\u30c3\u30af\u306e\u3072\u3068\u3064\u3067\u3042\u308b\u3002\u719f\u7df4\u3068\u5fcd\u8010\u3092\u3082\u3063\u3066\u5b9f\u884c\u3059\u308c\u3070\u3001\u975e\u5e38\u306b\u9ad8\u54c1\u8cea\u306a\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5f97\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002\u3053\u306e\u65b9\u6cd5\u3067\u306f\u3001\u5c11\u91cf\u306e\u56fa\u4f53\u8a66\u6599\u3092\u3001\u5927\u91cf\u306e\u9ad8\u7d14\u5ea6\u3001\u8d64\u5916\u900f\u904e\u6027\u306eKBr\u7c89\u672b\u3068\u5bc6\u63a5\u306b\u6df7\u5408\u3059\u308b\u3002\u3053\u306e\u6df7\u5408\u7269\u3092\u91d1\u578b\u3067\u9ad8\u5727\u30d7\u30ec\u30b9\u3057\u3066\u3001\u5c0f\u3055\u306a\u900f\u660e\u306a\u30c7\u30a3\u30b9\u30af\u307e\u305f\u306f\u30da\u30ec\u30c3\u30c8\u3092\u5f62\u6210\u3057\u3001\u3053\u308c\u3092\u5206\u5149\u8a08\u306e\u8a66\u6599\u30db\u30eb\u30c0\u30fc\u306b\u76f4\u63a5\u30bb\u30c3\u30c8\u3059\u308b\u3002<\/p>\n<h3 id=\"the-rationale-behind-alkali-halides\">\u30cf\u30ed\u30b2\u30f3\u5316\u30a2\u30eb\u30ab\u30ea\u306e\u6839\u62e0<\/h3>\n<p>\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u6750\u6599\u306e\u9078\u629e\u306f\u3001\u5bfe\u8c61\u9818\u57df\uff08\u901a\u5e384000-400cm-\u00b9\uff09\u306e\u8d64\u5916\u7dda\u306b\u5bfe\u3057\u3066\u900f\u660e\u3067\u306a\u3051\u308c\u3070\u306a\u3089\u306a\u3044\u3068\u3044\u3046\u5358\u7d14\u306a\u8981\u4ef6\u306b\u652f\u914d\u3055\u308c\u308b\u3002\u81ed\u5316\u30ab\u30ea\u30a6\u30e0(KBr)\u3084\u5869\u5316\u30ca\u30c8\u30ea\u30a6\u30e0(NaCl)\u306e\u3088\u3046\u306a\u30cf\u30ed\u30b2\u30f3\u5316\u30a2\u30eb\u30ab\u30ea\u306f\u3001\u3053\u306e\u57fa\u6e96\u306b\u3074\u3063\u305f\u308a\u5f53\u3066\u306f\u307e\u308a\u307e\u3059\u3002\u3053\u308c\u3089\u306f\u7d50\u6676\u683c\u5b50\u3092\u5f62\u6210\u3059\u308b\u30a4\u30aa\u30f3\u5869\u3067\u3042\u308a\u3001IR\u4e2d\u57df\u306b\u632f\u52d5\u30e2\u30fc\u30c9\u3092\u6301\u305f\u306a\u3044\u3002KBr\u304c\u7279\u306b\u597d\u307e\u308c\u308b\u306e\u306f\u3001\u67d4\u3089\u304b\u304f\u53ef\u935b\u6027\u3067\u3042\u308a\u3001\u5727\u529b\u4e0b\u3067\u6d41\u52d5\u3057\u3066\u51dd\u96c6\u6027\u306e\u3042\u308b\u900f\u660e\u306a\u5186\u76e4\u3092\u5f62\u6210\u3057\u3001\u8a66\u6599\u7c92\u5b50\u3092\u52b9\u679c\u7684\u306b\u5c01\u3058\u8fbc\u3081\u308b\u304b\u3089\u3067\u3042\u308b\u3002NaCl\u3082\u9078\u629e\u80a2\u306e\u4e00\u3064\u3067\u3042\u308b\u304c\u3001\u786c\u304f\u3001\u3088\u308a\u9ad8\u3044\u5727\u529b\u3092\u5fc5\u8981\u3068\u3059\u308b\u3002\u4e0d\u7d14\u7269\u304c\u3042\u308b\u3068\u4e0d\u8981\u306a\u5438\u53ce\u5e2f\u304c\u751f\u3058\u308b\u53ef\u80fd\u6027\u304c\u3042\u308b\u305f\u3081\u3001\u5206\u5149\u5b66\u30b0\u30ec\u30fc\u30c9\u306eKBr\u3092\u4f7f\u7528\u3059\u308b\u3053\u3068\u304c\u6975\u3081\u3066\u91cd\u8981\u3067\u3042\u308b\u3002<\/p>\n<h3 id=\"step-by-step-guide-to-creating-a-perfect-pellet\">\u5b8c\u74a7\u306a\u30da\u30ec\u30c3\u30c8\u3092\u4f5c\u308b\u305f\u3081\u306e\u30b9\u30c6\u30c3\u30d7\u30fb\u30d0\u30a4\u30fb\u30b9\u30c6\u30c3\u30d7\u30fb\u30ac\u30a4\u30c9<\/h3>\n<p>KBr\u30da\u30ec\u30c3\u30c8\u306e\u4f5c\u6210\u306f\u3001\u30e9\u30dc\u306e\u8077\u4eba\u6280\u306e\u4e00\u5f62\u614b\u3067\u3042\u308b\u3002\u6700\u7d42\u7684\u306a\u30b9\u30da\u30af\u30c8\u30eb\u306e\u54c1\u8cea\u306b\u306f\u3001\u5404\u5de5\u7a0b\u304c\u6b20\u304b\u305b\u306a\u3044\u3002<\/p>\n<ol>\n<li><strong>\u6750\u6599\u3092\u4e7e\u71e5\u3055\u305b\u308b\uff1a<\/strong> \u5148\u306b\u8ff0\u3079\u305f\u3088\u3046\u306b\u3001KBr\u306f\u5438\u6e7f\u6027\u304c\u3042\u308b\u3002\u5c11\u91cf\u306e\u5206\u5149\u5b66\u30b0\u30ec\u30fc\u30c9\u306eKBr\u7c89\u672b\u3092\u3001\uff5e110\u2103\u306e\u30aa\u30fc\u30d6\u30f3\u3067\u6570\u6642\u9593\u4e7e\u71e5\u3055\u305b\u308b\u3053\u3068\u304b\u3089\u59cb\u3081\u308b\u3002\u4f7f\u7528\u3059\u308b\u307e\u3067\u30c7\u30b7\u30b1\u30fc\u30bf\u30fc\u3067\u4fdd\u7ba1\u3059\u308b\u3002\u53ef\u80fd\u3067\u3042\u308c\u3070\u3001\u8a66\u6599\u81ea\u4f53\u3082\u5341\u5206\u306b\u4e7e\u71e5\u3055\u305b\u308b\u3002<\/li>\n<li><strong>\u7c89\u7815\u3068\u6df7\u5408\uff1a<\/strong> \u4e7e\u71e5\u3057\u305f\u30e1\u30ce\u30a6\u4e73\u9262\u3068\u4e73\u68d2\u306b\u3001\u4e7e\u71e5KBr\u3092\u7d04100\uff5e200mg\u5165\u308c\u308b\u3002\u56fa\u5f62\u8a66\u6599\u30921-2mg\u52a0\u3048\u308b\u3002\u3053\u306e\u6bd4\u7387\u304c\u91cd\u8981\u3067\u3001\u3088\u304f\u3042\u308b\u9593\u9055\u3044\u306f\u8a66\u6599\u306e\u91cf\u304c\u591a\u3059\u304e\u308b\u3053\u3068\u3067\u3059\u3002\u7406\u60f3\u7684\u306a\u8a66\u6599\u6fc3\u5ea6\u306f\u3001\u91cd\u91cf\u6bd4\u30670.5%\u304b\u30891.0%\u306e\u9593\u3067\u3042\u308b\u3002\u6df7\u5408\u7269\u3092\u6fc0\u3057\u304f\u7c89\u7815\u3057\u59cb\u3081\u308b\u3002\u76ee\u7684\u306f\u3001\u5149\u306e\u6563\u4e71\u3092\u9632\u3050\u305f\u3081\u306b\u8a66\u6599\u306e\u7c92\u5b50\u5f84\u30922 \u00b5m\u4ee5\u4e0b\u306b\u3059\u308b\u3068\u540c\u6642\u306b\u3001\u3053\u308c\u3089\u306e\u5fae\u7c92\u5b50\u3092KBr\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u5168\u4f53\u306b\u5747\u4e00\u306b\u5206\u6563\u3055\u305b\u308b\u3053\u3068\u3067\u3059\u3002\u6700\u7d42\u7684\u306a\u6df7\u5408\u7269\u306f\u3001\u6d41\u52d5\u6027\u306e\u3042\u308b\u5c0f\u9ea6\u7c89\u306e\u3088\u3046\u306a\u7c89\u672b\u3067\u3001\u76ee\u306b\u898b\u3048\u308b\u30b5\u30f3\u30d7\u30eb\u306e\u584a\u306f\u306a\u3044\u306f\u305a\u3067\u3042\u308b\u3002<\/li>\n<li><strong>\u30c0\u30a4\u3092\u88c5\u586b\u3059\u308b\uff1a<\/strong> 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id=\"troubleshooting-common-pellet-problems\">\u4e00\u822c\u7684\u306a\u30da\u30ec\u30c3\u30c8\u306e\u30c8\u30e9\u30d6\u30eb\u30b7\u30e5\u30fc\u30c6\u30a3\u30f3\u30b0<\/h3>\n<p>\u5b8c\u74a7\u306a\u30da\u30ec\u30c3\u30c8\u3078\u306e\u9053\u306f\u3001\u6f5c\u5728\u7684\u306a\u30d5\u30e9\u30b9\u30c8\u30ec\u30fc\u30b7\u30e7\u30f3\u3067\u8217\u88c5\u3055\u308c\u3066\u3044\u308b\u3002\u305d\u306e\u539f\u56e0\u3092\u7406\u89e3\u3059\u308b\u3053\u3068\u304c\u3001\u514b\u670d\u3078\u306e\u9375\u3068\u306a\u308b\u3002<\/p>\n<ul>\n<li><strong>\u66c7\u308a\u307e\u305f\u306f\u4e0d\u900f\u660e\u306a\u30da\u30ec\u30c3\u30c8\uff1a<\/strong> 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id=\"method-2-the-mull-technique-a-suspension-based-artform\">\u65b9\u6cd52\uff1a\u30df\u30e5\u30eb\u30fb\u30c6\u30af\u30cb\u30c3\u30af-\u30b5\u30b9\u30da\u30f3\u30c7\u30c3\u30c9\u30fb\u30a2\u30fc\u30c8\u30d5\u30a9\u30fc\u30e0<\/h2>\n<p>\u30de\u30eb\u6cd5\u306f\u3001KBr\u30da\u30ec\u30c3\u30c8\u6cd5\u306b\u4ee3\u308f\u308b\u3001\u3088\u308a\u8fc5\u901f\u3067\u7c21\u4fbf\u306a\u56fa\u4f53\u8a66\u6599\u306e\u8abf\u88fd\u6cd5\u3067\u3059\u3002\u6e7f\u6c17\u306b\u654f\u611f\u306a\u8a66\u6599\u3001\u52a0\u5727\u4e0b\u3067KBr\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u3068\u53cd\u5fdc\u3059\u308b\u53ef\u80fd\u6027\u306e\u3042\u308b\u8a66\u6599\u3001\u30da\u30ec\u30c3\u30c8\u306b\u7c89\u7815\u3059\u308b\u306e\u304c\u56f0\u96e3\u306a\u8a66\u6599\u306b\u7279\u306b\u6709\u52b9\u3067\u3059\u3002\u56fa\u4f53\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u306b\u8a66\u6599\u3092\u5206\u6563\u3055\u305b\u308b\u4ee3\u308f\u308a\u306b\u3001\u30de\u30ea\u30f3\u30b0\u6cd5\u3067\u306f\u3001\u5fae\u7c89\u7815\u3057\u305f\u8a66\u6599\u3092\u30de\u30ea\u30f3\u30b0\u5264\u3068\u3057\u3066\u77e5\u3089\u308c\u308b\u7c98\u6027\u306e\u3042\u308b\u8d64\u5916\u7dda\u900f\u904e\u6027\u306e\u6db2\u4f53\u306b\u61f8\u6fc1\u3057\u307e\u3059\u3002<\/p>\n<h3 id=\"when-to-choose-a-mull-over-a-pellet\">\u30da\u30ec\u30c3\u30c8\u3088\u308a\u30de\u30eb\u3092\u9078\u3076\u3068\u304d<\/h3>\n<p>KBr\u30da\u30ec\u30c3\u30c8\u6cd5\u306f\u3088\u308a\u9ad8\u5206\u89e3\u80fd\u306e\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5f97\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u304c\u3001\u7279\u5b9a\u306e\u72b6\u6cc1\u306b\u304a\u3044\u3066\u306f\u3001mull\u6cd5\u306b\u306f\u660e\u78ba\u306a\u5229\u70b9\u304c\u3042\u308b\u3002\u7d4c\u8def\u9577\u3084\u6fc3\u5ea6\u3092\u6b63\u78ba\u306b\u518d\u73fe\u3059\u308b\u3053\u3068\u306f\u975e\u5e38\u306b\u96e3\u3057\u3044\u305f\u3081\u3001\u57fa\u672c\u7684\u306b\u306f\u5b9a\u6027\u7684\u306a\u65b9\u6cd5\u3067\u3042\u308b\u3002\u6b21\u306e\u3088\u3046\u306a\u5834\u5408\u306b\u30de\u30eb\u6cd5\u3092\u9078\u629e\u3059\u308b\uff1a<\/p>\n<ul>\n<li>\u78ba\u304b\u306a\u30b5\u30f3\u30d7\u30eb\u3092\u5bfe\u8c61\u3068\u3057\u305f\u8fc5\u901f\u3067\u5b9a\u6027\u7684\u306a\u8abf\u67fb\u304c\u5fc5\u8981\u3060\u3002<\/li>\n<li>\u8a66\u6599\u306f\u30cf\u30ed\u30b2\u30f3\u5316\u30a2\u30eb\u30ab\u30ea\u3068\u53cd\u5fdc\u3059\u308b\u3053\u3068\u304c\u77e5\u3089\u308c\u3066\u3044\u308b\uff08\u4f8b\u3048\u3070\u3001\u3044\u304f\u3064\u304b\u306e\u30a2\u30df\u30f3\u5869\u306fKBr\u3068\u30a4\u30aa\u30f3\u4ea4\u63db\u3092\u8d77\u3053\u3059\u3053\u3068\u304c\u3042\u308b\uff09\u3002<\/li>\n<li>\u30b5\u30f3\u30d7\u30eb\u306f\u30da\u30ec\u30c3\u30c8\u30d7\u30ec\u30b9\u306e\u9ad8\u5727\u306b\u5f31\u3044\u3002<\/li>\n<li>\u8a66\u6599\u306f\u874b\u72b6\u307e\u305f\u306f\u6cb9\u72b6\u3067\u3001KBr\u3067\u306f\u3046\u307e\u304f\u7c89\u7815\u3067\u304d\u306a\u3044\u3002<\/li>\n<li>\u8a73\u7d30\u306a\u69cb\u9020\u89e3\u660e\u3092\u884c\u3046\u306e\u3067\u306f\u306a\u304f\u3001\u7279\u5b9a\u306e\u5b98\u80fd\u57fa\u306e\u6709\u7121\u3092\u30b9\u30af\u30ea\u30fc\u30cb\u30f3\u30b0\u3059\u308b\u306e\u3067\u3059\u3002<\/li>\n<\/ul>\n<h3 id=\"selecting-the-right-mulling-agent\">\u6b63\u3057\u3044\u30de\u30ea\u30f3\u30b0\u30fb\u30a8\u30fc\u30b8\u30a7\u30f3\u30c8\u306e\u9078\u629e<\/h3>\n<p>\u7406\u60f3\u7684\u306a\u30de\u30ea\u30f3\u30b0\u5264\u306f\u3001\u5316\u5b66\u7684\u306b\u4e0d\u6d3b\u6027\u3067\u3001\u4e0d\u63ee\u767a\u6027\u3067\u3001\u5438\u53ce\u5e2f\u304c\u5c11\u306a\u304f\u975e\u5e38\u306b\u30b7\u30f3\u30d7\u30eb\u306a\u8d64\u5916\u30b9\u30da\u30af\u30c8\u30eb\u3092\u6301\u3064\u6db2\u4f53\u3067\u3042\u308b\u3002\u5358\u4e00\u306e\u7269\u8cea\u3067\u5b8c\u74a7\u306a\u3082\u306e\u306f\u306a\u3044\u305f\u3081\u3001\u5b8c\u5168\u306a\u753b\u50cf\u3092\u5f97\u308b\u305f\u3081\u306b\u306f\u3001\u901a\u5e382\u3064\u306e\u7570\u306a\u308b\u85ac\u5264\u3092\u7d44\u307f\u5408\u308f\u305b\u3066\u4f7f\u7528\u3059\u308b\u3002<\/p>\n<ul>\n<li><strong>\u30cc\u30b8\u30e7\u30fc\u30eb\uff08\u30df\u30cd\u30e9\u30eb\u30aa\u30a4\u30eb\uff09\uff1a<\/strong> \u3053\u308c\u306f\u6700\u3082\u4e00\u822c\u7684\u306a\u30e0\u30ea\u30f3\u30b0\u5264\u3067\u3042\u308b\u3002\u30cc\u30b8\u30e7\u30fc\u30eb\u306f\u91cd\u8cea\u30d1\u30e9\u30d5\u30a3\u30f3\u30aa\u30a4\u30eb\u3067\u3001\u9577\u9396\u98fd\u548c\u70ad\u5316\u6c34\u7d20\u306e\u6df7\u5408\u7269\u3067\u3042\u308b\u3002\u305d\u306e\u30b9\u30da\u30af\u30c8\u30eb\u306f\u975e\u5e38\u306b\u5358\u7d14\u3067\u3001\u5f37\u3044C-H\u4f38\u7e2e\u30d0\u30f3\u30c9\uff08\uff5e2850\uff5e2960cm-\u00b9\uff09\u3068C-H\u5c48\u66f2\u30d0\u30f3\u30c9\uff08\uff5e1460cm-\u00b9\u3068\uff5e1375cm-\u00b9\uff09\u3092\u793a\u3059\u3002\u4e2d\u8d64\u5916\u57df\u306e\u5927\u90e8\u5206\u306f\u900f\u660e\u3067\u3042\u308b\u3002<\/li>\n<li><strong>Fluorolube\uff08\u30d1\u30fc\u30d5\u30eb\u30aa\u30ed\u70ad\u5316\u6c34\u7d20\uff09\uff1a<\/strong> Nujol\u3067\u4e0d\u660e\u77ad\u306b\u306a\u3063\u305fC-H\u9818\u57df\u306b\u8208\u5473\u304c\u3042\u308b\u5834\u5408\u306f\u3001Fluorolube\u3092\u4f7f\u3063\u3066\u7b2c\u4e8c\u306e\u30de\u30eb\u3092\u8abf\u88fd\u3059\u308b\u3002\u3053\u306e\u7269\u8cea\u306fC-F\u7d50\u5408\u304b\u3089\u306a\u308a\u3001\u4f4e\u3044\u6ce2\u6570\uff081300cm-\u00b9\u4ee5\u4e0b\uff09\u3067\u5f37\u304f\u5438\u53ce\u3059\u308b\u3002\u305d\u306e\u30b9\u30da\u30af\u30c8\u30eb\u306fC-H\u4f38\u7e2e\u9818\u57df\u3067\u660e\u77ad\u3067\u3042\u308b\u3002<\/li>\n<\/ul>\n<p>Nujol\u3067\u8a66\u6599\u306e\u30b9\u30da\u30af\u30c8\u30eb\u30921\u3064\u3001Fluorolube\u30672\u3064\u76ee\u306e\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5b9f\u884c\u3059\u308b\u3053\u3068\u3067\u30012\u3064\u306e\u30b9\u30da\u30af\u30c8\u30eb\u3092\u7cbe\u795e\u7684\u306b\uff08\u307e\u305f\u306f\u30bd\u30d5\u30c8\u30a6\u30a7\u30a2\u3092\u4f7f\u3063\u3066\uff09\u3064\u306a\u304e\u5408\u308f\u305b\u3001\u5168\u7bc4\u56f2\u306b\u308f\u305f\u308b\u8a66\u6599\u306e\u771f\u306e\u5438\u53ce\u3092\u793a\u3059\u30b3\u30f3\u30dd\u30b8\u30c3\u30c8\u3092\u4f5c\u6210\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002<\/p>\n<h3 id=\"the-art-of-preparing-a-mull\">\u30df\u30e5\u30eb\u306e\u6e96\u5099\u306e\u6975\u610f<\/h3>\n<ol>\n<li><strong>\u30b5\u30f3\u30d7\u30eb\u3092\u7814\u78e8\u3059\u308b\uff1a<\/strong> \u5c11\u91cf\u306e\u56fa\u4f53\u8a66\u6599\uff08\u901a\u5e382\uff5e5mg\uff09\u3092\u3001\u5e73\u3089\u3067\u78e8\u3044\u305f\u5869\u306e\u677f\uff08NaCl\u3084KBr\u306a\u3069\uff09\u306e\u4e0a\u306b\u7f6e\u304f\u304b\u3001\u30e1\u30ce\u30a6\u4e73\u9262\u306b\u5165\u308c\u308b\u3002\u3053\u308c\u3092\u7d30\u304b\u304f\u7c89\u7815\u3059\u308b\u3002<\/li>\n<li><strong>\u30de\u30ea\u30f3\u30b0\u5264\u3092\u52a0\u3048\u308b\uff1a<\/strong> \u30e0\u30ea\u30f3\u30b0\u5264\uff08\u30cc\u30b8\u30e7\u30fc\u30eb\u306a\u3069\uff09\u30921\uff5e2\u6ef4\u52a0\u3048\u308b\u3002<\/li>\n<li><strong>\u30da\u30fc\u30b9\u30c8\u306e\u4f5c\u6210<\/strong> \u30b9\u30d1\u30c1\u30e5\u30e9\u307e\u305f\u306f\u4e73\u68d2\u3092\u4f7f\u3044\u3001\u6ed1\u3089\u304b\u3067\u5747\u4e00\u306a\u30da\u30fc\u30b9\u30c8\u72b6\u306b\u306a\u308b\u307e\u3067\u3001\u7c89\u672b\u3068\u6db2\u4f53\u3092\u3059\u308a\u6df7\u305c\u308b\u3002\u6fc3\u539a\u306a\u30af\u30ea\u30fc\u30e0\u3084\u6b6f\u78e8\u304d\u7c89\u306e\u3088\u3046\u306a\u7c98\u5ea6\u306b\u3059\u308b\u3002\u76ee\u6a19\u306f\u3001\u30e0\u30ea\u30f3\u30b0\u5264\u306e\u5c48\u6298\u7387\u3092\u6d6e\u904a\u7c92\u5b50\u306e\u5c48\u6298\u7387\u306b\u8fd1\u3065\u3051\u308b\u3053\u3068\u3067\u3001\u6563\u4e71\u3092\u6700\u5c0f\u9650\u306b\u6291\u3048\u308b\u3002<\/li>\n<li><strong>\u30b5\u30f3\u30d7\u30eb\u3092\u30de\u30a6\u30f3\u30c8\u3059\u308b\uff1a<\/strong> \u30bd\u30eb\u30c8\u30d7\u30ec\u30fc\u30c8\u306b\u30da\u30fc\u30b9\u30c8\u3092\u3053\u3059\u308a\u3064\u3051\u308b\u30022\u679a\u76ee\u306e\u5869\u306e\u76bf\u3092\u4e0a\u306b\u7f6e\u304d\u3001\u4e92\u3044\u306e\u76bf\u3092\u8efd\u304f\u56de\u8ee2\u3055\u305b\u3001\u30e0\u30eb\u3092\u8584\u304f\u5747\u4e00\u306a\u819c\u306b\u5e83\u3052\u3001\u9589\u3058\u8fbc\u3081\u3089\u308c\u305f\u6c17\u6ce1\u3092\u7d5e\u308a\u51fa\u3059\u3002\u6700\u7d42\u7684\u306a\u819c\u306f\u3001\u900f\u660e\u3067\u306f\u306a\u304f\u3001\u308f\u305a\u304b\u306b\u534a\u900f\u660e\u306b\u898b\u3048\u308b\u3088\u3046\u306b\u3059\u308b\u3002<\/li>\n<li><strong>\u5206\u6790\u3059\u308b\uff1a<\/strong> \u5869\u30d7\u30ec\u30fc\u30c8\u306e\u300c\u30b5\u30f3\u30c9\u30a4\u30c3\u30c1\u300d\u3092\u5206\u5149\u8a08\u306e\u8a66\u6599\u30db\u30eb\u30c0\u30fc\u306b\u30bb\u30c3\u30c8\u3057\u3001\u30b9\u30da\u30af\u30c8\u30eb\u3092\u53d6\u5f97\u3059\u308b\u3002<\/li>\n<\/ol>\n<h3 id=\"common-pitfalls-and-how-to-avoid-them\">\u3088\u304f\u3042\u308b\u843d\u3068\u3057\u7a74\u3068\u305d\u306e\u907f\u3051\u65b9<\/h3>\n<ul>\n<li><strong>\u30de\u30ea\u30f3\u30b0\u30fb\u30a8\u30fc\u30b8\u30a7\u30f3\u30c8\u30fb\u30d4\u30fc\u30af\u30b9\u304c\u512a\u52e2\uff1a<\/strong> \u3053\u306e\u73fe\u8c61\u306f\u3001\u8a66 \u6599\u306b\u5bfe\u3057\u3066\u30df\u30e5\u30fc\u30ea\u30f3\u30b0\u5264\u304c\u591a\u3059\u304e\u308b\u5834\u5408\u306b\u8d77\u3053\u308a\u307e\u3059\u3002Nujol\u307e\u305f\u306fFluorolube\u306e\u5927\u304d\u306a\u30d0\u30f3\u30c9\u306e\u4e0a\u306b\u8a66\u6599\u306e\u30d4\u30fc\u30af\u304c\u5c0f\u3055\u304f\u8868\u793a\u3055\u308c\u307e\u3059\u3002\u30da\u30fc\u30b9\u30c8\u3092\u4f5c\u6210\u3059\u308b\u305f\u3081\u306b\u5fc5\u8981\u306a\u6700\u5c0f\u91cf\u306e\u6db2\u4f53\u306e\u307f\u3092\u4f7f\u7528\u3057\u3066\u304f\u3060\u3055\u3044\u3002<\/li>\n<li><strong>\u6563\u4e71\u3068\u4e4f\u3057\u3044\u30d4\u30fc\u30af\u5f62\u72b6\uff1a<\/strong> \u3053\u308c\u306f\u3001\u6700\u521d\u306e\u56fa\u5f62\u7269\u304c\u30de\u30ea\u30f3\u30b0\u524d\u307e\u305f\u306f\u30de\u30ea\u30f3\u30b0\u4e2d\u306b\u5341\u5206\u306b\u7d30\u304b\u304f\u7c89\u7815\u3055\u308c\u306a\u304b\u3063\u305f\u3053\u3068\u3092\u793a\u3057\u3066\u3044\u308b\u3002\u7c92\u5b50\u304c\u307e\u3060\u5927\u304d\u3059\u304e\u308b\u306e\u3060\u3002<\/li>\n<li><strong>\u30b9\u30da\u30af\u30c8\u30eb\u306a\u3057\uff08\u307e\u305f\u306f\u975e\u5e38\u306b\u5f31\u3044\u30b9\u30da\u30af\u30c8\u30eb\uff09\uff1a<\/strong> \u3053\u308c\u306f\u3001\u30de\u30eb\u304c\u539a\u3059\u304e\u3066\u5168\u4f53\u304c\u5438\u53ce\u3055\u308c\u3066\u3057\u307e\u3046\u304b\u3001\u30da\u30fc\u30b9\u30c8\u4e2d\u306e\u30b5\u30f3\u30d7\u30eb\u304c\u5358\u306b\u5341\u5206\u3067\u306a\u3044\u5834\u5408\u306b\u8d77\u3053\u308a\u3046\u308b\u3002<\/li>\n<li><strong>\u6c17\u6ce1\uff1a<\/strong> \u3053\u308c\u3089\u306f\u5927\u304d\u306a\u6563\u4e71\u3068\u7d4c\u8def\u9577\u306e\u3070\u3089\u3064\u304d\u3092\u5f15\u304d\u8d77\u3053\u3059\u53ef\u80fd\u6027\u304c\u3042\u308b\u30022\u679a\u306e\u30bd\u30eb\u30c8\u30d7\u30ec\u30fc\u30c8\u3092\u62bc\u3057\u4ed8\u3051\u308b\u969b\u306b\u306f\u3001\u5fc5\u305a\u3053\u308c\u3089\u3092\u7d5e\u308a\u51fa\u3059\u3053\u3068\u3002<\/li>\n<\/ul>\n<h2 id=\"method-3-attenuated-total-reflectance-atr-the-modern-paradigm\">\u65b9\u6cd53\uff1a\u6e1b\u8870\u5168\u53cd\u5c04\uff08ATR\uff09-\u73fe\u4ee3\u306e\u30d1\u30e9\u30c0\u30a4\u30e0<\/h2>\n<p>\u3053\u306e20\u5e74\u9593\u3067\u3001\u6e1b\u8870\u5168\u53cd\u5c04\uff08ATR\uff09\u306f\u65e5\u5e38\u7684\u306a\u8d64\u5916\u5206\u6790\u306b\u9769\u547d\u3092\u3082\u305f\u3089\u3057\u3001\u591a\u304f\u306e\u30e9\u30dc\u3067\u624b\u9593\u306e\u304b\u304b\u308b\u30da\u30ec\u30c3\u30c8\u6cd5\u3084\u30de\u30eb\u6cd5\u306b\u53d6\u3063\u3066\u4ee3\u308f\u308a\u307e\u3057\u305f\u3002ATR\u306f\u8a66\u6599\u306e\u524d\u51e6\u7406\u3092\u307b\u3068\u3093\u3069\u5fc5\u8981\u3068\u3057\u306a\u3044\u8868\u9762\u6e2c\u5b9a\u6280\u8853\u3067\u3042\u308b\u305f\u3081\u3001\u9a5a\u304f\u307b\u3069\u901f\u304f\u3001\u6c4e\u7528\u6027\u304c\u9ad8\u304f\u3001\u4f7f\u3044\u3084\u3059\u3044\u3002\u5805\u7262\u306a <a href=\"https:\/\/www.hcftir.com\/ir-sample-preparation-category\/\" rel=\"nofollow\">FTIR\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u30a2\u30af\u30bb\u30b5\u30ea\u30fc<\/a> ATR\u306f\u3001\u73fe\u4ee3\u306eFTIR\u5206\u5149\u6cd5\u306e\u4e3b\u529b\u3068\u306a\u3063\u3066\u3044\u308b\u3002<\/p>\n<h3 id=\"the-physics-of-atr-ftir\">ATR-FTIR\u306e\u7269\u7406\u5b66<\/h3>\n<p>ATR\u306e\u539f\u7406\u306f\u30a8\u30ec\u30ac\u30f3\u30c8\u3060\u3002IR\u30d3\u30fc\u30e0\u3092\u8a66\u6599\u306b\u901a\u3059\u4ee3\u308f\u308a\u306b\u3001\u30c0\u30a4\u30e4\u30e2\u30f3\u30c9\u3001\u30bb\u30ec\u30f3\u5316\u4e9c\u925b\uff08ZnSe\uff09\u3001\u30b2\u30eb\u30de\u30cb\u30a6\u30e0\uff08Ge\uff09\u306a\u3069\u306e\u9ad8\u5c48\u6298\u7387\u7d50\u6676\u306b\u30d3\u30fc\u30e0\u3092\u5c0e\u304f\u3002\u3053\u306eATR\u7d50\u6676\u306f\u3001\u8a66\u6599\u304c\u7f6e\u304b\u308c\u308b\u8868\u9762\u3067IR\u30d3\u30fc\u30e0\u304c\u5168\u53cd\u5c04\u3059\u308b\u3088\u3046\u306b\u8a2d\u8a08\u3055\u308c\u3066\u3044\u308b\u3002<\/p>\n<p>\u3057\u304b\u3057\u3001\u3053\u306e\u53cd\u5c04\u306f\u91cf\u5b50\u529b\u5b66\u7684\u306a\u610f\u5473\u3067\u306f\u5b8c\u5168\u3067\u306f\u306a\u3044\u3002\u53cd\u5c04\u306e\u6642\u70b9\u3067\u306f\u3001\u96fb\u78c1\u6ce2\u3068\u3057\u3066\u77e5\u3089\u308c\u308b <strong>\u30a8\u30d0\u30cd\u30c3\u30bb\u30f3\u30c8\u6ce2<\/strong>\u77ac\u9593\u7684\u306b\u7d50\u6676\u8868\u9762\u304b\u3089\u975e\u5e38\u306b\u77ed\u3044\u8ddd\u96e2\uff08\u901a\u5e380.5\uff5e2\u30de\u30a4\u30af\u30ed\u30e1\u30fc\u30c8\u30eb\uff09\u3092\u900f\u904e\u3057\u3001\u8a66\u6599\u306b\u5165\u5c04\u3059\u308b\u3002\u7d50\u6676\u306b\u63a5\u89e6\u3055\u305b\u305f\u8a66\u6599\u306b\u8d64\u5916\u5149\u306e\u5468\u6ce2\u6570\u3067\u5438\u53ce\u3059\u308b\u5b98\u80fd\u57fa\u304c\u3042\u308c\u3070\u3001\u3053\u306e\u8fd1\u63a5\u6ce2\u304b\u3089\u30a8\u30cd\u30eb\u30ae\u30fc\u3092\u5438\u53ce\u3059\u308b\u3002\u3053\u306e\u30a8\u30d0\u30cd\u30c3\u30bb\u30f3\u30c8\u6ce2\u306e\u300c\u6e1b\u8870\u300d\u304c\u691c\u51fa\u3055\u308c\u3001\u5f97\u3089\u308c\u305f\u4fe1\u53f7\u304c\u51e6\u7406\u3055\u308c\u3066\u8d64\u5916\u30b9\u30da\u30af\u30c8\u30eb\u304c\u751f\u6210\u3055\u308c\u308b\u3002<\/p>\n<h3 id=\"why-atr-is-so-popular-advantages-and-applications\">ATR\u304c\u4eba\u6c17\u306e\u7406\u7531\uff1a\u5229\u70b9\u3068\u5fdc\u7528<\/h3>\n<p>ATR\u306e\u4eba\u6c17\u306f\u3001\u305d\u306e\u5b9f\u7528\u7684\u306a\u5229\u70b9\u306b\u7531\u6765\u3059\u308b\uff1a<\/p>\n<ul>\n<li><strong>\u6700\u5c0f\u9650\u306e\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\uff1a<\/strong> \u307b\u3068\u3093\u3069\u306e\u56fa\u4f53\u3084\u6db2\u4f53\u3067\u306f\u3001\u30b5\u30f3\u30d7\u30eb\u3092ATR\u7d50\u6676\u306e\u4e0a\u306b\u7f6e\u304d\u3001\u5727\u529b\u3092\u304b\u3051\u3066\u78ba\u5b9f\u306b\u63a5\u89e6\u3055\u305b\u3001\u30b9\u30ad\u30e3\u30f3\u3092\u5b9f\u884c\u3059\u308b\u3060\u3051\u3067\u3059\u3002\u7c89\u672b\u306f\u76f4\u63a5\u5206\u6790\u3067\u304d\u3001\u30dd\u30ea\u30de\u30fc\u306f\u7d50\u6676\u306b\u62bc\u3057\u4ed8\u3051\u308b\u3053\u3068\u304c\u3067\u304d\u3001\u6db2\u4f53\u306f1\u6ef4\u3067\u5341\u5206\u3067\u3059\u3002<\/li>\n<li><strong>\u30b9\u30d4\u30fc\u30c9\u3060\uff1a<\/strong> KBr\u30da\u30ec\u30c3\u30c8\u3067\u306f10\uff5e20\u5206\u304b\u304b\u308b\u306e\u306b\u5bfe\u3057\u3001\u5206\u6790\u306f1\u5206\u4ee5\u5185\u3067\u5b8c\u4e86\u3059\u308b\u3002<\/li>\n<li><strong>\u6c4e\u7528\u6027\u304c\u3042\u308b\uff1a<\/strong> ATR\u306f\u3001\u786c\u3044\u7c89\u4f53\u3001\u67d4\u3089\u304b\u3044\u30dd\u30ea\u30de\u30fc\u3001\u30da\u30fc\u30b9\u30c8\u3001\u30b2\u30eb\u3001\u7d44\u7e54\u3001\u5e03\u3001\u6c34\u6eb6\u6db2\u306a\u3069\u3001\u3055\u307e\u3056\u307e\u306a\u7a2e\u985e\u306e\u30b5\u30f3\u30d7\u30eb\u3092\u6271\u3046\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002\u30d1\u30b9\u306e\u9577\u3055\u304c\u975e\u5e38\u306b\u77ed\u304f\u3001\u30b5\u30f3\u30d7\u30eb\u91cf\u306b\u4f9d\u5b58\u3057\u306a\u3044\u305f\u3081\u3001\u9ad8\u5438\u53ce\u7269\u8cea\u3084\u4e0d\u900f\u660e\u7269\u8cea\u3067\u3082\u5206\u6790\u304c\u53ef\u80fd\u3067\u3059\u3002<\/li>\n<li><strong>\u975e\u7834\u58ca\uff1a<\/strong> \u8a66\u6599\u306f\u901a\u5e38\u3001\u5206\u6790\u306b\u3088\u3063\u3066\u5909\u5316\u3059\u308b\u3053\u3068\u306f\u306a\u304f\u3001\u5b8c\u5168\u306b\u56de\u53ce\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002<\/li>\n<li><strong>\u518d\u73fe\u6027\uff1a<\/strong> \u6709\u52b9\u5149\u8def\u9577\u306f\u3001\u30b5\u30f3\u30d7\u30eb\u306e\u8abf\u88fd\u65b9\u6cd5\u3067\u306f\u306a\u304f\u3001\u7d50\u6676\u306e\u7279\u6027\u3068\u5149\u306e\u6ce2\u9577\u306b\u3088\u3063\u3066\u6c7a\u5b9a\u3055\u308c\u308b\u3002\u3053\u306e\u305f\u3081\u3001\u518d\u73fe\u6027\u306e\u9ad8\u3044\u30b9\u30da\u30af\u30c8\u30eb\u304c\u5f97\u3089\u308c\u3001\u5b9a\u91cf\u5206\u6790\u3084\u54c1\u8cea\u7ba1\u7406\u30a2\u30d7\u30ea\u30b1\u30fc\u30b7\u30e7\u30f3\u306b\u304a\u3044\u3066\u5927\u304d\u306a\u5229\u70b9\u3068\u306a\u308b\u3002<\/li>\n<\/ul>\n<h3 id=\"best-practices-for-atr-analysis\">ATR\u5206\u6790\u306e\u30d9\u30b9\u30c8\u30d7\u30e9\u30af\u30c6\u30a3\u30b9<\/h3>\n<p>ATR\u306f\u30b7\u30f3\u30d7\u30eb\u3060\u304c\u3001\u6700\u9ad8\u306e\u7d50\u679c\u3092\u51fa\u3059\u306b\u306f\u7d30\u90e8\u306b\u307e\u3067\u6ce8\u610f\u3092\u6255\u3046\u5fc5\u8981\u304c\u3042\u308b\u3002<\/p>\n<ul>\n<li><strong>\u826f\u597d\u306a\u30b3\u30f3\u30bf\u30af\u30c8\u3092\u78ba\u4fdd\u3059\u308b\uff1a<\/strong> \u30a8\u30d0\u30cd\u30c3\u30bb\u30f3\u30c8\u6ce2\u306f\u7d50\u6676\u8868\u9762\u304b\u3089\u6570\u30de\u30a4\u30af\u30ed\u30e1\u30fc\u30c8\u30eb\u3057\u304b\u5e83\u304c\u3063\u3066\u3044\u306a\u3044\u3002\u305d\u306e\u305f\u3081\u3001\u8a66\u6599\u3068\u7d50\u6676\u306e\u5bc6\u63a5\u306a\u63a5\u89e6\u304c\u7d76\u5bfe\u4e0d\u53ef\u6b20\u3067\u3042\u308b\u3002\u56fa\u4f53\u8a66\u6599\u306e\u5834\u5408\u306f\u3001\u52a0\u5727\u30af\u30e9\u30f3\u30d7\u3092\u4f7f\u7528\u3057\u3066\u8a66\u6599\u3092\u7d50\u6676\u306b\u3057\u3063\u304b\u308a\u3068\u5b89\u5b9a\u3057\u3066\u62bc\u3057\u4ed8\u3051\u307e\u3059\u3002\u63a5\u89e6\u304c\u4e0d\u5341\u5206\u3060\u3068\u3001\u30b9\u30da\u30af\u30c8\u30eb\u304c\u5f31\u304f\u30ce\u30a4\u30ba\u304c\u591a\u304f\u306a\u308a\u307e\u3059\u3002<\/li>\n<li><strong>\u30af\u30ea\u30b9\u30bf\u30eb\u3092\u5165\u5ff5\u306b\u30af\u30ea\u30fc\u30cb\u30f3\u30b0\u3059\u308b\uff1a<\/strong> ATR\u306f\u8868\u9762\u6280\u8853\u3067\u3042\u308b\u305f\u3081\u3001\u524d\u306e\u30b5\u30f3\u30d7\u30eb\u3067\u7d50\u6676\u306b\u6b8b\u3063\u305f\u6b8b\u7559\u7269\u306f\u6b21\u306e\u30b9\u30da\u30af\u30c8\u30eb\u306b\u73fe\u308c\u307e\u3059\u3002\u5404\u6e2c\u5b9a\u5f8c\u3001\u7d50\u6676\u3092\u5b8c\u5168\u306b\u30af\u30ea\u30fc\u30cb\u30f3\u30b0\u3059\u308b\u5fc5\u8981\u304c\u3042\u308a\u307e\u3059\u3002\u9069\u5207\u306a\u6eb6\u5a92\uff08\u8a66\u6599\u3084\u7d50\u6676\u306e\u6750\u8cea\u306b\u5fdc\u3058\u3066\u3001\u30a4\u30bd\u30d7\u30ed\u30d1\u30ce\u30fc\u30eb\u3084\u30a2\u30bb\u30c8\u30f3\u306a\u3069\uff09\u3067\u6e7f\u3089\u305b\u305f\u67d4\u3089\u304b\u3044\u5e03\u3084\u7dbf\u68d2\u304c\u4e00\u822c\u7684\u306b\u4f7f\u7528\u3055\u308c\u307e\u3059\u3002<\/li>\n<li><strong>\u6b63\u3057\u3044\u30af\u30ea\u30b9\u30bf\u30eb\u3092\u9078\u3076\uff1a<\/strong> \u3055\u307e\u3056\u307e\u306aATR\u7d50\u6676\u6750\u6599\u304c\u3042\u308a\u3001\u305d\u306e\u9078\u629e\u306f\u8a66\u6599\u306b\u3088\u3063\u3066\u7570\u306a\u308b\u3002\n<ul>\n<li><strong>\u30c0\u30a4\u30e4\u30e2\u30f3\u30c9<\/strong> \u975e\u5e38\u306b\u786c\u304f\u3001\u8010\u4e45\u6027\u304c\u3042\u308a\u3001\u5316\u5b66\u7684\u306b\u4e0d\u6d3b\u6027\u3002\u6700\u3082\u30aa\u30fc\u30eb\u30e9\u30a6\u30f3\u30c9\u306a\u9078\u629e\u80a2\u3067\u3059\u304c\u3001\u6700\u3082\u9ad8\u4fa1\u3067\u3082\u3042\u308a\u307e\u3059\u3002\u786c\u3044\u7c89\u4f53\u3001\u8150\u98df\u6027\u7269\u8cea\u3001\u3055\u307e\u3056\u307e\u306a\u30e6\u30fc\u30b6\u30fc\u304c\u95a2\u4e0e\u3059\u308b\u65e5\u5e38\u7684\u306a\u4f7f\u7528\u306b\u6700\u9069\u3067\u3059\u3002<\/li>\n<li><strong>\u30bb\u30ec\u30f3\u5316\u4e9c\u925b\uff08ZnSe\uff09\uff1a<\/strong> \u30c0\u30a4\u30e4\u30e2\u30f3\u30c9\u306b\u4ee3\u308f\u308b\u4e00\u822c\u7684\u3067\u5b89\u4fa1\u306a\u30c0\u30a4\u30e4\u30e2\u30f3\u30c9\u3002\u6db2\u4f53\u3001\u67d4\u3089\u304b\u3044\u7c89\u4f53\u3001\u30dd\u30ea\u30de\u30fc\u306b\u512a\u308c\u3066\u3044\u308b\u3002\u3057\u304b\u3057\u3001\u67d4\u3089\u304b\u304f\u3001\u50b7\u304c\u3064\u304d\u3084\u3059\u304f\u3001\u5f37\u9178\u3084\u5f37\u5869\u57fa\u306b\u4fb5\u3055\u308c\u307e\u3059\u3002<\/li>\n<li><strong>\u30b2\u30eb\u30de\u30cb\u30a6\u30e0\uff08Ge\uff09\uff1a<\/strong> \u5c48\u6298\u7387\u304c\u975e\u5e38\u306b\u9ad8\u3044\u305f\u3081\u3001\u6d78\u900f\u6df1\u5ea6\u304c\u975e\u5e38\u306b\u77ed\u3044\uff08\uff5e0.5 \u00b5m\uff09\u3002\u3053\u306e\u305f\u3081\u3001\u9ad8\u5438\u53ce\u6027\u30b5\u30f3\u30d7\u30eb\uff08\u70ad\u7d20\u5145\u586b\u30dd\u30ea\u30de\u30fc\u306a\u3069\uff09\u3084\u8584\u3044\u8868\u9762\u5c64\u304b\u3089\u306e\u4fe1\u53f7\u306e\u5897\u5f37\u306b\u6700\u9069\u3002<\/li>\n<\/ul>\n<\/li>\n<\/ul>\n<p><strong>\u88682\uff1a\u4e00\u822c\u7684\u306a\u8d64\u5916\u7dda\u900f\u904e\u6027\u6750\u6599\u306e\u7279\u6027<\/strong><\/p>\n<table class=\"mce-item-table\" style=\"width:100%; border-collapse: collapse;\" border=\"1\">\n<thead>\n<tr>\n<th style=\"text-align:left;\">\u7d20\u6750<\/th>\n<th style=\"text-align:left;\">\u4f7f\u7528\u53ef\u80fd\u6ce2\u6570\u7bc4\u56f2 (cm-\u00b9)<\/th>\n<th style=\"text-align:left;\">\u6c34\u6eb6\u6027<\/th>\n<th style=\"text-align:left;\">\u4ee3\u8868\u7684\u306a\u30a2\u30d7\u30ea\u30b1\u30fc\u30b7\u30e7\u30f3<\/th>\n<\/tr>\n<\/thead>\n<tbody>\n<tr>\n<td style=\"text-align:left;\"><strong>\u5869\u5316\u30ca\u30c8\u30ea\u30a6\u30e0 (NaCl)<\/strong><\/td>\n<td style=\"text-align:left;\">40,000 &#8211; 625<\/td>\n<td style=\"text-align:left;\">\u9ad8\u3044\uff08\u53ef\u6eb6\u6027\uff09<\/td>\n<td style=\"text-align:left;\">\u30c8\u30e9\u30f3\u30b9\u30df\u30c3\u30b7\u30e7\u30f3\u30a6\u30a3\u30f3\u30c9\u30a6\u3001\u30da\u30ec\u30c3\u30c8\u30de\u30c8\u30ea\u30c3\u30af\u30b9\uff08\u73fe\u5728\u306f\u5c11\u306a\u304f\u306a\u3063\u3066\u3044\u308b\uff09<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u81ed\u5316\u30ab\u30ea\u30a6\u30e0 (KBr)<\/strong><\/td>\n<td style=\"text-align:left;\">40,000 &#8211; 385<\/td>\n<td style=\"text-align:left;\">\u9ad8\u3044\uff08\u53ef\u6eb6\u6027\uff09<\/td>\n<td style=\"text-align:left;\">\u30da\u30ec\u30c3\u30c8\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u3001\u900f\u904e\u7a93<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u30d5\u30c3\u5316\u30ab\u30eb\u30b7\u30a6\u30e0(CaF\u2082)<\/strong><\/td>\n<td style=\"text-align:left;\">70,000 &#8211; 1100<\/td>\n<td style=\"text-align:left;\">\u4f4e\u3044\uff08\u4e0d\u6eb6\u6027\uff09<\/td>\n<td style=\"text-align:left;\">\u6c34\u6eb6\u6db2\u7528\u7a93\u3001\u53ef\u5909\u6e29\u5ea6\u30bb\u30eb<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u30bb\u30ec\u30f3\u5316\u4e9c\u925b\uff08ZnSe\uff09<\/strong><\/td>\n<td style=\"text-align:left;\">20,000 &#8211; 650<\/td>\n<td style=\"text-align:left;\">\u4f4e\u3044\uff08\u4e0d\u6eb6\u6027\uff09<\/td>\n<td style=\"text-align:left;\">ATR\u7d50\u6676\uff08\u30bd\u30d5\u30c8\u30b5\u30f3\u30d7\u30eb\uff09\u3001\u900f\u904e\u7a93<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u30c0\u30a4\u30e4\u30e2\u30f3\u30c9<\/strong><\/td>\n<td style=\"text-align:left;\">45,000 - 200\uff08\u30bf\u30a4\u30d7IIa\uff09<\/td>\n<td style=\"text-align:left;\">\u306a\u3057\uff08\u4e0d\u6eb6\u6027\uff09<\/td>\n<td style=\"text-align:left;\">\u30e6\u30cb\u30d0\u30fc\u30b5\u30ebATR\u7d50\u6676\uff08\u786c\u8cea\u3001\u7814\u78e8\u6027\u3001\u8150\u98df\u6027\u8a66\u6599\uff09<\/td>\n<\/tr>\n<tr>\n<td style=\"text-align:left;\"><strong>\u30b2\u30eb\u30de\u30cb\u30a6\u30e0 (Ge)<\/strong><\/td>\n<td style=\"text-align:left;\">5,500 &#8211; 830<\/td>\n<td style=\"text-align:left;\">\u306a\u3057\uff08\u4e0d\u6eb6\u6027\uff09<\/td>\n<td style=\"text-align:left;\">\u9ad8\u5438\u53ce\u8a66\u6599\u7528ATR\u7d50\u6676\uff08\u30ab\u30fc\u30dc\u30f3\u30d6\u30e9\u30c3\u30af\u306a\u3069\uff09<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<h3 id=\"understanding-atr-spectral-differences\">ATR\u30b9\u30da\u30af\u30c8\u30eb\u306e\u9055\u3044\u3092\u7406\u89e3\u3059\u308b<\/h3>\n<p>ATR\u30b9\u30da\u30af\u30c8\u30eb\u306f\u3001\uff08KBr\u30da\u30ec\u30c3\u30c8\u304b\u3089\u306e\u30b9\u30da\u30af\u30c8\u30eb\u306e\u3088\u3046\u306a\uff09\u900f\u904e\u30b9\u30da\u30af\u30c8\u30eb\u3068\u540c\u4e00\u3067\u306f\u306a\u3044\u3053\u3068\u3092\u8a8d\u8b58\u3059\u308b\u3053\u3068\u304c\u91cd\u8981\u3067\u3042\u308b\u3002\u30a8\u30d0\u30cd\u30c3\u30bb\u30f3\u30c8\u6ce2\u306e\u6027\u8cea\u4e0a\u3001\u6d78\u900f\u306e\u6df1\u3055\u306f\u5149\u306e\u6ce2\u9577\u306b\u4f9d\u5b58\u3059\u308b\u3002\u6ce2\u9577\u304c\u9577\u3044\u307b\u3069\uff08\u6ce2\u6570\u304c\u4f4e\u3044\u307b\u3069\uff09\u6d78\u900f\u306f\u6df1\u304f\u306a\u308b\u3002\u3053\u306e\u305f\u3081\u3001ATR\u30b9\u30da\u30af\u30c8\u30eb\u306e\u30d4\u30fc\u30af\u306e\u76f8\u5bfe\u5f37\u5ea6\u306f\u3001\u9ad8\u6ce2\u6570\u9818\u57df\u3068\u6bd4\u8f03\u3057\u3066\u4f4e\u6ce2\u6570\uff08\u30d5\u30a3\u30f3\u30ac\u30fc\u30d7\u30ea\u30f3\u30c8\uff09\u9818\u57df\u3067\u5897\u5f37\u3055\u308c\u308b\u3002\u3053\u308c\u306f\u4e88\u6e2c\u53ef\u80fd\u306a\u7269\u7406\u7684\u52b9\u679c\u3067\u3042\u308a\u3001\u6700\u65b0\u306e\u5206\u5149\u6cd5\u30bd\u30d5\u30c8\u30a6\u30a7\u30a2\u30d1\u30c3\u30b1\u30fc\u30b8\u306e\u591a\u304f\u306b\u306f\u3001ATR\u30b9\u30da\u30af\u30c8\u30eb\u3092\u3088\u308a\u900f\u904e\u30b9\u30da\u30af\u30c8\u30eb\u306b\u8fd1\u3044\u5f62\u306b\u5909\u63db\u3057\u3001\u904e\u53bb\u306e\u30b9\u30da\u30af\u30c8\u30eb\u30e9\u30a4\u30d6\u30e9\u30ea\u3068\u306e\u6bd4\u8f03\u3092\u5bb9\u6613\u306b\u3059\u308b\u3001\u30ef\u30f3\u30af\u30ea\u30c3\u30af\u306e\u300cATR\u88dc\u6b63\u300d\u30a2\u30eb\u30b4\u30ea\u30ba\u30e0\u304c\u542b\u307e\u308c\u3066\u3044\u307e\u3059\u3002<\/p>\n<h2 id=\"method-4-thin-film-analysis-for-polymers-and-soluble-materials\">\u65b9\u6cd54\uff1a\u30dd\u30ea\u30de\u30fc\u3068\u53ef\u6eb6\u6027\u7269\u8cea\u306e\u8584\u819c\u5206\u6790<\/h2>\n<p>\u591a\u304f\u306e\u9ad8\u5206\u5b50\u6750\u6599\u3084\u63ee\u767a\u6027\u6eb6\u5a92\u306b\u53ef\u6eb6\u306a\u56fa\u4f53\u306e\u5834\u5408\u3001\u8584\u304f\u81ea\u7acb\u3057\u305f\u30d5\u30a3\u30eb\u30e0\u3092\u4f5c\u88fd\u3059\u308b\u304b\u3001\u8d64\u5916\u7dda\u900f\u904e\u6027\u306e\u57fa\u677f\u4e0a\u306b\u30d5\u30a3\u30eb\u30e0\u3092\u30ad\u30e3\u30b9\u30c8\u3059\u308b\u3053\u3068\u304c\u3001\u5206\u6790\u306b\u6700\u9069\u306a\u65b9\u6cd5\u3067\u3042\u308b\u3002\u3053\u306e\u65b9\u6cd5\u3067\u306f\u3001KBr\u3084Nujol\u306e\u3088\u3046\u306a\u30de\u30c8\u30ea\u30c3\u30af\u30b9\u6750\u6599\u306e\u4f7f\u7528\u3092\u907f\u3051\u3001\u8a66\u6599\u305d\u306e\u3082\u306e\u306e\u7d14\u7c8b\u306a\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5f97\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002\u91cd\u8981\u306a\u8ab2\u984c\u306f\u3001\u5168\u5438\u53ce\u3092\u5f15\u304d\u8d77\u3053\u3059\u3053\u3068\u306a\u304f\u3001IR\u30d3\u30fc\u30e0\u304c\u901a\u904e\u3059\u308b\u306e\u306b\u5341\u5206\u8584\u304f\u5747\u4e00\u306a\u30d5\u30a3\u30eb\u30e0\u3092\u4f5c\u6210\u3059\u308b\u3053\u3068\u3067\u3042\u308b\u3002<\/p>\n<h3 id=\"solution-casting-method\">\u6eb6\u6db2\u92f3\u9020\u6cd5<\/h3>\n<p>\u3053\u308c\u306f\u30d5\u30a3\u30eb\u30e0\u3092\u6e96\u5099\u3059\u308b\u6700\u3082\u4e00\u822c\u7684\u306a\u65b9\u6cd5\u3067\u3042\u308b\u3002\u624b\u9806\u306f\u7c21\u5358\u3060\uff1a<\/p>\n<ol>\n<li><strong>\u30b5\u30f3\u30d7\u30eb\u3092\u6eb6\u89e3\u3059\u308b\uff1a<\/strong> \u5c11\u91cf\u306e\u8a66\u6599\uff08\u30dd\u30ea\u30b9\u30c1\u30ec\u30f3\u306a\u3069\u306e\u30dd\u30ea\u30de\u30fc\u3084\u53ef\u6eb6\u6027\u6709\u6a5f\u56fa\u4f53\u306a\u3069\uff09\u3092\u9069\u5f53\u306a\u63ee\u767a\u6027\u6eb6\u5a92\u306b\u6eb6\u304b\u3059\u3002\u6eb6\u5a92\u306e\u9078\u629e\u306f\u975e\u5e38\u306b\u91cd\u8981\u3067\u3001\u8a66\u6599\u3092\u5b8c\u5168\u306b\u6eb6\u89e3\u3057\u3001\u6b8b\u6e23\u3092\u6b8b\u3055\u305a\u306b\u304d\u308c\u3044\u306b\u84b8\u767a\u3057\u3001\u8a66\u6599\u3068\u53cd\u5fdc\u3057\u306a\u3044\u3082\u306e\u3067\u306a\u3051\u308c\u3070\u306a\u3089\u306a\u3044\u3002\u4e00\u822c\u7684\u306a\u9078\u629e\u80a2\u3068\u3057\u3066\u306f\u3001\u30b8\u30af\u30ed\u30ed\u30e1\u30bf\u30f3\u3001\u30af\u30ed\u30ed\u30db\u30eb\u30e0\u3001\u30a2\u30bb\u30c8\u30f3\u3001\u30c8\u30eb\u30a8\u30f3\u306a\u3069\u304c\u3042\u308b\u3002<\/li>\n<li><strong>\u6620\u753b\u306e\u30ad\u30e3\u30b9\u30c8<\/strong> \u3067\u304d\u305f\u6eb6\u6db2\u3092\u6e05\u6f54\u306a\u5e73\u3089\u306a\u9762\u306b\u6570\u6ef4\u5782\u3089\u3059\u3002\u3053\u308c\u306f\u3001\u8d64\u5916\u900f\u904e\u6027\u306e\u5869\u30d7\u30ec\u30fc\u30c8\uff08KBr\u307e\u305f\u306fNaCl\uff09\u3067\u3082\u3088\u3044\u3057\u3001\u30ac\u30e9\u30b9\u88fd\u9855\u5fae\u93e1\u30b9\u30e9\u30a4\u30c9\u306e\u3088\u3046\u306a\u4f7f\u3044\u6368\u3066\u306e\u8868\u9762\u3067\u3082\u3088\u304f\u3001\u5f8c\u3067\u30d5\u30a3\u30eb\u30e0\u3092\u306f\u304c\u3059\u3053\u3068\u304c\u3067\u304d\u308b\u3002<\/li>\n<li><strong>\u6eb6\u5a92\u3092\u84b8\u767a\u3055\u305b\u308b\uff1a<\/strong> \u6eb6\u5a92\u3092\u3086\u3063\u304f\u308a\u3068\u5b8c\u5168\u306b\u84b8\u767a\u3055\u305b\u308b\u3002\u3053\u308c\u306f\u5ba4\u6e29\u3067\u3001\u6642\u306b\u306f\u7a92\u7d20\u306e\u7a4f\u3084\u304b\u306a\u6d41\u308c\u306e\u4e0b\u3067\u3001\u3042\u308b\u3044\u306f\u30d2\u30e5\u30fc\u30e0\u30d5\u30fc\u30c9\u306e\u4e2d\u3067\u884c\u3046\u3053\u3068\u304c\u3067\u304d\u308b\u3002\u3086\u3063\u304f\u308a\u3068\u84b8\u767a\u3055\u305b\u308b\u3053\u3068\u3067\u3001\u3088\u308a\u5747\u4e00\u306a\u819c\u3092\u5f62\u6210\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002\u3053\u306e\u5de5\u7a0b\u3092\u6025\u3050\u3068\u3001\u6c17\u6ce1\u304c\u5165\u3063\u305f\u308a\u3001\u8868\u9762\u304c\u4e0d\u5747\u4e00\u3067\u3072\u3073\u5272\u308c\u305f\u308a\u3059\u308b\u3053\u3068\u304c\u3042\u308b\u3002<\/li>\n<li><strong>\u5206\u6790\u3059\u308b\uff1a<\/strong> \u5869\u30d7\u30ec\u30fc\u30c8\u306b\u30ad\u30e3\u30b9\u30c8\u3057\u305f\u5834\u5408\u306f\u3001\u30d7\u30ec\u30fc\u30c8\u3092\u5206\u5149\u8a08\u306b\u76f4\u63a5\u53d6\u308a\u4ed8\u3051\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002\u81ea\u7acb\u578b\u30d5\u30a3\u30eb\u30e0\u3092\u4f5c\u6210\u3057\u305f\u5834\u5408\uff08\u30ac\u30e9\u30b9\u304b\u3089\u5265\u304c\u3059\u306a\u3069\uff09\u3001\u539a\u7d19\u3084\u91d1\u5c5e\u88fd\u306e\u30db\u30eb\u30c0\u30fc\u306b\u53d6\u308a\u4ed8\u3051\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002<\/li>\n<\/ol>\n<p>\u819c\u539a\u306f\u3001\u6eb6\u6db2\u306e\u6fc3\u5ea6\u3068\u84b8\u7740\u91cf\u306b\u3088\u3063\u3066\u30b3\u30f3\u30c8\u30ed\u30fc\u30eb\u3055\u308c\u308b\u3002\u826f\u597d\u306a\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5f97\u308b\u305f\u3081\u306e\u7406\u60f3\u7684\u306a\u819c\u539a\u3092\u5f97\u308b\u306b\u306f\u3001\u6570\u56de\u306e\u8a66\u884c\u304c\u5fc5\u8981\u306a\u5834\u5408\u304c\u3042\u308b\u3002<\/p>\n<h3 id=\"melt-casting-for-thermoplastics\">\u71b1\u53ef\u5851\u6027\u30d7\u30e9\u30b9\u30c1\u30c3\u30af\u306e\u6eb6\u878d\u92f3\u9020<\/h3>\n<p>\u9069\u5ea6\u306a\u6e29\u5ea6\u3067\u5206\u89e3\u305b\u305a\u306b\u6eb6\u878d\u3059\u308b\u71b1\u53ef\u5851\u6027\u30dd\u30ea\u30de\u30fc\u306e\u5834\u5408\u3001\u6eb6\u878d\u7269\u304b\u3089\u30d5\u30a3\u30eb\u30e0\u3092\u5f62\u6210\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002<\/p>\n<ol>\n<li>\u5c11\u91cf\u306e\u30dd\u30ea\u30de\u30fc\u7c89\u672b\u307e\u305f\u306f\u30da\u30ec\u30c3\u30c8\u30922\u679a\u306e\u5869\u30d7\u30ec\u30fc\u30c8\u306e\u9593\u306b\u7f6e\u304f\u3002<\/li>\n<li>\u30db\u30c3\u30c8\u30d7\u30ec\u30fc\u30c8\u3067\u30a2\u30bb\u30f3\u30d6\u30ea\u3092\u30dd\u30ea\u30de\u30fc\u306e\u878d\u70b9\u304e\u308a\u304e\u308a\u307e\u3067\u52a0\u71b1\u3059\u308b\u3002<\/li>\n<li>\u30c8\u30c3\u30d7\u30d7\u30ec\u30fc\u30c8\u306b\u512a\u3057\u304f\u5727\u529b\u3092\u304b\u3051\u3001\u6eb6\u878d\u30dd\u30ea\u30de\u30fc\u3092\u8584\u304f\u5747\u4e00\u306a\u30d5\u30a3\u30eb\u30e0\u306b\u7d5e\u308b\u3002<\/li>\n<li>\u5ba4\u6e29\u307e\u3067\u3086\u3063\u304f\u308a\u51b7\u307e\u3059\u3002<\/li>\n<li>\u51fa\u6765\u4e0a\u304c\u3063\u305f\u30b5\u30f3\u30c9\u30a4\u30c3\u30c1\u306f\u76f4\u63a5\u5206\u6790\u3067\u304d\u308b\u3002<\/li>\n<\/ol>\n<p>\u3053\u306e\u65b9\u6cd5\u306f\u8fc5\u901f\u3067\u6eb6\u5a92\u3092\u4f7f\u7528\u3057\u306a\u3044\u304c\u3001\u71b1\u7684\u306b\u5b89\u5b9a\u306a\u30dd\u30ea\u30de\u30fc\u306b\u306e\u307f\u9069\u3057\u3066\u3044\u308b\u3002<\/p>\n<h3 id=\"considerations-for-film-preparation\">\u30d5\u30a3\u30eb\u30e0\u306e\u6e96\u5099\u306b\u95a2\u3059\u308b\u8003\u5bdf<\/h3>\n<p>\u30d5\u30a3\u30eb\u30e0\u306e\u30b9\u30da\u30af\u30c8\u30e9\u30e0\u306e\u8cea\u306f\u3001\u30d5\u30a3\u30eb\u30e0\u306e\u8cea\u306b\u5b8c\u5168\u306b\u4f9d\u5b58\u3059\u308b\u3002<\/p>\n<ul>\n<li><strong>\u539a\u307f\u3068\u5747\u4e00\u6027\uff1a<\/strong> \u7406\u60f3\u7684\u306a\u819c\u539a\u306f\u901a\u5e385\uff5e20\u03bcm\u3067\u3042\u308b\u3002\u819c\u539a\u304c\u539a\u3059\u304e\u308b\u3068\u3001\u4e3b\u8981\u306a\u30d4\u30fc\u30af\u304c\u30d5\u30e9\u30c3\u30c8\u30c8\u30c3\u30d7\u306b\u306a\u308b\u3002\u819c\u539a\u304c\u8584\u3059\u304e\u308b\u3068\u30b7\u30b0\u30ca\u30eb\u304c\u5f31\u304f\u306a\u308b\u3002\u819c\u539a\u304c\u5747\u4e00\u3067\u306a\u3044\u3068\u3001\u30d9\u30fc\u30b9\u30e9\u30a4\u30f3\u304c\u306a\u3060\u3089\u304b\u306b\u306a\u308b\u3002<\/li>\n<li><strong>\u5e72\u6e09\u7e1e\uff1a<\/strong> \u5e73\u884c\u306a\u8868\u9762\u3092\u6301\u3064\u975e\u5e38\u306b\u6ed1\u3089\u304b\u3067\u5747\u4e00\u306a\u30d5\u30a3\u30eb\u30e0\u306f\u3001\u5149\u5b66\u30a8\u30bf\u30ed\u30f3\u3068\u3057\u3066\u6a5f\u80fd\u3057\u3001\u30b9\u30da\u30af\u30c8\u30eb\u306e\u30d9\u30fc\u30b9\u30e9\u30a4\u30f3\u3092\u6a2a\u5207\u308b\u6b63\u5f26\u6ce2\u72b6\u306e\u30ea\u30c3\u30d7\u30eb\uff08\u5e72\u6e09\u7e1e\uff09\u3092\u767a\u751f\u3055\u305b\u308b\u3053\u3068\u304c\u3042\u308a\u307e\u3059\u3002\u3053\u306e\u5e72\u6e09\u7e1e\u306f\u30bd\u30d5\u30c8\u30a6\u30a7\u30a2\u3067\u9664\u53bb\u3067\u304d\u308b\u5834\u5408\u3082\u3042\u308a\u307e\u3059\u304c\u3001\u5b8c\u5168\u3067\u306a\u3044\u8868\u9762\u3092\u308f\u305a\u304b\u306b\u4f5c\u308b\u304b\u3001\u30d3\u30fc\u30e0\u5185\u3067\u8a66\u6599\u3092\u308f\u305a\u304b\u306b\u50be\u3051\u308b\u3053\u3068\u306b\u3088\u3063\u3066\u3001\u5e72\u6e09\u7e1e\u3092\u56de\u907f\u3057\u305f\u65b9\u304c\u3088\u3044\u5834\u5408\u304c\u591a\u304f\u3042\u308a\u307e\u3059\u3002<\/li>\n<li><strong>\u6b8b\u7559\u6eb6\u5264\uff1a<\/strong> \u30ad\u30e3\u30b9\u30c6\u30a3\u30f3\u30b0\u6eb6\u5a92\u304c\u3059\u3079\u3066\u84b8\u767a\u3057\u3066\u3044\u308b\u3053\u3068\u304c\u7d76\u5bfe\u4e0d\u53ef\u6b20\u3067\u3042\u308b\u3002\u305d\u3046\u3057\u306a\u3044\u3068\u3001\u30b9\u30da\u30af\u30c8\u30eb\u306b\u6eb6\u5a92\u306e\u30d4\u30fc\u30af\u304c\u73fe\u308c\u308b\u3002\u771f\u7a7a\u30aa\u30fc\u30d6\u30f3\u3067\u7a4f\u3084\u304b\u306b\u6e29\u3081\u308b\u3053\u3068\u3067\u3001\u6eb6\u5a92\u306e\u6700\u5f8c\u306e\u75d5\u8de1\u3092\u53d6\u308a\u9664\u304f\u3053\u3068\u304c\u3067\u304d\u308b\u3002<\/li>\n<\/ul>\n<h2 id=\"method-5-the-direct-examination-of-liquids-and-solutions\">\u65b9\u6cd55\uff1a\u6db2\u4f53\u3068\u6eb6\u6db2\u306e\u76f4\u63a5\u691c\u67fb<\/h2>\n<p>IR\u5206\u6790\u7528\u306e\u6db2\u4f53\u30b5\u30f3\u30d7\u30eb\u306e\u8abf\u88fd\u306f\u3001\u3059\u3079\u3066\u306e\u624b\u9806\u306e\u4e2d\u3067\u6700\u3082\u7c21\u5358\u306a\u5834\u5408\u304c\u591a\u3044\u3002\u4e3b\u306a\u9078\u629e\u80a2\u306f\u3001\u6db2\u4f53\u3092 \"\u30cb\u30fc\u30c8\"\uff08\u7d14\u7c8b\u306a\u307e\u307e\uff09\u5206\u6790\u3059\u308b\u304b\u3001\u8d64\u5916\u900f\u904e\u6027\u6eb6\u5a92\u306b\u6eb6\u304b\u3057\u305f\u6eb6\u6db2\u3068\u3057\u3066\u5206\u6790\u3059\u308b\u304b\u3067\u3042\u308b\u3002\u3053\u306e\u9078\u629e\u306f\u3001\u6db2\u4f53\u306e\u7279\u6027\u3001\u7279\u306b\u7c98\u5ea6\u3068\u8d64\u5916\u5438\u5149\u5f37\u5ea6\u306b\u3088\u3063\u3066\u6c7a\u307e\u308b\u3002<\/p>\n<h3 id=\"neat-liquid-analysis-using-salt-plates\">\u30bd\u30eb\u30c8\u30d7\u30ec\u30fc\u30c8\u3092\u7528\u3044\u305f\u6e05\u6f84\u6db2\u5206\u6790<\/h3>\n<p>\u307b\u3068\u3093\u3069\u306e\u4e0d\u63ee\u767a\u6027\u6709\u6a5f\u6db2\u4f53\u306b\u3068\u3063\u3066\u3001\u3053\u308c\u306f\u8003\u3048\u5f97\u308b\u9650\u308a\u6700\u3082\u5358\u7d14\u306a\u65b9\u6cd5\u3067\u3042\u308b\u3002<\/p>\n<ol>\n<li>\u6e05\u6f54\u3067\u4e7e\u71e5\u3057\u305f\u5869\u30d7\u30ec\u30fc\u30c8\uff08NaCl\u307e\u305f\u306fKBr\u304c\u4e00\u822c\u7684\u3067\u5b89\u4fa1\uff09\u3092\u5e73\u3089\u306a\u9762\u306b1\u679a\u7f6e\u304f\u3002<\/li>\n<li>\u30cb\u30fc\u30c8\u30ea\u30ad\u30c3\u30c9\u3092\u76bf\u306e\u4e2d\u592e\u306b1\u6ef4\u52a0\u3048\u308b\u3002<\/li>\n<li>2\u679a\u76ee\u306e\u5869\u76bf\u3092\u4e0a\u306b\u7f6e\u304f\u3002<\/li>\n<li>\u6bdb\u7d30\u7ba1\u73fe\u8c61\u306b\u3088\u308a\u3001\u6db2\u4f53\u304c\u30d7\u30ec\u30fc\u30c8\u306e\u9593\u306b\u8584\u3044\u30d5\u30a3\u30eb\u30e0\u72b6\u306b\u5f15\u304d\u8fbc\u307e\u308c\u308b\u3002\u7de9\u3084\u304b\u306a\u5727\u529b\u3092\u52a0\u3048\u3066\u539a\u3055\u3092\u8abf\u6574\u3059\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002\u30d1\u30b9\u306e\u9577\u3055\u306f\u4e00\u822c\u7684\u306b\u975e\u5e38\u306b\u77ed\u304f\u30010.01\uff5e0.05mm\u7a0b\u5ea6\u3067\u3059\u3002<\/li>\n<li>\u30a2\u30bb\u30f3\u30d6\u30ea\u3092\u5206\u5149\u8a08&#039;\u306e\u30e6\u30cb\u30d0\u30fc\u30b5\u30eb\u30b9\u30e9\u30a4\u30c9\u30de\u30a6\u30f3\u30c8\u306b\u7f6e\u304d\u3001\u30b9\u30da\u30af\u30c8\u30eb\u3092\u53ce\u96c6\u3057\u307e\u3059\u3002<\/li>\n<\/ol>\n<p>\u3053\u306e\u65b9\u6cd5\u306f\u9ad8\u901f\u3067\u6eb6\u5a92\u3092\u5fc5\u8981\u3068\u3057\u306a\u3044\u304c\u3001\u63ee\u767a\u6027\u306e\u6db2\u4f53\uff08\u84b8\u767a\u3057\u3066\u3057\u307e\u3046\uff09\u3084\u5b9a\u91cf\u5206\u6790\u306b\u306f\u9069\u3055\u306a\u3044\u3002<\/p>\n<h3 id=\"solution-analysis-using-sealed-cells\">\u5bc6\u9589\u30bb\u30eb\u3092\u7528\u3044\u305f\u6eb6\u6db2\u5206\u6790<\/h3>\n<p>\u5b9a\u91cf\u5206\u6790\u3084\u63ee\u767a\u6027\u6db2\u4f53\u306e\u5206\u6790\u306b\u306f\u3001\u65e2\u77e5\u306e\u4e00\u5b9a\u306e\u7d4c\u8def\u9577\u3092\u6301\u3064\u5bc6\u9589\u578b\u30bb\u30eb\u304c\u5fc5\u8981\u3067\u3042\u308b\u3002\u3053\u306e\u3088\u3046\u306a\u30bb\u30eb\u306f\u3001\u3057\u3070\u3057\u3070\u300c\u8131\u7740\u5f0f\u300d\u307e\u305f\u306f\u300c\u5bc6\u9589\u5f0f\u300d\u3068\u547c\u3070\u308c\u3001\u7279\u5b9a\u306e\u539a\u3055\uff08\u4f8b\u3048\u3070\u30010.1mm\u30010.5mm\u30011.0mm\uff09\u306e\u8584\u3044\u30b9\u30da\u30fc\u30b5\u30fc\uff08\u30ac\u30b9\u30b1\u30c3\u30c8\uff09\u3067\u4ed5\u5207\u3089\u308c\u305f2\u3064\u306e\u8d64\u5916\u7dda\u900f\u904e\u7a93\u3067\u69cb\u6210\u3055\u308c\u3066\u3044\u307e\u3059\u3002<\/p>\n<ol>\n<li><strong>\u6eb6\u6db2\u3092\u6e96\u5099\u3059\u308b\uff1a<\/strong> \u8a66\u6599\uff08\u6db2\u4f53\u3067\u3082\u56fa\u4f53\u3067\u3082\u3088\u3044\uff09\u3092\u9069\u5f53\u306aIR\u900f\u660e\u6eb6\u5a92\u306b\u6eb6\u89e3\u3057\u3001\u65e2\u77e5\u306e\u6fc3\u5ea6\uff08\u4f8b\u3048\u30705-10% w\/v\uff09\u306b\u3059\u308b\u3002<\/li>\n<li><strong>\u30bb\u30eb\u3092\u57cb\u3081\u308b\uff1a<\/strong> \u30bb\u30eb\u306b\u306f\u6ce8\u5165\u53e3\u3068\u6392\u51fa\u53e3\u304c\u3042\u308b\uff08\u591a\u304f\u306f\u30eb\u30a2\u30fc\u30ed\u30c3\u30af\u7d99\u624b\uff09\u3002\u30b7\u30ea\u30f3\u30b8\u3092\u7528\u3044\u3001\u6eb6\u6db2\u3092\u4e00\u65b9\u306e\u30dd\u30fc\u30c8\u306b\u6ce8\u5165\u3057\u3001\u30bb\u30eb\u304c\u6e80 \u305f\u3055\u308c\u3001\u3082\u3046\u4e00\u65b9\u306e\u30dd\u30fc\u30c8\u304b\u3089\u6db2\u4f53\u304c\u51fa\u3066\u304f\u308b\u307e\u3067\u6ce8\u5165\u3059\u308b\u3002\u305d\u306e\u5f8c\u3001\u30dd\u30fc\u30c8\u306f\u30d7\u30e9\u30b0\u3067\u5bc6\u9589\u3055\u308c\u308b\u3002<\/li>\n<li><strong>\u5206\u6790\u3059\u308b\uff1a<\/strong> \u5145\u586b\u3057\u305f\u30bb\u30eb\u3092\u5206\u5149\u8a08\u306b\u30bb\u30c3\u30c8\u3059\u308b\u3002\u307e\u305a\u3001\u307e\u3063\u305f\u304f\u540c\u3058\u30bb\u30eb\u3067\u7d14\u6eb6\u5a92\u306e\u30d0\u30c3\u30af\u30b0\u30e9\u30a6\u30f3\u30c9\u30b9\u30da\u30af\u30c8\u30eb\u3092\u6e2c\u5b9a\u3059\u308b\u3053\u3068\u304c\u91cd\u8981\u3067\u3059\u3002\u3059\u308b\u3068\u3001\u30bd\u30d5\u30c8\u30a6\u30a7\u30a2\u304c\u81ea\u52d5\u7684\u306b\u30b5\u30f3\u30d7\u30eb\u6eb6\u6db2\u306e\u30b9\u30da\u30af\u30c8\u30eb\u304b\u3089\u6eb6\u5a92\u306e\u5438\u5149\u5ea6\u3092\u5dee\u3057\u5f15\u304d\u3001\u6eb6\u8cea\u306e\u307f\u306e\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5f97\u308b\u3053\u3068\u304c\u3067\u304d\u307e\u3059\u3002<\/li>\n<\/ol>\n<h3 id=\"choosing-solvents-and-cell-materials\">\u6eb6\u5a92\u3068\u30bb\u30eb\u6750\u6599\u306e\u9078\u629e<\/h3>\n<p>\u6eb6\u5a92\u306e\u9078\u629e\u306f\u59a5\u5354\u306e\u7523\u7269\u3067\u3042\u308b\u3002\u7406\u60f3\u7684\u306a\u6eb6\u5a92\u306f\u4e2d\u8d64\u5916\u57df\u3067\u5b8c\u5168\u306b\u900f\u660e\u306a\u3082\u306e\u3060\u304c\u3001\u305d\u306e\u3088\u3046\u306a\u6eb6\u5a92\u306f\u5b58\u5728\u3057\u306a\u3044\u3002<\/p>\n<ul>\n<li><strong>\u56db\u5869\u5316\u70ad\u7d20\uff08CCl_2084\uff09\uff1a<\/strong> \u5e83\u3044\u9818\u57df\u3067\u900f\u660e\u306a\u512a\u308c\u305f\u6eb6\u5264\u3060\u304c\u3001800cm-\u00b9\u4ed8\u8fd1\u306b\u5f37\u3044\u5438\u53ce\u304c\u3042\u308b\u3002\u6bd2\u6027\u3082\u5f37\u304f\u3001\u73fe\u5728\u3067\u306f\u591a\u304f\u306e\u5730\u57df\u3067\u4f7f\u7528\u304c\u5236\u9650\u3055\u308c\u3066\u3044\u308b\u3002<\/li>\n<li><strong>\u30af\u30ed\u30ed\u30db\u30eb\u30e0\uff08CHCl\u2083\uff09\u3068\u30b8\u30af\u30ed\u30ed\u30e1\u30bf\u30f3\uff08CH\u2082Cl\u2082\uff09\uff1a<\/strong> \u6c4e\u7528\u6eb6\u5264\u3068\u3057\u3066\u512a\u308c\u3066\u3044\u308b\u304c\u3001C-H\u5c48\u66f2\u3068C-Cl\u4f38\u7e2e\u9818\u57df\u306b\u5927\u304d\u306a\u5438\u53ce\u5e2f\u304c\u3042\u308b\u3002<\/li>\n<li><strong>\u4e8c\u786b\u5316\u70ad\u7d20\uff08CS\u2082\uff09\uff1a<\/strong> CCl_2084\u304c\u5438\u53ce\u3059\u308b\u9818\u57df\u3067\u306f\u900f\u660e\u3067\u3042\u308b\u305f\u3081\u3001CCl_2084\u3092\u88dc\u3046\u306e\u306b\u9069\u3057\u3066\u3044\u308b\u3002\u3057\u304b\u3057\u3001\u5f15\u706b\u6027\u3001\u63ee\u767a\u6027\u3001\u6bd2\u6027\u304c\u9ad8\u3044\u3002<\/li>\n<\/ul>\n<p>\u30bb\u30eb\u7a93\u6750\u306f\u3001\u4f7f\u7528\u3059\u308b\u6eb6\u5a92\u306b\u5bfe\u3057\u3066\u4e0d\u6d3b\u6027\u3067\u306a\u3051\u308c\u3070\u306a\u3089\u306a\u3044\u3002NaCl\u3084KBr\u306f\u5b89\u4fa1\u3060\u304c\u3001\u6c34\u3084\u30a2\u30eb\u30b3\u30fc\u30eb\u306b\u6eb6\u3051\u308b\u3002\u6c34\u6eb6\u6db2\u3084\u30a2\u30eb\u30b3\u30fc\u30eb\u6eb6\u6db2\u3092\u4f7f\u7528\u3059\u308b\u5834\u5408\u306f\u3001\u30d5\u30c3\u5316\u30ab\u30eb\u30b7\u30a6\u30e0\uff08CaF\u2082\uff09\u3084\u30bb\u30ec\u30f3\u5316\u4e9c\u925b\uff08ZnSe\uff09\u306e\u3088\u3046\u306a\u4e0d\u6eb6\u6027\u306e\u7a93\u6750\u3092\u4f7f\u7528\u3057\u306a\u3051\u308c\u3070\u306a\u3089\u306a\u3044\u3002\u30bb\u30eb\u306e\u5149\u8def\u9577\u306f\u3001\u4e88\u60f3\u3055\u308c\u308b\u6fc3\u5ea6\u306b\u57fa\u3065\u3044\u3066\u9078\u629e\u3055\u308c\u308b\uff1a\u3088\u308a\u5e0c\u8584\u306a\u6eb6\u6db2\u306f\u3001\u9069\u5207\u306a\u4fe1\u53f7\u3092\u751f\u6210\u3059\u308b\u305f\u3081\u306b\u9577\u3044\u5149\u8def\u9577\u3092\u5fc5\u8981\u3068\u3059\u308b\u3002<\/p>\n<h2 id=\"method-6-capturing-the-freedom-of-gas-phase-molecules\">\u65b9\u6cd56\uff1a\u6c17\u76f8\u5206\u5b50\u306e\u81ea\u7531\u5ea6\u3092\u6349\u3048\u308b<\/h2>\n<p>\u6c17\u76f8\u306e\u8d64\u5916\u5206\u5149\u6cd5\u306f\u3001\u5206\u5b50\u306e\u69cb\u9020\u3068\u30c0\u30a4\u30ca\u30df\u30af\u30b9\u3092\u77e5\u308b\u305f\u3081\u306e\u30e6\u30cb\u30fc\u30af\u306a\u7a93\u3092\u63d0\u4f9b\u3059\u308b\u3002\u6c17\u76f8\u306e\u5206\u5b50\u306f\u96e2\u308c\u3066\u3044\u3066\u81ea\u7531\u306b\u56de\u8ee2\u3059\u308b\u305f\u3081\u3001\u305d\u306e\u8d64\u5916\u30b9\u30da\u30af\u30c8\u30eb\u306f\u51dd\u7e2e\u76f8\uff08\u6db2\u4f53\u3084\u56fa\u4f53\uff09\u3068\u306f\u7570\u306a\u308b\u3002\u6c17\u76f8\u306e\u30b9\u30da\u30af\u30c8\u30eb\u306f\u3001\u5e45\u5e83\u3044\u5438\u53ce\u5e2f\u306e\u4ee3\u308f\u308a\u306b\u3001\u632f\u52d5\u30a8\u30cd\u30eb\u30ae\u30fc\u6e96\u4f4d\u3068\u56de\u8ee2\u30a8\u30cd\u30eb\u30ae\u30fc\u6e96\u4f4d\u306e\u540c\u6642\u5909\u5316\u306b\u5bfe\u5fdc\u3059\u308b\u3001\u30b7\u30e3\u30fc\u30d7\u3067\u660e\u78ba\u306a\u7dda\u3092\u793a\u3059\u3002<\/p>\n<h3 id=\"the-gas-cell-design-and-function\">\u30ac\u30b9\u96fb\u6c60\uff1a\u8a2d\u8a08\u3068\u6a5f\u80fd<\/h3>\n<p>\u6c17\u4f53\u306e\u5bc6\u5ea6\u306f\u975e\u5e38\u306b\u4f4e\u3044\u305f\u3081\u3001\u691c\u51fa\u53ef\u80fd\u306a\u5438\u53ce\u3092\u751f\u307f\u51fa\u3059\u306e\u306b\u5341\u5206\u306a\u5206\u5b50\u3092\u8d64\u5916\u7dda\u30d3\u30fc\u30e0\u306b\u53d6\u308a\u8fbc\u3080\u306b\u306f\u3001\u9577\u3044\u5149\u8def\u9577\u304c\u5fc5\u8981\u3068\u306a\u308b\u3002\u5178\u578b\u7684\u306a\u30ac\u30b9\u30bb\u30eb\u306f\u3001\u4e21\u7aef\u306b\u8d64\u5916\u7dda\u900f\u904e\u7a93\u306e\u3042\u308b\u5186\u7b52\u5f62\u306e\u7ba1\uff08\u30ac\u30e9\u30b9\u3084\u91d1\u5c5e\u88fd\u304c\u591a\u3044\uff09\u3067\u3042\u308b\u3002<\/p>\n<ul>\n<li><strong>\u5358\u7d14\u306a\u6c17\u4f53\u96fb\u6c60\uff1a<\/strong> \u7d14\u30ac\u30b9\u3084\u6fc3\u539a\u6df7\u5408\u30ac\u30b9\u306e\u30eb\u30fc\u30c1\u30f3\u5206\u6790\u306b\u306f\u30015cm\u308410cm\u306e\u56fa\u5b9a\u30d1\u30b9\u9577\u306e\u30bb\u30eb\u3067\u5341\u5206\u306a\u5834\u5408\u304c\u591a\u3044\u3002<\/li>\n<li><strong>\u30ed\u30f3\u30b0\u30d1\u30b9\u30fb\u30ac\u30b9\u30bb\u30eb<\/strong> \u5fae\u91cf\u30ac\u30b9\u5206\u6790\uff08\u74b0\u5883\u30e2\u30cb\u30bf\u30ea\u30f3\u30b0\u306a\u3069\uff09\u306e\u5834\u5408\u306f\u3001\u3082\u3063\u3068\u9577\u3044\u7d4c\u8def\u9577\u304c\u5fc5\u8981\u306b\u306a\u308b\u3002\u3053\u306e\u3088\u3046\u306a\u30bb\u30eb\u3067\u306f\u3001\u5185\u90e8\u30df\u30e9\u30fc\u3092\u4f7f\u7528\u3057\u3066\u3001\u8d64\u5916\u7dda\u30d3\u30fc\u30e0\u3092\u30ac\u30b9\u4e2d\u3067\u4f55\u5ea6\u3082\u53cd\u5c04\u3055\u305b\u3066\u304b\u3089\u51fa\u5c04\u3057\u307e\u3059\u3002\u3053\u308c\u306b\u3088\u308a\u3001\u7269\u7406\u7684\u306b\u30b3\u30f3\u30d1\u30af\u30c8\u306a\u30bb\u30eb\u5185\u3067\u4f55\u30e1\u30fc\u30c8\u30eb\u3082\u306e\u6709\u52b9\u5149\u8def\u9577\uff0810\u30e1\u30fc\u30c8\u30eb\u300120\u30e1\u30fc\u30c8\u30eb\u3001\u3042\u308b\u3044\u306f100\u30e1\u30fc\u30c8\u30eb\uff09\u3092\u5b9f\u73fe\u3067\u304d\u308b\u3002<\/li>\n<\/ul>\n<p>\u30bb\u30eb\u306e\u7a93\u306f\u901a\u5e38\u3001KBr\u307e\u305f\u306fNaCl\u3067\u3067\u304d\u3066\u304a\u308a\u3001\u6c4e\u7528\u6027\u304c\u3042\u308b\u3002\u30bb\u30eb\u306f\u771f\u7a7a\u6c17\u5bc6\u3067\u306a\u3051\u308c\u3070\u306a\u3089\u305a\u3001\u30bb\u30eb\u5185\u3092\u6392\u6c17\u3057\u3001\u30ac\u30b9\u8a66\u6599\u3092\u5c0e\u5165\u3059\u308b\u305f\u3081\u306e\u30dd\u30fc\u30c8\u304c\u5fc5\u8981\u3067\u3042\u308b\u3002<\/p>\n<h3 id=\"preparing-a-gas-sample\">\u30ac\u30b9\u30b5\u30f3\u30d7\u30eb\u306e\u6e96\u5099<\/h3>\n<p>\u8abf\u88fd\u30d7\u30ed\u30bb\u30b9\u3067\u306f\u3001\u30bb\u30eb\u5185\u306e\u30ac\u30b9\u306e\u5727\u529b\u3092\u30b3\u30f3\u30c8\u30ed\u30fc\u30eb\u3059\u308b\u3002<\/p>\n<ol>\n<li><strong>\u72ec\u623f\u304b\u3089\u907f\u96e3\u3059\u308b\uff1a<\/strong> \u30ac\u30b9\u30bb\u30eb\u306f\u771f\u7a7a\u30e9\u30a4\u30f3\u306b\u63a5\u7d9a\u3055\u308c\u3001\u7a7a\u6c17\u3084\u305d\u306e\u4ed6\u306e\u6b8b\u7559\u30ac\u30b9\u3092\u9664\u53bb\u3059\u308b\u305f\u3081\u306b\u6392\u6c17\u3055\u308c\u308b\u3002\u7a7a\u306e\u30bb\u30eb\u306e\u30d0\u30c3\u30af\u30b0\u30e9\u30a6\u30f3\u30c9\u30b9\u30da\u30af\u30c8\u30eb\u304c\u8a18\u9332\u3055\u308c\u308b\u3002<\/li>\n<li><strong>\u30b5\u30f3\u30d7\u30eb\u3092\u7d39\u4ecb\u3059\u308b\uff1a<\/strong> \u30ac\u30b9\u30b5\u30f3\u30d7\u30eb\u306f\u3001\u5727\u529b\u8a08\u3067\u6e2c\u5b9a\u3055\u308c\u308b\u6240\u671b\u306e\u5206\u5727\u306b\u9054\u3059\u308b\u307e\u3067\u3001\u30ac\u30b9\u30dc\u30f3\u30d9\u307e\u305f\u306f\u53ce\u96c6\u5bb9\u5668\u304b\u3089\u30bb\u30eb\u306b\u5c0e\u5165\u3055\u308c\u308b\u3002\u5727\u529b\u306f\u30ac\u30b9\u306e\u6fc3\u5ea6\u3092\u6c7a\u5b9a\u3059\u308b\u3002\u7d14\u30ac\u30b9\u306e\u5834\u5408\u300110\uff5e100torr\u306e\u5727\u529b\u304c\u9069\u5f53\u3067\u3042\u308d\u3046\u3002\u6df7\u5408\u30ac\u30b9\u4e2d\u306e\u5fae\u91cf\u6210\u5206\u306e\u5834\u5408\u306f\u3001\u3088\u308a\u9ad8\u3044\u5168\u5727\u304c\u5fc5\u8981\u306a\u5834\u5408\u304c\u3042\u308b\u3002<\/li>\n<li><strong>\u30b9\u30da\u30af\u30c8\u30e9\u30e0\u3092\u7372\u5f97\u3059\u308b<\/strong> \u30bb\u30eb\u3092\u5206\u5149\u8a08\u306b\u30bb\u30c3\u30c8\u3057\u3001\u30b5\u30f3\u30d7\u30eb\u306e\u30b9\u30da\u30af\u30c8\u30eb\u3092\u53d6\u5f97\u3059\u308b\u3002<\/li>\n<\/ol>\n<h3 id=\"unique-features-of-gas-phase-spectra\">\u6c17\u76f8\u30b9\u30da\u30af\u30c8\u30eb\u306e\u30e6\u30cb\u30fc\u30af\u306a\u7279\u5fb4<\/h3>\n<p>\u6c17\u76f8\u30b9\u30da\u30af\u30c8\u30eb\u306e\u6700\u3082\u9855\u8457\u306a\u7279\u5fb4\u306f\u3001\u305d\u306e\u5fae\u7d30\u69cb\u9020\u3067\u3042\u308b\u3002\u6db2\u4f53\u3067\u898b\u3089\u308c\u308b\u5e83\u3044\u632f\u52d5\u30d0\u30f3\u30c9\u306f\u3001\u4e00\u9023\u306e\u92ed\u3044\u7dda\u306b\u5206\u89e3\u3055\u308c\u308b\u3002HCl\u306e\u3088\u3046\u306a\u5358\u7d14\u306a2\u539f\u5b50\u5206\u5b50\u306e\u5834\u5408\u3001\u3053\u308c\u306f\u4e2d\u592e\u306e\u30ae\u30e3\u30c3\u30d7\u306e\u4e21\u5074\u306b\u3042\u308b2\u672c\u306e \"\u5206\u5c90 \"\u7dda\uff08P\u5206\u5c90\u3068R\u5206\u5c90\uff09\u3068\u3057\u3066\u73fe\u308c\u308b\u3002\u3088\u308a\u8907\u96d1\u306a\u5206\u5b50\u306e\u5834\u5408\u3001\u69cb\u9020\u306f\u3088\u308a\u8907\u96d1\u306b\u306a\u308b\u304c\u3001\u5206\u5b50\u306e\u6163\u6027\u30e2\u30fc\u30e1\u30f3\u30c8\u3001\u7d50\u5408\u306e\u9577\u3055\u3001\u7d50\u5408\u89d2\u5ea6\u306b\u95a2\u3059\u308b\u8c4a\u5bcc\u306a\u60c5\u5831\u304c\u542b\u307e\u308c\u3066\u3044\u308b\u3002\u3053\u306e\u30ec\u30d9\u30eb\u306e\u8a73\u7d30\u306a\u60c5\u5831\u306f\u3001\u57fa\u790e\u7684\u306a\u7269\u7406\u5316\u5b66\u306e\u7814\u7a76\u306b\u3068\u3063\u3066\u306f\u975e\u5e38\u306b\u8cb4\u91cd\u3067\u3042\u308b\u304c\u3001\u65e5\u5e38\u7684\u306a\u5b9a\u6027\u540c\u5b9a\u306b\u306f\u4e0d\u5fc5\u8981\u306a\u8907\u96d1\u3055\u3067\u3042\u308b\u3053\u3068\u304c\u591a\u3044\u3002<\/p>\n<h2 id=\"method-7-advanced-and-specialized-reflectance-techniques\">\u65b9\u6cd57\uff1a\u9ad8\u5ea6\u3067\u7279\u6b8a\u306a\u53cd\u5c04\u7387\u6280\u8853<\/h2>\n<p>\u4e00\u822c\u7684\u306a\u624b\u6cd5\u4ee5\u5916\u306b\u3082\u3001\u900f\u904e\u6cd5\u3084ATR\u6cd5\u3067\u306f\u53d6\u308a\u6271\u3044\u304c\u96e3\u3057\u3044\u3001\u3042\u308b\u3044\u306f\u4e0d\u53ef\u80fd\u306a\u30b5\u30f3\u30d7\u30eb\u3092\u5206\u6790\u3059\u308b\u305f\u3081\u306e\u7279\u6b8a\u306a\u624b\u6cd5\u304c\u3044\u304f\u3064\u304b\u5b58\u5728\u3059\u308b\u3002\u3053\u308c\u3089\u306f\u4e3b\u306b\u53cd\u5c04\u6cd5\u3067\u3042\u308a\u3001\u8a66\u6599\u3092\u900f\u904e\u3059\u308b\u5149\u3067\u306f\u306a\u304f\u3001\u53cd\u5c04\u307e\u305f\u306f\u6563\u4e71\u3059\u308b\u8d64\u5916\u5149\u3092\u6e2c\u5b9a\u3059\u308b\u3002\u3053\u308c\u3089\u306e\u624b\u6cd5\u306b\u306f\u5c02\u7528\u306e\u30a2\u30af\u30bb\u30b5\u30ea\u30fc\u304c\u5fc5\u8981\u3067\u3001\u3053\u308c\u3089\u3092\u7406\u89e3\u3059\u308b\u3053\u3068\u3067\u3001FTIR\u306e\u6709\u7528\u6027\u304c\u56f0\u96e3\u306a\u7814\u7a76\u5206\u91ce\u306b\u3082\u5e83\u304c\u308a\u307e\u3059\u3002\u3055\u307e\u3056\u307e\u306a <a href=\"https:\/\/www.hcftir.com\/ir-sample-preparation-category\/\" rel=\"nofollow\">\u9ad8\u5ea6\u306aFTIR\u524d\u51e6\u7406\u30b5\u30f3\u30d7\u30eb\u524d\u51e6\u7406\u30c4\u30fc\u30eb<\/a> \u3053\u308c\u3089\u306e\u65b9\u6cd5\u3092\u4fc3\u9032\u3059\u308b\u3002<\/p>\n<h3 id=\"diffuse-reflectance-infrared-fourier-transform-spectroscopy-drifts\">\u62e1\u6563\u53cd\u5c04\u8d64\u5916\u30d5\u30fc\u30ea\u30a8\u5909\u63db\u5206\u5149\u6cd5(DRIFTS)<\/h3>\n<p>DRIFTS\u306f\u3001\u30da\u30ec\u30c3\u30c8\u72b6\u306b\u30d7\u30ec\u30b9\u3059\u308b\u3053\u3068\u304c\u56f0\u96e3\u306a\u7c89\u672b\u72b6\u56fa\u4f53\u3084\u3001\u305d\u306e\u307e\u307e\u306e\u5f62\u72b6\u3067\u5206\u6790\u3059\u308b\u306e\u304c\u6700\u9069\u306a\u56fa\u4f53\u306e\u5206\u6790\u306b\u6700\u9069\u306a\u624b\u6cd5\u3067\u3059\u3002\u307e\u305f\u3001\u8868\u9762\u304c\u7c97\u3044\u30b5\u30f3\u30d7\u30eb\u306b\u3082\u6700\u9069\u3067\u3059\u3002<\/p>\n<ul>\n<li><strong>\u539f\u5247\uff1a<\/strong> IR\u30d3\u30fc\u30e0\u306f\u7c89\u672b\u306e\u8868\u9762\u306b\u96c6\u5149\u3055\u308c\u308b\u3002\u5149\u306f\u8a66\u6599\u306e\u4e2d\u306b\u5c11\u3057\u5165\u308a\u3001\u7c92\u5b50\u306b\u3088\u3063\u3066\u3042\u3089\u3086\u308b\u65b9\u5411\u306b\u6563\u4e71\u3055\u308c\u308b\u3002\u3053\u306e\u300c\u6563\u6f2b\u6563\u4e71\u300d\u3055\u308c\u305f\u5149\u306f\u3001\u30b5\u30f3\u30d7\u30eb\u306e\u5438\u53ce\u60c5\u5831\u3092\u6301\u3061\u3001\u4e00\u7d44\u306e\u30df\u30e9\u30fc\u306b\u3088\u3063\u3066\u96c6\u3081\u3089\u308c\u3001\u30c7\u30a3\u30c6\u30af\u30bf\u30fc\u306b\u5c0e\u304b\u308c\u308b\u3002<\/li>\n<li><strong>\u30b5\u30f3\u30d7\u30eb\u306e\u6e96\u5099\uff1a<\/strong> \u8a66\u6599\u306f\u901a\u5e38\u3001KBr\u306e\u3088\u3046\u306a\u975e\u5438\u53ce\u6027\u306e\u7c89\u672b\u3068\u6df7\u305c\u3066\u5e0c\u91c8\u3059\u308b\uff08\u30da\u30ec\u30c3\u30c8\u6cd5\u306b\u4f3c\u3066\u3044\u308b\u304c\u3001\u52a0\u5727\u3057\u306a\u3044\uff09\u3002\u3053\u3046\u3059\u308b\u3053\u3068\u3067\u3001\u62e1\u6563\u53cd\u5c04\u7387\u3092\u9ad8\u3081\u3001\u30b9\u30da\u30af\u30c8\u30eb\u3092\u6b6a\u307e\u305b\u308b\u93e1\u9762\u53cd\u5c04\u7387\u3092\u6700\u5c0f\u9650\u306b\u6291\u3048\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u3002\u3053\u306e\u6df7\u5408\u7269\u3092\u5c0f\u3055\u306a\u30b5\u30f3\u30d7\u30eb\u30ab\u30c3\u30d7\u306b\u5165\u308c\u308b\u3002\u5fc5\u8981\u306a\u6e96\u5099\u306f\u3001\u5fae\u7d30\u3067\u5747\u4e00\u306a\u7c92\u5b50\u5f84\u3092\u78ba\u4fdd\u3059\u308b\u305f\u3081\u306e\u7c89\u7815\u3060\u3051\u3067\u3042\u308b\u3002<\/li>\n<li><strong>\u30a2\u30d7\u30ea\u30b1\u30fc\u30b7\u30e7\u30f3<\/strong> DRIFTS\u306f\u89e6\u5a92\u7814\u7a76\uff08\u89e6\u5a92\u8868\u9762\u306b\u5438\u7740\u3057\u305f\u5316\u5b66\u7a2e\u306e\u7814\u7a76\uff09\u3001\u5730\u7403\u5316\u5b66\uff08\u571f\u58cc\u3084\u9271\u7269\u306e\u5206\u6790\uff09\u3001\u6cd5\u533b\u5b66\u306a\u3069\u3067\u5e83\u304f\u4f7f\u308f\u308c\u3066\u3044\u308b\u3002<\/li>\n<\/ul>\n<p>\u3053\u306e\u95a2\u6570\u306f\u8a66\u6599\u306e\u53cd\u5c04\u7387\u3068\u6fc3\u5ea6\u3092\u95a2\u4fc2\u4ed8\u3051\u3001\u5358\u7d14\u306a\u53cd\u5c04\u7387\u30d7\u30ed\u30c3\u30c8\u3088\u308a\u3082\u6fc3\u5ea6\u306b\u5bfe\u3057\u3066\u3088\u308a\u76f4\u7dda\u7684\u306a\u30b9\u30da\u30af\u30c8\u30eb\u3092\u63d0\u4f9b\u3059\u308b\u3002<\/p>\n<h3 id=\"specular-reflectance\">\u93e1\u9762\u53cd\u5c04\u7387<\/h3>\n<p>\u93e1\u9762\u53cd\u5c04\u7387\u306f\u3001\u6ed1\u3089\u304b\u3067\u5e73\u3089\u306a\u8868\u9762\u304b\u3089\u306e\u93e1\u306e\u3088\u3046\u306a\u53cd\u5c04\u3092\u6e2c\u5b9a\u3059\u308b\u3002\u5165\u5c04\u89d2\u3068\u53cd\u5c04\u89d2\u306f\u7b49\u3057\u3044\u3002<\/p>\n<ul>\n<li><strong>\u539f\u5247\uff1a<\/strong> IR\u30d3\u30fc\u30e0\u306f\u30b5\u30f3\u30d7\u30eb\u8868\u9762\u304b\u3089\u76f4\u63a5\u53cd\u5c04\u3055\u308c\u308b\u3002\u3053\u308c\u306f\u3001\u91d1\u5c5e\u30d1\u30cd\u30eb\u4e0a\u306e\u8584\u3044\u30dd\u30ea\u30de\u30fc\u819c\u306e\u3088\u3046\u306a\u3001\u53cd\u5c04\u57fa\u677f\u4e0a\u306e\u8584\u3044\u30b3\u30fc\u30c6\u30a3\u30f3\u30b0\u306e\u5206\u6790\u306b\u6700\u3082\u52b9\u679c\u7684\u3067\u3042\u308b\u3002<\/li>\n<li><strong>\u30b0\u30ec\u30fc\u30ba\u89d2\u306e\u93e1\u9762\u53cd\u5c04\u7387\uff1a<\/strong> \u7279\u6b8a\u306a\u30d0\u30ea\u30a8\u30fc\u30b7\u30e7\u30f3\u3068\u3057\u3066\u3001\u975e\u5e38\u306b\u9ad8\u3044\u5165\u5c04\u89d2\uff08\u4f8b\u3048\u3070\u300180-85\u00b0\uff09\u3092\u4f7f\u7528\u3057\u307e\u3059\u3002\u53cd\u5c04\u5438\u53ce\u8d64\u5916\u5206\u5149\u6cd5(RAIRS)\u3068\u547c\u3070\u308c\u308b\u3053\u306e\u624b\u6cd5\u306f\u3001\u91d1\u5c5e\u8868\u9762\u306e\u975e\u5e38\u306b\u8584\u3044\u819c(\u5358\u4e00\u5206\u5b50\u5c64\u3067\u3055\u3048\u3082)\u306b\u5bfe\u3057\u3066\u975e\u5e38\u306b\u654f\u611f\u3067\u3059\u3002\u8868\u9762\u79d1\u5b66\u306b\u304a\u3051\u308b\u5f37\u529b\u306a\u30c4\u30fc\u30eb\u3067\u3042\u308b\u3002<\/li>\n<li><strong>\u30b5\u30f3\u30d7\u30eb\u306e\u6e96\u5099\uff1a<\/strong> \u552f\u4e00\u306e\u6761\u4ef6\u306f\u3001\u6ed1\u3089\u304b\u3067\u53cd\u5c04\u6027\u306e\u3042\u308b\u30b5\u30f3\u30d7\u30eb\u8868\u9762\u3067\u3042\u308b\u3002<\/li>\n<\/ul>\n<h3 id=\"photoacoustic-spectroscopy-pas\">\u5149\u97f3\u97ff\u5206\u5149\u6cd5 (PAS)<\/h3>\n<p>PAS\u306f\u3001\u6975\u3081\u3066\u4e0d\u900f\u660e\u306a\u7269\u8cea\u3001\u751f\u4f53\u7d44\u7e54\u3001\u4e0d\u898f\u5247\u306a\u5f62\u72b6\u306e\u7269\u4f53\u306a\u3069\u3001\u4e8b\u5b9f\u4e0a\u3042\u3089\u3086\u308b\u5f62\u72b6\u306e\u30b5\u30f3\u30d7\u30eb\u3092\u5206\u6790\u3067\u304d\u308b\u30e6\u30cb\u30fc\u30af\u306a\u975e\u7834\u58ca\u6280\u8853\u3067\u3042\u308b\u3002\u8d64\u5916\u30b9\u30da\u30af\u30c8\u30eb\u3092\u300c\u898b\u308b\u300d\u306e\u3067\u306f\u306a\u304f\u3001\u300c\u805e\u304f\u300d\u306e\u3067\u3042\u308b\u3002<\/p>\n<ul>\n<li><strong>\u539f\u5247\uff1a<\/strong> \u8a66\u6599\u306f\u3001\u30d8\u30ea\u30a6\u30e0\u306e\u3088\u3046\u306a\u4e0d\u6d3b\u6027\u30ac\u30b9\u3092\u542b\u3080\u5bc6\u9589\u3055\u308c\u305f\u30c1\u30e3\u30f3\u30d0\u30fc\u5185\u306b\u7f6e\u304b\u308c\u308b\u3002\u8a66\u6599\u306b\u306f\u5206\u5149\u5668\u304b\u3089\u5909\u8abf\u3055\u308c\u305f\u8d64\u5916\u7dda\u30d3\u30fc\u30e0\u304c\u7167\u5c04\u3055\u308c\u308b\u3002\u8a66\u6599\u304c\u7279\u5b9a\u306e\u5468\u6ce2\u6570\u306e\u8d64\u5916\u7dda\u3092\u5438\u53ce\u3059\u308b\u3068\u3001\u767a\u71b1\u3059\u308b\u3002\u3053\u306e\u71b1\u304c\u5468\u56f2\u306e\u6c17\u4f53\u306b\u4f1d\u308f\u308a\u3001\u6c17\u4f53\u304c\u81a8\u5f35\u3057\u3066\u5727\u529b\u6ce2\uff08\u97f3\uff09\u304c\u767a\u751f\u3059\u308b\u3002\u30c1\u30e3\u30f3\u30d0\u30fc\u5185\u306e\u9ad8\u611f\u5ea6\u30de\u30a4\u30af\u30ed\u30db\u30f3\u304c\u3053\u306e\u97f3\u3092\u691c\u51fa\u3059\u308b\u3002\u97f3\u306e\u5f37\u3055\u306f\u3001\u5438\u53ce\u3055\u308c\u305f\u5149\u306e\u91cf\u306b\u6bd4\u4f8b\u3059\u308b\u3002\u3059\u3079\u3066\u306e\u8d64\u5916\u5468\u6ce2\u6570\u3092\u30b9\u30ad\u30e3\u30f3\u3059\u308b\u3053\u3068\u3067\u3001\u5149\u97f3\u97ff\u8d64\u5916\u30b9\u30da\u30af\u30c8\u30eb\u304c\u751f\u6210\u3055\u308c\u308b\u3002<\/li>\n<li><strong>\u30b5\u30f3\u30d7\u30eb\u306e\u6e96\u5099\uff1a<\/strong> \u57fa\u672c\u7684\u306b\u306f\u4f55\u3082\u5fc5\u8981\u306a\u3044\u3002\u8a66\u6599\u3092\u30bb\u30eb\u306b\u5165\u308c\u308b\u3060\u3051\u3067\u3059\u3002\u305d\u306e\u305f\u3081\u3001\u7c89\u7815\u3001\u5727\u643e\u3001\u6eb6\u89e3\u3067\u304d\u306a\u3044\u7269\u8cea\u306e\u300c\u305d\u306e\u307e\u307e\u300d\u5206\u6790\u306b\u6700\u9069\u3067\u3059\u3002<\/li>\n<\/ul>\n<p>\u3053\u308c\u3089\u306e\u9ad8\u5ea6\u306a\u624b\u6cd5\u306f\u3001\u8d64\u5916\u5206\u5149\u6cd5\u306e\u9a5a\u304f\u3079\u304d\u9069\u5fdc\u6027\u3092\u793a\u3057\u3066\u3044\u307e\u3059\u3002\u88c5\u7f6e\u3001\u30a2\u30af\u30bb\u30b5\u30ea\u3001\u8abf\u88fd\u6280\u8853\u306e\u9069\u5207\u306a\u7d44\u307f\u5408\u308f\u305b\u3092\u9078\u629e\u3059\u308b\u3053\u3068\u306b\u3088\u308a\u3001\u5316\u5b66\u8005\u306f\u307b\u3068\u3093\u3069\u3059\u3079\u3066\u306e\u7269\u8cea\u304b\u3089\u610f\u5473\u306e\u3042\u308b\u69cb\u9020\u30b9\u30c8\u30fc\u30ea\u30fc\u3092\u5f15\u304d\u51fa\u3059\u3053\u3068\u304c\u3067\u304d\u308b\u3002<\/p>\n<h2 id=\"frequently-asked-questions-faq\">\u3088\u304f\u3042\u308b\u8cea\u554f\uff08FAQ\uff09<\/h2>\n<p><strong>1.\u306a\u305cKBr\u30da\u30ec\u30c3\u30c8\u306f\u6fc1\u308a\u3001\u30b9\u30da\u30af\u30c8\u30eb\u306f\u60aa\u3044\u306e\u3067\u3059\u304b\uff1f<\/strong> \u30da\u30ec\u30c3\u30c8\u304c\u767d\u6fc1\u3059\u308b\u306e\u306f\u3001\u6c34\u5206\u306e\u6df7\u5165\u304b\u7c89\u7815\u4e0d\u8db3\u304c\u539f\u56e0\u3067\u3042\u308b\u3053\u3068\u304c\u591a\u3044\u3002KBr\u306f\u5438\u6e7f\u6027\u304c\u9ad8\u3044\u305f\u3081\u3001\u5341\u5206\u306b\u4e7e\u71e5\u3055\u305b\u3066\u304a\u304f\u5fc5\u8981\u304c\u3042\u308b\u3002\u8a66\u6599\u306e\u7c92\u5b50\u304c\u5927\u304d\u3059\u304e\u308b\u3068\u3001\u8d64\u5916\u5149\u304c\u6563\u4e71\u3057\u3001\u30d9\u30fc\u30b9\u30e9\u30a4\u30f3\u304c\u50be\u3044\u305f\u308a\u3001\u30d4\u30fc\u30af\u306e\u5b9a\u7fa9\u304c\u60aa\u304f\u306a\u308a\u307e\u3059\u3002\u8a66\u6599\u3068KBr\u306e\u6df7\u5408\u7269\u3092\u3088\u308a\u5f37\u529b\u306b\u3001\u3088\u308a\u9577\u6642\u9593\u7c89\u7815\u3057\u3066\u307f\u3066\u304f\u3060\u3055\u3044\u3002<\/p>\n<p><strong>2.\u79c1\u306e\u30b9\u30da\u30af\u30c8\u30eb\u306e3400cm-\u00b9\u4ed8\u8fd1\u306b\u3042\u308b\u5927\u304d\u304f\u30d6\u30ed\u30fc\u30c9\u306a\u30d4\u30fc\u30af\u306f\u4f55\u3092\u610f\u5473\u3059\u308b\u306e\u3067\u3057\u3087\u3046\u304b\uff1f<\/strong> 3200-3600cm\u00b9\u306e\u5f37\u3044\u30d6\u30ed\u30fc\u30c9\u306a\u5438\u53ce\u5e2f\u306f\u3001\u6c34\u306b\u3088\u308bO-H\u4f38\u7e2e\u632f\u52d5\u306e\u5178\u578b\u7684\u306a\u7279\u5fb4\u3067\u3042\u308b\u30021640cm-\u00b9\u4ed8\u8fd1\u306b\u306f\u3001H-O-H\u5c48\u66f2\u30e2\u30fc\u30c9\u306b\u3088\u308b\u3001\u3088\u308a\u5c0f\u3055\u304f\u30b7\u30e3\u30fc\u30d7\u306a\u30d4\u30fc\u30af\u304c\u73fe\u308c\u308b\u3053\u3068\u304c\u3042\u308a\u307e\u3059\u3002\u3053\u308c\u306f\u3001\u8a66\u6599\u3001KBr\u3001\u307e\u305f\u306f\u5869\u30d7\u30ec\u30fc\u30c8\u304c\u5341\u5206\u306b\u4e7e\u71e5\u3057\u3066\u3044\u306a\u3044\u3053\u3068\u3092\u793a\u3057\u3066\u3044\u307e\u3059\u3002<\/p>\n<p><strong>3.\u8d64\u5916\u5206\u5149\u6cd5\u306e\u6eb6\u5a92\u3068\u3057\u3066\u6c34\u3092\u4f7f\u3046\u3053\u3068\u306f\u3067\u304d\u307e\u3059\u304b\uff1f<\/strong> \u4e00\u822c\u7684\u306b\u306f\u3001\u305d\u3046\u3067\u306f\u306a\u3044\u3002\u6c34\u306f\u975e\u5e38\u306b\u5f37\u3044\u8d64\u5916\u5438\u53ce\u4f53\u3067\u3042\u308a\u3001\u305d\u306e\u5e45\u5e83\u3044\u30d4\u30fc\u30af\u306f\u4e2d\u8d64\u5916\u30b9\u30da\u30af\u30c8\u30eb\u306e\u5927\u90e8\u5206\u3092\u96a0\u3057\u3066\u3057\u307e\u3046\u3002\u3055\u3089\u306b\u3001NaCl\u3084KBr\u306e\u3088\u3046\u306a\u4e00\u822c\u7684\u306aIR\u7a93\u6750\u306e\u591a\u304f\u306f\u6c34\u306b\u6eb6\u3051\u308b\u305f\u3081\u3001\u7834\u58ca\u3055\u308c\u3066\u3057\u307e\u3044\u307e\u3059\u3002\u6c34\u6eb6\u6db2\u306e\u5834\u5408\u3001\u6c34\u306b\u6eb6\u3051\u306a\u3044\u7d50\u6676\uff08\u30c0\u30a4\u30e4\u30e2\u30f3\u30c9\u3084ZnSe\u306a\u3069\uff09\u3092\u4f7f\u3063\u305fATR\u6280\u8853\u3092\u4f7f\u3046\u304b\u3001CaF\u2082\u306e\u3088\u3046\u306a\u6c34\u306b\u6eb6\u3051\u306a\u3044\u7a93\u3092\u6301\u3064\u7279\u6b8a\u306a\u900f\u904e\u30bb\u30eb\u3092\u4f7f\u3046\u5fc5\u8981\u304c\u3042\u308a\u307e\u3059\u3002<\/p>\n<p><strong>4.ATR\u30b9\u30da\u30af\u30c8\u30eb\u3068\u900f\u904e\uff08KBr\u30da\u30ec\u30c3\u30c8\uff09\u30b9\u30da\u30af\u30c8\u30eb\u306e\u4e3b\u306a\u9055\u3044\u306f\uff1f<\/strong> \u76f8\u5bfe\u7684\u306a\u30d4\u30fc\u30af\u5f37\u5ea6\u304c\u7570\u306a\u308b\u3002ATR\u30b9\u30da\u30af\u30c8\u30eb\u3067\u306f\u3001\u6ce2\u6570\u306e\u4f4e\u3044\uff08\u6ce2\u9577\u306e\u9577\u3044\uff09\u30d4\u30fc\u30af\u306f\u3001\u6ce2\u6570\u306e\u9ad8\u3044\u30d4\u30fc\u30af\u306b\u6bd4\u3079\u3066\u76f8\u5bfe\u7684\u306b\u5f37\u304f\u898b\u3048\u308b\u3002\u3053\u308c\u306f\u3001\u30a8\u30d0\u30cd\u30c3\u30bb\u30f3\u30c8\u6ce2\u306e\u900f\u904e\u6df1\u5ea6\u306b\u95a2\u9023\u3059\u308b\u7269\u7406\u7684\u306a\u30a2\u30fc\u30c1\u30d5\u30a1\u30af\u30c8\u3067\u3042\u308b\u3002\u307b\u3068\u3093\u3069\u306e\u6700\u65b0\u306e\u30bd\u30d5\u30c8\u30a6\u30a7\u30a2\u306b\u306f\u3001\u30b9\u30da\u30af\u30c8\u30eb\u3092\u5f93\u6765\u306e\u900f\u904e\u30b9\u30da\u30af\u30c8\u30eb\u306b\u8fd1\u3065\u3051\u3066\u30e9\u30a4\u30d6\u30e9\u30ea\u30fc\u691c\u7d22\u3092\u884c\u3046\u305f\u3081\u306e\u300cATR\u88dc\u6b63\u300d\u6a5f\u80fd\u304c\u3042\u308b\u3002<\/p>\n<p><strong>5.NaCl\u307e\u305f\u306fKBr\u30bd\u30eb\u30c8\u30d7\u30ec\u30fc\u30c8\u306e\u30af\u30ea\u30fc\u30cb\u30f3\u30b0\u65b9\u6cd5\u3092\u6559\u3048\u3066\u304f\u3060\u3055\u3044\u3002<\/strong> \u6c34\u306f\u7d76\u5bfe\u306b\u4f7f\u7528\u3057\u306a\u3044\u3053\u3068\u3002\u30bd\u30eb\u30c8\u30fb\u30d7\u30ec\u30fc\u30c8\u3092\u30af\u30ea\u30fc\u30cb\u30f3\u30b0\u3059\u308b\u306b\u306f\u3001\u30d2\u30e5\u30fc\u30e0\u30d5\u30fc\u30c9\u306e\u4e2d\u3067\u3001\u4e7e\u71e5\u30a2\u30bb\u30c8\u30f3\u3084\u30b8\u30af\u30ed\u30ed\u30e1\u30bf\u30f3\u306a\u3069\u306e\u4e7e\u71e5\u3057\u305f\u63ee\u767a\u6027\u6eb6\u5264\u3067\u6e7f\u3089\u305b\u305f\u3001\u67d4\u3089\u304b\u304f\u7cf8\u304f\u305a\u306e\u51fa\u306a\u3044\u30c6\u30a3\u30c3\u30b7\u30e5\u3084\u5e03\u3067\u512a\u3057\u304f\u62ed\u3044\u3066\u304f\u3060\u3055\u3044\u3002\u5186\u307e\u305f\u306f8\u306e\u5b57\u3092\u63cf\u304f\u3088\u3046\u306b\u3001\u900f\u660e\u306b\u306a\u308b\u307e\u3067\u78e8\u304f\u3002\u8868\u9762\u306b\u6307\u7d0b\u304c\u4ed8\u304b\u306a\u3044\u3088\u3046\u306b\u5e38\u306b\u7aef\u3092\u6301\u3063\u3066\u6271\u3044\u3001\u4e7e\u71e5\u3057\u305f\u72b6\u614b\u3092\u4fdd\u3064\u305f\u3081\u306b\u30c7\u30b7\u30b1\u30fc\u30bf\u30fc\u306b\u5165\u308c\u3066\u4fdd\u7ba1\u3059\u308b\u3002<\/p>\n<p><strong>6.IR\u30b9\u30da\u30af\u30c8\u30eb\u306b\u5fc5\u8981\u306a\u30b5\u30f3\u30d7\u30eb\u91cf\u306f\uff1f<\/strong> \u305d\u308c\u306f\u6280\u8853\u306b\u5927\u304d\u304f\u4f9d\u5b58\u3059\u308b\u3002KBr\u30da\u30ec\u30c3\u30c8\u306a\u30891\uff5e2\u30df\u30ea\u30b0\u30e9\u30e0\u3067\u3088\u3044\u3002\u30de\u30eb\u306e\u5834\u5408\u306f\u3001\u304a\u305d\u3089\u304f2\uff5e5\u30df\u30ea\u30b0\u30e9\u30e0\u3002ATR\u306e\u5834\u5408\u3001\u5fc5\u8981\u306a\u91cf\u306f1\u30df\u30ea\u30b0\u30e9\u30e0\u4ee5\u4e0b\u3067\u3001\u7d50\u6676\u8868\u9762\u3092\u8986\u3046\u306e\u306b\u5341\u5206\u306a\u91cf\u3067\u3042\u308b\u3053\u3068\u304c\u591a\u3044\u3002\u3053\u306e\u3088\u3046\u306a\u5fae\u91cf\u306e\u7269\u8cea\u304b\u3089\u8a73\u7d30\u306a\u69cb\u9020\u60c5\u5831\u3092\u5f97\u308b\u3053\u3068\u304c\u3067\u304d\u308b\u306e\u306f\u3001FTIR\u306e\u6700\u5927\u306e\u5f37\u307f\u3067\u3042\u308b\u3002<\/p>\n<h2 id=\"a-final-reflection-on-practice-and-precision\">\u7df4\u7fd2\u3068\u7cbe\u5ea6\u306b\u95a2\u3059\u308b\u6700\u5f8c\u306e\u8003\u5bdf<\/h2>\n<p>\u8d64\u5916\u5206\u5149\u6cd5\u306e\u305f\u3081\u306e\u8a66\u6599\u8abf\u88fd\u306e\u69d8\u3005\u306a\u65b9\u6cd5\u3092\u901a\u3057\u3066\u306e\u65c5\u306f\u3001\u4e2d\u5fc3\u7684\u306a\u771f\u5b9f\u3092\u660e\u3089\u304b\u306b\u3059\u308b\uff1a\u88c5\u7f6e\u306f\u53d7\u52d5\u7684\u306a\u89b3\u5bdf\u8005\u3067\u3042\u308a\u3001\u88c5\u7f6e\u304c\u8a18\u9332\u3059\u308b\u30b9\u30da\u30af\u30c8\u30eb\u306f\u6211\u3005\u306e\u884c\u52d5\u306e\u76f4\u63a5\u7684\u306a\u7d50\u679c\u3067\u3042\u308b\u3002\u88c5\u7f6e\u306f\u53d7\u52d5\u7684\u306a\u89b3\u5bdf\u8005\u3067\u3042\u308a\u3001\u8a18\u9332\u3055\u308c\u308b\u30b9\u30da\u30af\u30c8\u30eb\u306f\u6211\u3005\u306e\u884c\u52d5\u306e\u76f4\u63a5\u7684\u306a\u7d50\u679c\u306a\u306e\u3067\u3042\u308b\u3002\u3053\u306e\u30d7\u30ed\u30bb\u30b9\u306f\u3001\u6025\u304c\u306a\u3051\u308c\u3070\u306a\u3089\u306a\u3044\u5358\u306a\u308b\u96d1\u7528\u3067\u306f\u306a\u304f\u3001\u79d1\u5b66\u7684\u63a2\u7a76\u306e\u4e0d\u53ef\u6b20\u306a\u4e00\u90e8\u306a\u306e\u3067\u3042\u308b\u3002\u30da\u30ec\u30c3\u30c8\u304b\u30de\u30eb\u304b\u3001ATR\u304b\u900f\u904e\u304b\u3001\u6eb6\u5a92A\u304b\u6eb6\u5a92B\u304b\u3001\u305d\u308c\u305e\u308c\u306e\u9078\u629e\u304c\u3001\u5206\u5b50\u304c\u8a9e\u308b\u30b9\u30c8\u30fc\u30ea\u30fc\u3092\u5f62\u4f5c\u308b\u3002\u719f\u616e\u3055\u308c\u3001\u5b9f\u8df5\u3055\u308c\u305f\u30a2\u30d7\u30ed\u30fc\u30c1\u306f\u3001\u30b5\u30f3\u30d7\u30eb\u8abf\u88fd\u3092\u30d5\u30e9\u30b9\u30c8\u30ec\u30fc\u30b7\u30e7\u30f3\u306e\u6e90\u304b\u3089\u3001\u767a\u898b\u306e\u305f\u3081\u306e\u5f37\u529b\u306a\u30c4\u30fc\u30eb\u3078\u3068\u5909\u3048\u308b\u3002\u30b7\u30e3\u30fc\u30d7\u306a\u30d4\u30fc\u30af\u3068\u5e73\u5766\u306a\u30d9\u30fc\u30b9\u30e9\u30a4\u30f3\u3092\u6301\u3064\u6700\u7d42\u30b9\u30da\u30af\u30c8\u30eb\u306e\u660e\u77ad\u3055\u306f\u3001\u30b9\u30da\u30af\u30c8\u30ed\u30e1\u30fc\u30bf\u30fc\u306e\u30d1\u30ef\u30fc\u3060\u3051\u3067\u306a\u304f\u3001\u305d\u306e\u524d\u306b\u7acb\u3064\u5206\u6790\u8005\u306e\u6ce8\u610f\u6df1\u3055\u3001\u30b9\u30ad\u30eb\u3001\u7406\u89e3\u306e\u8a3c\u3067\u3082\u3042\u308b\u3002\u5b8c\u74a7\u306a\u30b9\u30da\u30af\u30c8\u30eb\u306e\u8ffd\u6c42\u306f\u3001\u8981\u3059\u308b\u306b\u3001\u6df7\u3058\u308a\u3051\u306e\u306a\u3044\u5316\u5b66\u7684\u771f\u5b9f\u306e\u8ffd\u6c42\u306a\u306e\u3067\u3042\u308b\u3002<\/p>\n<h2 id=\"references\">\u53c2\u8003\u6587\u732e<\/h2>\n<p>Harvey, D. (2019).\u5206\u6790\u5316\u5b662.1.Chemistry LibreTexts.)<\/p>\n<p>Matusiewicz, H. (2017).\u7121\u6a5f\u5fae\u91cf\u5143\u7d20\u5206\u6790\u306e\u305f\u3081\u306e\u8a66\u6599\u8abf\u88fd\u3002Pure and Applied Chemistry, 89(5), 629-642. <a href=\"https:\/\/doi.org\/10.1515\/pac-2016-0916\" rel=\"nofollow\">https:\/\/doi.org\/10.1515\/pac-2016-0916<\/a><\/p>\n<p>Popiel, S. (2024).\u6709\u6a5f\u91d1\u5c5e\u9aa8\u683c\u3092\u5438\u7740\u5264\u3068\u3059\u308b\u5206\u6790\u7528\u6db2\u4f53\u8a66\u6599\u8abf\u88fd\u6280\u8853\u306e\u6982\u8981\u3002Molecules, 29(19), 4752. <a href=\"https:\/\/doi.org\/10.3390\/molecules29194752\" rel=\"nofollow\">https:\/\/doi.org\/10.3390\/molecules29194752<\/a><\/p>\n<p>\u30b9\u30df\u30b9\uff0cB\uff0eKBr\u30da\u30ec\u30c3\u30c8\uff1a\u5931\u308f\u308c\u305f\u82b8\u8853\u3002Spectroscopy, 30(4), 29-33.<\/p>\n<p>\u30b9\u30df\u30b9\uff0cB\uff0e\u30de\u30eb\uff1a\u5931\u308f\u308c\u3001\u305d\u3057\u3066\u898b\u51fa\u3055\u308c\u305f\u82b8\u8853\u3002Spectroscopy, 33(11), 22-26.<\/p>\n<p>\u30b9\u30da\u30af\u30c8\u30ed\u30b9\u30b3\u30d4\u30fc\u30fb\u30e8\u30fc\u30ed\u30c3\u30d1(2023).\u81e8\u5e8a\u7814\u7a76\u304a\u3088\u3073\u6bd2\u6027\u5b66\u306b\u304a\u3051\u308b\u6db2\u4f53\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\u30fb\u30bf\u30f3\u30c7\u30e0\u8cea\u91cf\u5206\u6790\u306e\u305f\u3081\u306e\u30b5\u30f3\u30d7\u30eb\u8abf\u88fd\u5b9f\u8df5\u30ac\u30a4\u30c9\u3002 <a href=\"https:\/\/www.spectroscopyeurope.com\/article\/practical-guide-sample-preparation-liquid-chromatography-tandem-mass-spectrometry-clinical\" rel=\"nofollow\">https:\/\/www.spectroscopyeurope.com\/article\/practical-guide-sample-preparation-liquid-chromatography-tandem-mass-spectrometry-clinical<\/a><\/p>\n<p>Stuart, B. H. (2004).\u8d64\u5916\u5206\u5149\u6cd5\uff1aFundamentals and applications.John Wiley &amp; Sons. <a href=\"https:\/\/doi.org\/10.1002\/0470011138\" rel=\"nofollow\">https:\/\/doi.org\/10.1002\/0470011138<\/a><\/p>\n<p>Vickers, T. J., &amp; Mann, C. K. (2004).\u8d64\u5916\u5206\u5149\u6cd5\u306b\u304a\u3051\u308b\u8a66\u6599\u306e\u53d6\u308a\u6271\u3044\u3002J. M. Chalmers &amp; P. R. Griffiths (Eds.), Handbook of Vibrational Spectroscopy.John Wiley &amp; Sons. <a href=\"https:\/\/doi.org\/10.1002\/0470027320.s0201\" rel=\"nofollow\">https:\/\/doi.org\/10.1002\/0470027320.s0201<\/a><\/p>","protected":false},"excerpt":{"rendered":"<p>\u6982\u8981 \u8d64\u5916\uff08IR\uff09\u5206\u5149\u6cd5\u306f\u3001\u8d64\u5916\u7dda\u306e\u5438\u53ce\u3092\u6e2c\u5b9a\u3059\u308b\u3053\u3068\u306b\u3088\u3063\u3066\u5316\u5b66\u7269\u8cea\u3092\u540c\u5b9a\u3059\u308b\u305f\u3081\u306e\u5f37\u529b\u306a\u5206\u6790\u6280\u8853\u3067\u3042\u308b\u3002\u3057\u304b\u3057\u3001\u8d64\u5916\u30b9\u30da\u30af\u30c8\u30eb\u306e\u54c1\u8cea\u3068\u89e3\u91c8\u306e\u3057\u3084\u3059\u3055\u306f\u3001\u57fa\u672c\u7684\u306b\u8a66\u6599\u306e\u7dbf\u5bc6\u306a\u8abf\u88fd\u306b\u4f9d\u5b58\u3057\u3066\u3044\u307e\u3059\u3002\u672c\u66f8\u3067\u306f\u3001\u30d5\u30fc\u30ea\u30a8\u5909\u63db\u8d64\u5916\u5206\u5149\uff08FTIR\uff09\u5206\u6790\u7528\u306e\u8a66\u6599\u8abf\u88fd\u306b\u95a2\u308f\u308b\u624b\u6cd5\u3092\u5305\u62ec\u7684\u306b\u691c\u8a0e\u3057\u307e\u3059\u3002\u56fa\u4f53\u3001\u6db2\u4f53\u3001\u6c17\u4f53\u306b\u9069\u7528\u53ef\u80fd\u306a\u3001\u5b9f\u7e3e\u306e\u3042\u308b7\u3064\u306e\u30c6\u30af\u30cb\u30c3\u30af\u3092\u7cfb\u7d71\u7684\u306b\u691c\u8a0e\u3057\u3001\u305d\u308c\u305e\u308c\u306e\u7406\u8ad6\u7684\u80cc\u666f\u3068\u5b9f\u969b\u7684\u306a\u5b9f\u65bd\u65b9\u6cd5\u3092\u660e\u3089\u304b\u306b\u3057\u3066\u3044\u307e\u3059\u3002\u81ed\u5316\u30ab\u30ea\u30a6\u30e0(KBr)\u30da\u30ec\u30c3\u30c8\u3084Nujol\u30de\u30eb\u306e\u4f5c\u6210\u3068\u3044\u3063\u305f\u4f1d\u7d71\u7684\u306a\u624b\u6cd5\u304b\u3089\u3001\u6e1b\u8870\u5168\u53cd\u5c04(ATR)\u306e\u3088\u3046\u306a\u73fe\u4ee3\u7684\u3067\u5408\u7406\u7684\u306a\u30a2\u30d7\u30ed\u30fc\u30c1\u307e\u3067\u7db2\u7f85\u3057\u3066\u3044\u307e\u3059\u3002\u3055\u3089\u306b\u3001[...]\u3092<\/p>","protected":false},"author":1,"featured_media":5989,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[238],"tags":[],"class_list":["post-5988","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-news"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v24.4 - https:\/\/yoast.com\/wordpress\/plugins\/seo\/ -->\n<title>7 Proven Methods: A Guide on How to Prepare Sample for IR Spectroscopy - Hench Technology<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/www.hcftir.com\/ja\/7-proven-methods-a-guide-on-how-to-prepare-sample-for-ir-spectroscopy-article\/\" \/>\n<meta property=\"og:locale\" content=\"ja_JP\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"7 Proven Methods: A Guide on How to Prepare Sample for IR Spectroscopy - Hench Technology\" \/>\n<meta property=\"og:description\" content=\"Abstract Infrared (IR) spectroscopy is a potent analytical technique for identifying chemical substances by measuring their absorption of infrared radiation. 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The quality and interpretability of an IR spectrum, however, are fundamentally dependent on the meticulous preparation of the sample. This document provides a comprehensive examination of the methodologies involved in preparing samples for Fourier Transform Infrared (FTIR) analysis. It systematically explores seven distinct and proven techniques applicable to solids, liquids, and gases, elucidating the theoretical underpinnings and practical execution of each. The discussion covers traditional methods such as the creation of Potassium Bromide (KBr) pellets and Nujol mulls, as well as modern, streamlined approaches like Attenuated Total Reflectance (ATR). 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