{"id":6162,"date":"2025-12-30T09:38:26","date_gmt":"2025-12-30T09:38:26","guid":{"rendered":"https:\/\/www.hcftir.com\/?p=6162"},"modified":"2025-12-30T09:39:39","modified_gmt":"2025-12-30T09:39:39","slug":"whats-the-reason-for-cracking-and-chipping-when-demolding-ir-tablets","status":"publish","type":"post","link":"https:\/\/www.hcftir.com\/es\/whats-the-reason-for-cracking-and-chipping-when-demolding-ir-tablets-article\/","title":{"rendered":"\u00bfA qu\u00e9 se deben las grietas y astillas al desmoldar las pastillas IR?"},"content":{"rendered":"

Siempre hay algunos reci\u00e9n llegados que acaban de empezar a trabajar con Prensa IR de laboratorio<\/a> que plantean estas cuestiones. Hoy compartir\u00e9 contigo las razones y las soluciones.<\/p>\n\n\n\n

\"Desmoldeo<\/figure>\n\n\n\n

Las razones pueden resumirse en cuatro puntos.<\/h2>\n\n\n\n

1. Relaci\u00f3n inadecuada entre la muestra y el KBr<\/h3>\n\n\n\n

Esta es la raz\u00f3n principal.<\/p>\n\n\n\n

Si la proporci\u00f3n de la muestra es demasiado alta, se producir\u00e1 una disminuci\u00f3n de la adhesividad global de la mezcla, y las pastillas prensadas tendr\u00e1n una textura suelta. Durante el desmoldeo, son propensas a agrietarse y a desprender part\u00edculas;<\/p>\n\n\n\n

Si la proporci\u00f3n de KBr es demasiado alta y la muestra no se dispersa uniformemente, tambi\u00e9n habr\u00e1 zonas en las que las part\u00edculas se desprendan por falta de fuerza de adherencia.<\/p>\n\n\n\n

Recomendaci\u00f3n general de proporci\u00f3n: La proporci\u00f3n de masa de las muestras s\u00f3lidas respecto al KBr suele ser de 1:100 a 1:200. Para el experimento de prensado, es necesario realizar m\u00e1s pr\u00e1cticas y realizar los ajustes adecuados de la proporci\u00f3n dentro de un rango determinado.<\/p>\n\n\n\n

2.Molienda y mezcla insuficientes, con part\u00edculas gruesas<\/h3>\n\n\n\n

Las muestras y el KBr no se molieron a fondo, lo que dio lugar a tama\u00f1os de part\u00edcula demasiado grandes. Esto impedir\u00eda que las part\u00edculas se adhirieran estrechamente entre s\u00ed durante el prensado del comprimido, dejando muchos huecos. La estructura de la pastilla quedar\u00eda suelta, y se desmoronar\u00eda y caer\u00eda al retirar el molde por la fuerza.<\/p>\n\n\n\n

Adem\u00e1s, si se introduce humedad durante el proceso de trituraci\u00f3n, o si el propio KBr absorbe humedad, las part\u00edculas se aglutinar\u00e1n, lo que provocar\u00e1 una mezcla desigual y, potencialmente, una resistencia insuficiente en determinadas zonas.<\/p>\n\n\n\n

Soluci\u00f3n: Durante el proceso de molienda, procure operar en un entorno seco. Triture la mezcla hasta que no haya una sensaci\u00f3n evidente de part\u00edculas (normalmente de 3 a 5 minutos), y aseg\u00farese de que la muestra est\u00e1 completamente mezclada con KBr.<\/p>\n\n\n\n

\"Desmoldeo<\/figure>\n\n\n\n

3.Par\u00e1metros inadecuados para la operaci\u00f3n de prensado de comprimidos<\/h3>\n\n\n\n

Presi\u00f3n insuficiente o tiempo de retenci\u00f3n demasiado corto: Una presi\u00f3n insuficiente impide que las part\u00edculas se compriman hasta el punto en que las fuerzas intermoleculares puedan unirlas firmemente; un tiempo de retenci\u00f3n demasiado corto significa que la presi\u00f3n no puede distribuirse uniformemente por toda la l\u00e1mina, lo que da lugar a una estructura interna suelta y a un agrietamiento f\u00e1cil al desmoldar. Las condiciones convencionales son una presi\u00f3n de 10 a 15 MPa y un tiempo de mantenimiento de 1 a 2 minutos.<\/p>\n\n\n\n

Presi\u00f3n excesiva o aplicaci\u00f3n r\u00e1pida de la presi\u00f3n: La presi\u00f3n supera la capacidad del molde y de la muestra, o la aplicaci\u00f3n de presi\u00f3n es demasiado r\u00e1pida. En el interior de la chapa se generar\u00e1n tensiones internas. Cuando se desmolde la l\u00e1mina, la liberaci\u00f3n de tensiones provocar\u00e1 grietas.<\/p>\n\n\n\n

Operaci\u00f3n incorrecta antes de prensar: Al colocar la muestra en el molde, antes de insertar la varilla de prensado, aseg\u00farese de girar la varilla de prensado superior para asegurar que la muestra est\u00e9 uniformemente.<\/p>\n\n\n\n

Operaci\u00f3n de desmoldeo incorrecta: Si la fuerza durante el desmoldeo es demasiado fuerte o desigual, o si la pared interior del molde no est\u00e1 limpia, har\u00e1 que la pel\u00edcula se pegue al molde. Al despegarla, se desgarrar\u00e1 y caer\u00e1 con los restos.<\/p>\n\n\n\n

\"Desmoldeo<\/figure>\n\n\n\n

4.Problemas de calidad del reactivo KBr<\/h3>\n\n\n\n

Si la pureza del KBr utilizado es insuficiente, contiene impurezas o ha absorbido humedad y se ha vuelto grumoso tras un almacenamiento prolongado, afectar\u00e1 directamente al efecto de moldeado de los comprimidos, lo que provocar\u00e1 una textura suelta y un agrietamiento f\u00e1cil.<\/p>\n\n\n\n

Si la pureza del KBr utilizado es insuficiente, contiene impurezas o ha absorbido humedad y se ha vuelto grumoso tras un almacenamiento prolongado, afectar\u00e1 directamente al efecto de moldeado de los comprimidos, lo que provocar\u00e1 una textura suelta y un agrietamiento f\u00e1cil. Soluci\u00f3n: Seleccione el reactivo KBr de grado espectral de Tianjin Hengchuangda Company. Antes de usarlo, s\u00e9quelo a 110-120\u2103 durante 2-4 horas. Al moler y mezclar las muestras, operar bajo una l\u00e1mpara de secado por infrarrojos. Gu\u00e1rdelo en un desecador para uso diario y copia de seguridad. \u00bfLo ha aprendido?<\/p>\n\n\n\n

\"Desmoldeo<\/figure>","protected":false},"excerpt":{"rendered":"

Siempre hay algunos reci\u00e9n llegados que acaban de empezar a trabajar con la prensa IR de laboratorio que plantean estas preguntas. Hoy compartir\u00e9 con ustedes las razones y las soluciones. Las razones pueden resumirse en cuatro puntos. 1. Proporci\u00f3n inadecuada de la muestra con respecto al KBr \u00c9sta es la raz\u00f3n principal. Si la proporci\u00f3n de la muestra [...]<\/p>","protected":false},"author":1,"featured_media":6167,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[238],"tags":[],"class_list":["post-6162","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-news"],"yoast_head":"\nWhat's the reason for cracking and chipping when demolding IR tablets? - Hench Technology<\/title>\n<meta name=\"description\" content=\"Explore the causes of cracking and chipping when demolding IR tablets. 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